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RESEARCH PAPER · Crystal Growth & Design · 2011

Hydrothermal Synthesis and Structural Characterization of Organically Templated Uranyl Diphosphonate Compounds

Pius O. Adelani, Allen G. Oliver, Thomas E. Albrecht‐Schmitt

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Hydrothermal Synthesis and Structural Characterization of Organically Templated Uranyl Diphosphonate CompoundsOriginalSyntheses of Uranyl Diphosphonate Compounds Using Encapsulated Cations as Structure Directing Agents59Heterobimetallic Copper(II) Uranyl Carboxyphenylphosphonates67Crystal Engineering with the Uranyl Cation III. Mixed Aliphatic Dicarboxylate/Aromatic Dipyridyl Coordination Polymers: Synthesis, Structures, and Speciation74Synthesis, Crystal Structures, and Luminescence and Magnetic Properties of 3D Chiral and Achiral Lanthanide Diphosphonates Containing Left- and Right-Handed Helical Chains51Coordination Polymers and Frameworks in Uranyl Ion Complexes with Sulfonates and Cucurbit[6]uril32Metal-Controlled Assembly of Uranyl Diphosphonates toward the Design of Functional Uranyl Nanotubules77In-Situ Raman Spectroscopy Studies of Room-Temperature and Hydrothermal Reactions1The structure and properties of a 3D pillared-layered metal organic framework Cu(II)-diphosphonate11Barium uranyl diphosphonates16Thorium and uranium diphosphonates: Syntheses, structures, and spectroscopic properties32Syntheses, structures and luminescent properties of two one-dimensional uranium oxyfluorides12Tailor-Made Zinc Uranyl Diphosphonates from Layered to Framework Structures46Ionothermal synthesis of uranyl compounds that incorporate imidazole derivatives14One-Dimensional Uranyl-2,2′-bipyridine Coordination Polymer with Cation–Cation Interactions: (UO2)2(2,2′-bpy)(CH3CO2)(O)(OH)44The First Uranyl Arsonates Featuring Heterometallic Cation–Cation Interactions with UVI═O–ZnII Bonding40Mixed-solvothermal synthesis, structures, luminescent and surface photovoltage properties of four new transition metal diphosphonates with a 3D supramolecular structure17Layered Uranyl Coordination Polymers Rigidly Pillared by Diphosphonates36From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange82Uranium diphosphonates templated by interlayer organic amines22Correlations and Differences between Uranium(VI) Arsonates and Phosphonates25Structures and Spectroscopy Studies of Two M(II)-Phosphonate Coordination Polymers Based on Alkaline Earth Metals (M = Ba, Mg)8Sulfonate Complexes of Actinide Ions: Structural Diversity in Uranyl Complexes with 2-Sulfobenzoate71An exploration of homo- and heterometallic UO 2 2+ hybrid materials containing chelidamic acid: synthesis, structure, and luminescence studies32Employing tripodal carboxylate ligand to construct Co(ii) coordination networks modulated by N-donor ligands: syntheses, structures and magnetic properties24One- to three-dimensional uranyl–organic assemblies with 3-sulfophthalic and 5-sulfoisophthalic acids29Two new uranyl fluoride complexes with UVIO–alkali (Na, Cs) interactions: Experimental and theoretical studies9Syntheses and Structures of a Series of Uranyl Phosphonates and Sulfonates: An Insight into Their Correlations and Discrepancies75Two Systems of [DabcoH2]2+/[PipH2]2+–Uranyl–Oxalate Showing Reversible Crystal-to-Crystal Transformations Controlled by the Diammonium/Uranyl/Oxalate Ratios in Aqueous Solutions ([DabcoH2]2+ = 1,4-Diazabicyclo-[2.2.2]-octaneH2 and [PipH2]2+ = PiperazineH2)23Syntheses, structures and luminescent properties of two organic templated uranyl phosphonates18Syntheses and Structures of Uranyl Ethylenediphosphonates: From Layers to Elliptical Nanochannels33Crystal structure of [M(H2O)6][UO2(CH3COO)3]2 (M=Mg2+, Co2+ and Zn2+)17Molecular and Polymeric Uranyl and Thorium Complexes with Sulfonate‐Containing Ligands33Syntheses, crystal structures, surface photovoltage, luminescence and molecular recognition properties of zinc(ii) and iron(ii) carboxyphosphonates with 2D and 3D supramolecular structures14The exploration of supramolecular interactions stemming from the [UO 2 (NCS) 4 (H 2 O)] 2− tecton and substituted pyridinium cations37Ionothermal and Hydrothermal Flux Syntheses of Five New Uranyl Phosphonates43Structural Variation within Heterometallic Uranyl Hybrids Based on Flexible Alkyldiphosphonate Ligands40Postsynthetic Rearrangement/Metalation as a Route to Bimetallic Uranyl Coordination Polymers: Syntheses, Structures, and Luminescence70Incorporation of Cu2+ Ions into Nanotubular Uranyl Diphosphonates28A new organically templated open-framework uranyl ethylenediphosphonate6CuPYDC Metalloligands and Postsynthetic Rearrangement/Metalation as Routes to Bimetallic Uranyl Containing Hybrid Materials: Syntheses, Structures, and Fluorescence37[(C 2 H 5 ) 4 N][U 2 O 4 (HCOO) 5 ], an Ammonium Uranyl Formate Framework Showing Para- to Ferro-Electric Transition: Synthesis, Structures, and Properties17The First Family of Actinide Carboxyphosphinates: Two‐ and Three‐Dimensional Uranyl Coordination Polymers27Use of 2,2-Bipyrimidine for the Preparation of UO22+-3d Diphosphonates18Synthesis, structural characterization and computational studies of layered metal phosphonates: [M(HO 3 P–C 5 H 4 N–PO 3 H) 2 (H 2 O) 2 ] n [M II = Co, Zn, Cd]8Uranyl–Organic Hybrids Designed from Hydroxyphosphonate14A new chiral uranyl phosphonate framework consisting of achiral building units generated from ionothermal reaction: structure and spectroscopy characterizations33Hybrid Materials of the f-Elements Part I5Hybrid Materials of the f-Elements Part II5Synthesis, structures, luminescent and molecular recognition properties of three new alkaline earth metal carboxyphosphonates with a 3D supramolecular structure5Two novel cadmium( ii ) carboxyphosphonates with 3D framework structure: synthesis, crystal structures, luminescence and molecular recognition properties15Rigid Phosphonic Acids as Building Blocks for Crystalline Hybrid Materials10Probing the Influence of Phosphonate Bonding Modes to Uranium(VI) on Structural Topology and Stability: A Complementary Experimental and Computational Investigation51Structural chemistry of uranium phosphonates143Structural and spectroscopic characterization of two new layered uranyl(VI) p-xylenediphosphonate compounds synthesized via ionothermal method13Synthesis, Structure, and Photoluminescence Properties of an Organically‐Templated Uranyl Selenite3Uranyl Carboxyphosphonates Derived from Hydrothermal in Situ Ligand Reaction: Syntheses, Structures, and Computational Investigations25Structural Variations of the First Family of Heterometallic Uranyl Carboxyphosphinate Assemblies by Synergy between Carboxyphosphinate and Imidazole Ligands21Two actinide-organic frameworks constructed by a tripodal flexible ligand: Occurrence of infinite {(UO2)O2(OH)3}4n and hexanuclear {Th6O4(OH)4} motifs14Syntheses, structures, and magnetic properties of cobalt(II) and nickel(II) coordination polymers based on a V-shaped ligand4A new uranyl triphosphonate constructed from semi-rigid triphosphonate ligand: New method for the construction of higher dimensional uranyl phosponates6A first principles study of energetics and electronic structural responses of uranium-based coordination polymers to Np incorporation5Molecular and Crystal Structures of Uranyl Nitrate Coordination Polymers with Double-Headed 2-Pyrrolidone Derivatives19Fabrication of New Uranyl Phosphonates by Varying Quaternary Ammonium Cation: Synthesis, Structure, Luminescent Properties, and Single-Crystal to Single-Crystal Transformation18A supramolecular uranyl phosphonate [BTEA]2[(UO2)2(1,3-pbpH2)2F2]: Synthesis, structure, and spectroscopic characterization8Structural Tuning and Sensitization of Uranyl Phosphonates by Incorporation of Countercations into the Framework16Two uranyl-copper(II) bimetallic coordination polymers containing trans-3,3(pyridyl)acrylic acid: Structural variance through synthetic subtleties9The role of 1-ethyl-3-methylimidazolium diethyl phosphate ionic liquid in uranyl phosphate compounds7A 3D uranyl phosphonate framework: Structure, characterization, and fluorescence performance6Features of Uranium Stereochemistry in Uranyl Oxofluorides6Regulating the Porosity of Uranyl Phosphonate Frameworks with Quaternary Ammonium: Structure, Characterization, and Fluorescent Temperature Sensors11Structural variation in Uranyl-Phosphonate networks utilizing tetrahedral Silicon-Centered phosphonate linkers2Alkali Metal-Directed Assembly and Structural Characterization of Layered Uranyl Tetrakisphosphonates2

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  1. Syntheses of Uranyl Diphosphonate Compounds Using Encapsulated Cations as Structure Directing Agents

    Crystal Growth & Design · 2011-08-05

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  2. Heterobimetallic Copper(II) Uranyl Carboxyphenylphosphonates

    Crystal Growth & Design · 2011-08-30

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  3. Crystal Engineering with the Uranyl Cation III. Mixed Aliphatic Dicarboxylate/Aromatic Dipyridyl Coordination Polymers: Synthesis, Structures, and Speciation

    Crystal Growth & Design · 2011-10-06

    Andrew T. Kerr, Christopher L. Cahill

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  4. Synthesis, Crystal Structures, and Luminescence and Magnetic Properties of 3D Chiral and Achiral Lanthanide Diphosphonates Containing Left- and Right-Handed Helical Chains

    Crystal Growth & Design · 2011-10-07

    Da‐Peng Dong, Lei Liu, Zhen‐Gang Sun, Cheng‐Qi Jiao, Zhongmin Liu, Chao Li, Yan‐Yu Zhu, Kai Chen, Chenglin Wang

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  5. Coordination Polymers and Frameworks in Uranyl Ion Complexes with Sulfonates and Cucurbit[6]uril

    Crystal Growth & Design · 2011-10-26

    P. Thuéry

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  6. Metal-Controlled Assembly of Uranyl Diphosphonates toward the Design of Functional Uranyl Nanotubules

    Inorganic Chemistry · 2011-11-03

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  7. In-Situ Raman Spectroscopy Studies of Room-Temperature and Hydrothermal Reactions

    MRS Proceedings · 2012-01-01

    Brendan T. McGrail, Laurent J. Jouffret, Eric M. Villa, Peter Carman Burns

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  8. The structure and properties of a 3D pillared-layered metal organic framework Cu(II)-diphosphonate

    Inorganica Chimica Acta · 2012-03-13

    Xiao-Min Zhao, Kui‐Rong Ma, Yu Zhang, Xiaojing Yang, Ming-Hui Cong

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  9. Barium uranyl diphosphonates

    Journal of Solid State Chemistry · 2012-04-06

    Anna‐Gay D. Nelson, Evgeny V. Alekseev, Rodney Charles Ewing, Thomas E. Albrecht‐Schmitt

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  10. Thorium and uranium diphosphonates: Syntheses, structures, and spectroscopic properties

    Journal of Solid State Chemistry · 2012-05-02

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  11. Syntheses, structures and luminescent properties of two one-dimensional uranium oxyfluorides

    Inorganic Chemistry Communications · 2012-06-12

    Hongyue Wu, Xiuyun Yang, Yunhui Li, Weiting Yang

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  12. Tailor-Made Zinc Uranyl Diphosphonates from Layered to Framework Structures

    Crystal Growth & Design · 2012-08-02

    Hongyue Wu, Weiting Yang, Zhong‐Ming Sun

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  13. Ionothermal synthesis of uranyl compounds that incorporate imidazole derivatives

    Journal of Solid State Chemistry · 2012-08-28

    Ernest M. Wylie, Megan K. Dustin, Jeremy S. Smith, Peter Carman Burns

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  14. One-Dimensional Uranyl-2,2′-bipyridine Coordination Polymer with Cation–Cation Interactions: (UO2)2(2,2′-bpy)(CH3CO2)(O)(OH)

    Inorganic Chemistry · 2012-09-24

    Pius O. Adelani, Peter Carman Burns

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  15. The First Uranyl Arsonates Featuring Heterometallic Cation–Cation Interactions with UVI═O–ZnII Bonding

    Inorganic Chemistry · 2012-09-28

    Tao Tian, Weiting Yang, Qing‐Jiang Pan, Zhong‐Ming Sun

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  16. Mixed-solvothermal synthesis, structures, luminescent and surface photovoltage properties of four new transition metal diphosphonates with a 3D supramolecular structure

    New Journal of Chemistry · 2012-10-04

    Hui Tian, Yan‐Yu Zhu, Zhen‐Gang Sun, Fei Tong, Jiang Zhu, Wei Chu, Shou‐Hui Sun, Mingjing Zheng

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  17. Layered Uranyl Coordination Polymers Rigidly Pillared by Diphosphonates

    Crystal Growth & Design · 2012-10-12

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  18. From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange

    Inorganic Chemistry · 2012-10-24

    Weiting Yang, Hongyue Wu, Run-Xue Wang, Qing‐Jiang Pan, Zhong‐Ming Sun, Hongjie Zhang

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  19. Uranium diphosphonates templated by interlayer organic amines

    Journal of Solid State Chemistry · 2012-10-24

    Anna‐Gay D. Nelson, Evgeny V. Alekseev, Thomas E. Albrecht‐Schmitt, Rodney Charles Ewing

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  20. Correlations and Differences between Uranium(VI) Arsonates and Phosphonates

    Inorganic Chemistry · 2012-10-25

    Pius O. Adelani, Laurent J. Jouffret, Jennifer E. S. Szymanowski, Peter Carman Burns

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  21. Structures and Spectroscopy Studies of Two M(II)-Phosphonate Coordination Polymers Based on Alkaline Earth Metals (M = Ba, Mg)

    Journal of Spectroscopy · 2012-11-28

    Kui‐Rong Ma, Chun-Li Wei, Yu Zhang, Yu‐He Kan, Ming-Hui Cong, Xiaojing Yang

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  22. Sulfonate Complexes of Actinide Ions: Structural Diversity in Uranyl Complexes with 2-Sulfobenzoate

    Inorganic Chemistry · 2012-12-07

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  23. An exploration of homo- and heterometallic UO 2 2+ hybrid materials containing chelidamic acid: synthesis, structure, and luminescence studies

    CrystEngComm · 2013-01-01

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  24. Employing tripodal carboxylate ligand to construct Co(ii) coordination networks modulated by N-donor ligands: syntheses, structures and magnetic properties

    Dalton Transactions · 2013-01-01

    Xue‐Zhi Song, Shu-Yan Song, Min Zhu, Zhao‐Min Hao, Xing Min Meng, Shu‐Na Zhao, Hongjie Zhang

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  25. One- to three-dimensional uranyl–organic assemblies with 3-sulfophthalic and 5-sulfoisophthalic acids

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  26. Two new uranyl fluoride complexes with UVIO–alkali (Na, Cs) interactions: Experimental and theoretical studies

    CrystEngComm · 2013-01-01

    Fei Chen, Cong‐Zhi Wang, Wei‐Qun Shi, Miao Zhang, Cai‐Ming Liu, Yuliang Zhao, Zhifang Chai

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  27. Syntheses and Structures of a Series of Uranyl Phosphonates and Sulfonates: An Insight into Their Correlations and Discrepancies

    Inorganic Chemistry · 2013-02-21

    Weiting Yang, Tao Tian, Hongyue Wu, Qing‐Jiang Pan, Song Dang, Zhong‐Ming Sun

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  28. Two Systems of [DabcoH2]2+/[PipH2]2+–Uranyl–Oxalate Showing Reversible Crystal-to-Crystal Transformations Controlled by the Diammonium/Uranyl/Oxalate Ratios in Aqueous Solutions ([DabcoH2]2+ = 1,4-Diazabicyclo-[2.2.2]-octaneH2 and [PipH2]2+ = PiperazineH2)

    Crystal Growth & Design · 2013-04-09

    Lühua Wang, Ran Shang, Zhong Zheng, Chunli Liu, Zhe‐Ming Wang

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  29. Syntheses, structures and luminescent properties of two organic templated uranyl phosphonates

    Inorganic Chemistry Communications · 2013-05-10

    Hongyue Wu, Yuqin Ma, Xiuwu Zhang, Hongwei Zhang, Xiuyun Yang, Yunhui Li, Hao Wang, Shuang Yao, Weiting Yang

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  30. Syntheses and Structures of Uranyl Ethylenediphosphonates: From Layers to Elliptical Nanochannels

    Inorganic Chemistry · 2013-05-23

    Tao Tian, Weiting Yang, Hao Wang, Song Dang, Qing‐Jiang Pan, Zhong‐Ming Sun

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  31. Crystal structure of [M(H2O)6][UO2(CH3COO)3]2 (M=Mg2+, Co2+ and Zn2+)

    Polyhedron · 2013-06-02

    Vladislav V. Klepov, Eugenia V. Peresypkina, Л. Б. Сережкина, М. О. Карасев, A.V. Virovets, Victor N. Serezhkin

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  32. Molecular and Polymeric Uranyl and Thorium Complexes with Sulfonate‐Containing Ligands

    European Journal of Inorganic Chemistry · 2013-11-25

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  33. Syntheses, crystal structures, surface photovoltage, luminescence and molecular recognition properties of zinc(ii) and iron(ii) carboxyphosphonates with 2D and 3D supramolecular structures

    CrystEngComm · 2013-11-25

    Wei Zhou, Yan‐Yu Zhu, Cheng‐Qi Jiao, Zhen‐Gang Sun, Shao-Ping Shi, Lu-Lu Dai, Tong Sun, Wenzhu Li, Ming-Xue Ma, Hui Luo

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  34. The exploration of supramolecular interactions stemming from the [UO 2 (NCS) 4 (H 2 O)] 2− tecton and substituted pyridinium cations

    CrystEngComm · 2013-12-06

    Robert G. Surbella, Christopher L. Cahill

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  35. Ionothermal and Hydrothermal Flux Syntheses of Five New Uranyl Phosphonates

    Crystal Growth & Design · 2013-12-11

    T. Gannon Parker, Justin N. Cross, Matthew J. Polinski, Jian Hung Lin, Thomas E. Albrecht‐Schmitt

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  36. Structural Variation within Heterometallic Uranyl Hybrids Based on Flexible Alkyldiphosphonate Ligands

    Crystal Growth & Design · 2014-02-07

    Weiting Yang, Fei‐Yan Yi, Tao Tian, Wan‐Guo Tian, Zhong‐Ming Sun

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  37. Postsynthetic Rearrangement/Metalation as a Route to Bimetallic Uranyl Coordination Polymers: Syntheses, Structures, and Luminescence

    Crystal Growth & Design · 2014-02-19

    Andrew T. Kerr, Christopher L. Cahill

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  38. Incorporation of Cu2+ Ions into Nanotubular Uranyl Diphosphonates

    Inorganic Chemistry · 2014-04-04

    Pius O. Adelani, Nathaniel D. Cook, Jean‐Marie Babo, Peter Carman Burns

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  39. A new organically templated open-framework uranyl ethylenediphosphonate

    Inorganic Chemistry Communications · 2014-05-24

    Wan‐Guo Tian, Xiuyun Yang, Yunhui Li, Xiao-Xiao Liu, Weiting Yang, Tao Tian

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  40. CuPYDC Metalloligands and Postsynthetic Rearrangement/Metalation as Routes to Bimetallic Uranyl Containing Hybrid Materials: Syntheses, Structures, and Fluorescence

    Crystal Growth & Design · 2014-06-30

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  41. [(C 2 H 5 ) 4 N][U 2 O 4 (HCOO) 5 ], an Ammonium Uranyl Formate Framework Showing Para- to Ferro-Electric Transition: Synthesis, Structures, and Properties

    Inorganic Chemistry · 2014-07-29

    Qianqian Zhu, Ran Shang, Sa Chen, Chunli Liu, Zhe‐Ming Wang, Song Wei Gao

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  42. The First Family of Actinide Carboxyphosphinates: Two‐ and Three‐Dimensional Uranyl Coordination Polymers

    European Journal of Inorganic Chemistry · 2014-09-22

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  43. Use of 2,2-Bipyrimidine for the Preparation of UO22+-3d Diphosphonates

    Crystal Growth & Design · 2014-10-12

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  44. Synthesis, structural characterization and computational studies of layered metal phosphonates: [M(HO 3 P–C 5 H 4 N–PO 3 H) 2 (H 2 O) 2 ] n [M II = Co, Zn, Cd]

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  45. Uranyl–Organic Hybrids Designed from Hydroxyphosphonate

    European Journal of Inorganic Chemistry · 2014-12-09

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  46. A new chiral uranyl phosphonate framework consisting of achiral building units generated from ionothermal reaction: structure and spectroscopy characterizations

    Dalton Transactions · 2015-01-01

    Tao Zheng, Yang Gao, Lanhua Chen, Zhiyong Liu, Juan Diwu, Zhifang Chai, Thomas E. Albrecht‐Schmitt, Shuao Wang

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  47. Hybrid Materials of the f-Elements Part I

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  48. Hybrid Materials of the f-Elements Part II

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  49. Synthesis, structures, luminescent and molecular recognition properties of three new alkaline earth metal carboxyphosphonates with a 3D supramolecular structure

    New Journal of Chemistry · 2015-01-01

    Hui Luo, Chao Ma, Cheng‐Qi Jiao, Zhen‐Gang Sun, Tong Sun, Ming-Xue Ma, Yan‐Yu Zhu, Wenzhu Li, Meiling Wang, Xiaowen Zhang

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  50. Two novel cadmium( ii ) carboxyphosphonates with 3D framework structure: synthesis, crystal structures, luminescence and molecular recognition properties

    RSC Advances · 2015-01-01

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