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RESEARCH PAPER · Inorganic Chemistry · 2001

Building Unit and Topological Evolution in the Hydrothermal DABCO−U−F System

Christopher L. Cahill, Peter Carman Burns

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Building Unit and Topological Evolution in the Hydrothermal DABCO−U−F SystemOriginalDirect Investigation of the Immobilization of Radionuclides in the Alteration Phases of Spent Nuclear Fuel1Direct Investigations of the Immobilization of Radionuclides in the Alteration Phases of Spent Nuclear Fuel0ChemInform Abstract: Building Unit and Topological Evolution in the Hydrothermal DABCO—U—F System.0Synthesis, Structural Characterization, and Topological Rearrangement of a Novel Open Framework U−O Material: (NH4)3(H2O)2{[(UO2)10O10(OH)][(UO4)(H2O)2]}68Syntheses and Crystal Structures of Two Topologically Related Modifications of Cs2[(UO2)2(MoO4)3]9422 New compounds and structures in the solid state2The Crystal Structure of Triuranyl Diphosphate Tetrahydrate89Hydrothermal Synthesis and Structure of a New One-Dimensional, Mixed-Metal U(VI) Iodate, Cs2[(UO2)(CrO4)(IO3)2]53Crystal Structures of Three Framework Alkali Metal Uranyl Phosphate Hydrates65Organically templated uranium(vi) sulfates: understanding phase stability using composition space83Synthesis of Cyclical Diamine Templated Uranium Sulfates103The Actinides34A Novel Open Framework Uranyl Molybdate: Synthesis and Structure of (NH4)4[(UO2)5(MoO4)7](H2O)567Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies17Direct Investigations of the Immobilization of Radionuclides in the Alteration Phases of Spent Nuclear Fuel4The effects of linear diamine chain length in uranium sulfates482D Chiral Uranyl( VI ) Coordination Polymers with Second‐Harmonic Generation Response and Ferroelectric Properties78Topological Evolution in Uranyl Dicarboxylates: Synthesis and Structures of One-Dimensional UO2(C6H8O4)(H2O)2 and Three-Dimensional UO2(C6H8O4)130Direct Investigations Of The Immobilization Of Radionuclides In The Alteration Phases Of Spent Nuclear Fuel0[N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride50Syntheses, Structures, Magnetic Properties, and X-ray Absorption Spectra of Carnotite-type Uranyl Chromium(V) Oxides: A[(UO2)2Cr2O8](H2O)n (A = K2, Rb2, Cs2, Mg; n = 0, 4)21Structures and syntheses of layered and framework amine-bearing uranyl phosphate and uranyl arsenates40[N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure32Direct Investigations of the Immobilization of Radionuclides in the Alteration Products of Spent Nuclear Fuel2Self‐Assembly of Protonated 1,12‐Dodecanediamine Molecules and Strongly Undulated Uranyl Selenate Sheets in the Structure of Amine‐Templated Uranyl Selenate: (H3O)2[C12H30N2]3[(UO2)4(SeO4)8](H2O)543Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure51K(UO)Si2O6: A Pentavalent−Uranium Silicate90[N(CH3)4][(UO2)2F5]: A new organically templated open-framework uranium oxide fluoride (MUF-2)38Synthesis, structure and fluorescent studies of novel uranium coordination polymers in the pyridinedicarboxylic acid system172UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure16Crystalline oxyfluorinated open-framework compounds: Silicates, metal phosphates, metal fluorides and metal-organic frameworks (MOF)81Product evolution in the Np(IV) fluorophosphate system15Anhydrous Photochemical Uranyl(VI) Reduction: Unprecedented Retention of Equatorial Coordination Accompanying Reversible Axial Oxo/Alkoxide Exchange45Hydrothermal synthesis, crystal structure, and characterization of a new pseudo-two-dimensional uranyl oxyfluoride, [N(C2H5)4]2[(UO2)4(OH2)3F10]17Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates23Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)6U(VI)-containing metal-organic frameworks and coordination polymers14Uranyl Coordination in Ionic Liquids: The Competition between Ionic Liquid Anions, Uranyl Counterions, and Cl- Anions Investigated by Extended X-ray Absorption Fine Structure and UV−Visible Spectroscopies and Molecular Dynamics Simulations87Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites31Novel two-dimensional uranyl–organic assemblages in the citrate and d (–)-citramalate families46The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies26Synthesis, crystal structures and properties of three new lanthanide 2,6-pyridinedicarboxylate complexes with zero-dimensional structure49Two novel uranyl–organic frameworks with cyclohexane-1,3-dicarboxylate ligands40Oxo ligand functionalization in the uranyl ion (UO22+)335Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization18Combination of covalent and hydrogen bonding in the formation of 3D uranyl-carboxylate networks28Synthesis, Structure, and Solid-State Transformation Studies of Phosphonoacetate Based Hybrid Compounds of Uranium and Thorium48Uranyl Bearing Hybrid Materials: Synthesis, Speciation, and Solid-State Structures418Hydrothermal synthesis and structural characterisation of [H 2 DABCO] 3 [Cu 16 Cl 22 ]: a new copper( i ) chloride framework15Bisactinyl halogenated complexes: relativistic density functional theory calculation and experimental synthesis9Crystal structures of tetravalent uranium fluorides obtained in the presence of hydrazine from uranyl source7Mild Hydrothermal Crystal Growth, Structure, and Magnetic Properties of Ternary U(IV) Containing Fluorides: LiUF5, KU2F9, K7U6F31, RbUF5, RbU2F9, and RbU3F1341Structural complexity in indium selenides prepared using bicyclic amines as structure-directing agents10Trivalent Cation-Controlled Phase Space of New U(IV) Fluorides, Na3MU6F30 (M = Al3+, Ga3+, Ti3+, V3+, Cr3+, Fe3+): Mild Hydrothermal Synthesis Including an in Situ Reduction Step, Structures, Optical, and Magnetic Properties28Hydrothermal syntheses and characterization of uranyl tungstates with electro-neutral structural units0Insight into the Uranyl Oxyfluoride Topologies through the Synthesis, Crystal Structure, and Evidence of a New Oxyfluoride Layer in [(UO2)4F13][Sr3(H2O)8](NO3)·H2O6[Co(H2O)6]3[U2O4F7]2: A Model System for Understanding the Formation of Dimensionally Reduced Materials11Solubilité et fluoration d’oxydes d’uranium en milieu liquide ionique0Two-Electron Oxidative Atom Transfer at a Homoleptic, Tetravalent Uranium Complex39Cyclic Aliphatic Hydrocarbons as Linkers in Metal‐Organic Frameworks: New Frontiers for Ligand Design32Controlling the Reduction of Chelated Uranyl to Stable Tetravalent Uranium Coordination Complexes in Aqueous Solution15Features of Uranium Stereochemistry in Uranyl Oxofluorides6Structural chemistry of fluoride complexes of uranyl8Evidence of a Uranium‐Paddlewheel Node in a Catecholate‐Based Metal–Organic Framework0Evidence of a Uranium‐Paddlewheel Node in a Catecholate‐Based Metal–Organic Framework6Structural, Spectroscopic, and Computational Analysis of Halogen- and Hydrogen-Bonding Effects within a Series of Uranyl Fluorides with 4-Halopyridinium3

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  1. Direct Investigation of the Immobilization of Radionuclides in the Alteration Phases of Spent Nuclear Fuel

    Unknown journal · 1999-06-01

    Peter Carman Burns, USDOE Office of Environmental Management (EM) (US), Robert J. Finch, David J. Wronkiewicz

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  2. Direct Investigations of the Immobilization of Radionuclides in the Alteration Phases of Spent Nuclear Fuel

    Unknown journal · 2001-06-01

    Peter Carman Burns, USDOE Office of Environmental Management (EM) (US), Robert J. Finch, David J. Wronkiewicz

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  3. ChemInform Abstract: Building Unit and Topological Evolution in the Hydrothermal DABCO—U—F System.

    ChemInform · 2001-06-19

    Christopher L. Cahill, Peter Carman Burns

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  4. Synthesis, Structural Characterization, and Topological Rearrangement of a Novel Open Framework U−O Material: (NH4)3(H2O)2{[(UO2)10O10(OH)][(UO4)(H2O)2]}

    Chemistry of Materials · 2001-09-28

    Yaping Li, Christopher L. Cahill, Peter Carman Burns

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  5. Syntheses and Crystal Structures of Two Topologically Related Modifications of Cs2[(UO2)2(MoO4)3]

    Inorganic Chemistry · 2001-12-06

    Sergey V. Krivovichev, Christopher L. Cahill, Peter Carman Burns

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  6. 22 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2002-01-01

    Martin P. Attfield

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  7. The Crystal Structure of Triuranyl Diphosphate Tetrahydrate

    Journal of Solid State Chemistry · 2002-01-01

    Andrew J. Locock, Peter Carman Burns

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  8. Hydrothermal Synthesis and Structure of a New One-Dimensional, Mixed-Metal U(VI) Iodate, Cs2[(UO2)(CrO4)(IO3)2]

    Inorganic Chemistry · 2002-04-02

    Richard E. Sykora, Daniel M. Wells, Thomas E. Albrecht‐Schmitt

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  9. Crystal Structures of Three Framework Alkali Metal Uranyl Phosphate Hydrates

    Journal of Solid State Chemistry · 2002-08-01

    Andrew J. Locock, Peter Carman Burns

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  10. Organically templated uranium(vi) sulfates: understanding phase stability using composition space

    Journal of Materials Chemistry · 2002-11-12

    Paul M. Thomas, Alexander J. Norquist, M.B. Doran, Dermot M. O'Hare

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  11. Synthesis of Cyclical Diamine Templated Uranium Sulfates

    Chemistry of Materials · 2002-11-12

    Alexander J. Norquist, Paul M. Thomas, M.B. Doran, Dermot M. O'Hare

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  12. The Actinides

    Elsevier eBooks · 2003-01-01

    Carol J. Burns, Mary P. Neu, Hakim Boukhalfa, Keith E. Gutowski, Nicholas J. Bridges, Robin Don Rogers

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  13. A Novel Open Framework Uranyl Molybdate: Synthesis and Structure of (NH4)4[(UO2)5(MoO4)7](H2O)5

    Inorganic Chemistry · 2003-03-14

    Sergey V. Krivovichev, Christopher L. Cahill, Peter Carman Burns

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  14. Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies

    Inorganic Chemistry · 2003-03-25

    Amanda C. Bean, Tyler A. Sullens, Wolfgang Runde, Thomas E. Albrecht‐Schmitt

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  15. Direct Investigations of the Immobilization of Radionuclides in the Alteration Phases of Spent Nuclear Fuel

    Unknown journal · 2003-06-01

    Peter Carman Burns, USDOE Office of Science (SC) (US), Argonne National Chemical Technology Division, Robert J. Finch, David J. Wronkiewicz

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  16. The effects of linear diamine chain length in uranium sulfates

    Solid State Sciences · 2003-06-30

    Alexander J. Norquist, M.B. Doran, Dermot M. O'Hare

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  17. 2D Chiral Uranyl( VI ) Coordination Polymers with Second‐Harmonic Generation Response and Ferroelectric Properties

    European Journal of Inorganic Chemistry · 2003-10-01

    Yong‐Rong Xie, Hong Lin Zhao, Xisen Wang, Zhi‐Rong Qu, Ren‐Gen Xiong, Xiang Xue, Zi‐Ling Xue, Xiao‐Zeng You

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  18. Topological Evolution in Uranyl Dicarboxylates: Synthesis and Structures of One-Dimensional UO2(C6H8O4)(H2O)2 and Three-Dimensional UO2(C6H8O4)

    Inorganic Chemistry · 2003-10-04

    Lauren A. Borkowski, Christopher L. Cahill

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  19. Direct Investigations Of The Immobilization Of Radionuclides In The Alteration Phases Of Spent Nuclear Fuel

    Unknown journal · 2003-12-31

    Peter Carman Burns, Robert J. Finch, David J. Wronkiewicz

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  20. [N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride

    Chemistry of Materials · 2004-01-30

    M.B. Doran, Clair L. Stuart, Alexander J. Norquist, Dermot M. O'Hare

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  21. Syntheses, Structures, Magnetic Properties, and X-ray Absorption Spectra of Carnotite-type Uranyl Chromium(V) Oxides: A[(UO2)2Cr2O8](H2O)n (A = K2, Rb2, Cs2, Mg; n = 0, 4)

    Chemistry of Materials · 2004-03-09

    Andrew J. Locock, S. Skanthakumar, Peter Carman Burns, L. Soderholm

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  22. Structures and syntheses of layered and framework amine-bearing uranyl phosphate and uranyl arsenates

    Journal of Solid State Chemistry · 2004-06-21

    Andrew J. Locock, Peter Carman Burns

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  23. [N(CH2CH2NH3)3][U3O2F13]·2H2O: A Novel Organically Templated Mixed-Valent Uranium Oxyfluoride with a Hybrid Network Structure

    Inorganic Chemistry · 2004-11-23

    Chih-Min Wang, Chia-Hsien Liao, Hsiu‐Mei Lin, Kwang‐Hwa Lii

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  24. Direct Investigations of the Immobilization of Radionuclides in the Alteration Products of Spent Nuclear Fuel

    Unknown journal · 2004-12-27

    Peter Carman Burns, Robert J. Finch, David J. Wronkiewicz

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  25. Self‐Assembly of Protonated 1,12‐Dodecanediamine Molecules and Strongly Undulated Uranyl Selenate Sheets in the Structure of Amine‐Templated Uranyl Selenate: (H3O)2[C12H30N2]3[(UO2)4(SeO4)8](H2O)5

    European Journal of Inorganic Chemistry · 2005-04-28

    Sergey V. Krivovichev, Volker Kahlenberg, Evgeniya Y. Avdontseva, Edgar Mersdorf, Reinhard Kaindl

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  26. Hydrothermal Synthesis and Characterization of [(UO2)2F8(H2O)2Zn2(4,4‘-bpy)2]·(4,4‘-bpy), a Mixed-Metal Uranyl Aquofluoride with a Pillared Layer Structure

    Inorganic Chemistry · 2005-07-29

    Chih-Min Wang, Chia-Hsien Liao, Hsien‐Ming Kao, Kwang‐Hwa Lii

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  27. K(UO)Si2O6: A Pentavalent−Uranium Silicate

    Journal of the American Chemical Society · 2005-08-10

    Chih-Shan Chen, Shang‐Fan Lee, Kwang‐Hwa Lii

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  28. [N(CH3)4][(UO2)2F5]: A new organically templated open-framework uranium oxide fluoride (MUF-2)

    Journal of Materials Chemistry · 2006-01-01

    Kang Min Ok, M.B. Doran, Dermot M. O'Hare

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  29. Synthesis, structure and fluorescent studies of novel uranium coordination polymers in the pyridinedicarboxylic acid system

    Dalton Transactions · 2006-01-01

    M. Frisch, Christopher L. Cahill

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  30. UF3(H2O)(C2O4)0.5: A Fluorooxalate of Tetravalent Uranium with a Three-Dimensional Framework Structure

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    Chih-Min Wang, Chia-Hsien Liao, Pei-Lin Chen, Kwang‐Hwa Lii

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  31. Crystalline oxyfluorinated open-framework compounds: Silicates, metal phosphates, metal fluorides and metal-organic frameworks (MOF)

    Journal of Fluorine Chemistry · 2006-09-20

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  32. Product evolution in the Np(IV) fluorophosphate system

    Journal of Solid State Chemistry · 2006-09-30

    Travis H. Bray, Tyler A. Sullens, Tatiana Y. Shvareva, Richard E. Sykora, Richard Geoffrey Haire, Thomas E. Albrecht‐Schmitt

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  33. Anhydrous Photochemical Uranyl(VI) Reduction: Unprecedented Retention of Equatorial Coordination Accompanying Reversible Axial Oxo/Alkoxide Exchange

    Journal of the American Chemical Society · 2006-10-07

    Shanmugaperumal Kannan, Anthony E. Vaughn, Eric M. Weis, Charles Leslie Barnes, Paul B. Duval

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  34. Hydrothermal synthesis, crystal structure, and characterization of a new pseudo-two-dimensional uranyl oxyfluoride, [N(C2H5)4]2[(UO2)4(OH2)3F10]

    Journal of Solid State Chemistry · 2006-11-14

    Kang Min Ok, Dermot M. O'Hare

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  35. Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates

    Journal of Solid State Chemistry · 2006-12-13

    Murielle Rivenet, Nicolas Vigier, Pascal Roussel, F. Abraham

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  36. Organically templated uranium( iv ) fluorooxalates with layer structures: (H 4 TREN)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (TREN = tris(2-aminoethyl)amine) and (H 4 APPIP)[U 2 F 6 (C 2 O 4 ) 3 ]·4H 2 O (APPIP = 1,4-bis(3-amino-propyl)piperazine)

    Dalton Transactions · 2007-01-01

    Chih-Min Wang, Yi‐Ying Wu, Pei-Lin Chen, Kwang‐Hwa Lii

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  37. U(VI)-containing metal-organic frameworks and coordination polymers

    Elsevier eBooks · 2007-01-01

    Christopher L. Cahill, Lauren A. Borkowski

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  38. Uranyl Coordination in Ionic Liquids: The Competition between Ionic Liquid Anions, Uranyl Counterions, and Cl- Anions Investigated by Extended X-ray Absorption Fine Structure and UV−Visible Spectroscopies and Molecular Dynamics Simulations

    Inorganic Chemistry · 2007-05-16

    C. Gaillard, Alain Chaumont, Isabelle Billard, Christoph Hennig, Ali Ouadi, Georges Wipff

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  39. Synthesis, Structure, and Upconversion Studies on Organically Templated Uranium Phosphites

    Inorganic Chemistry · 2007-08-24

    Sukhendu Bikas Mandal, Manabendra Chandra, Srinivasan Natarajan

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  40. Novel two-dimensional uranyl–organic assemblages in the citrate and d (–)-citramalate families

    CrystEngComm · 2007-12-14

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  41. The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies

    Chemistry of Materials · 2008-01-01

    Yu-Lun Lai, Ray‐Kuang Chiang, Kwang‐Hwa Lii, Sue‐Lein Wang

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  42. Synthesis, crystal structures and properties of three new lanthanide 2,6-pyridinedicarboxylate complexes with zero-dimensional structure

    Inorganica Chimica Acta · 2008-03-06

    C. Brouca-Cabarrecq, Jeannette Dexpert‐Ghys, Auguste Fernandes, Joël Jaud, Jean‐Christian Trombe

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  43. Two novel uranyl–organic frameworks with cyclohexane-1,3-dicarboxylate ligands

    CrystEngComm · 2008-11-19

    P. Thuéry

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  44. Oxo ligand functionalization in the uranyl ion (UO22+)

    Coordination Chemistry Reviews · 2009-06-22

    Skye Fortier, Trevor W. Hayton

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  45. Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization

    Inorganic Chemistry · 2010-02-12

    Vandavasi Koteswara Rao, K. Bharathi, Ramanath Prabhu, Manabendra Chandra, Srinivasan Natarajan

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  46. Combination of covalent and hydrogen bonding in the formation of 3D uranyl-carboxylate networks

    Inorganica Chimica Acta · 2010-07-01

    Sudipta Dalai, Madhusudan Bera, Abhinandan Rana, Durga Sankar Chowdhuri, Ennio Zangrando

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  47. Synthesis, Structure, and Solid-State Transformation Studies of Phosphonoacetate Based Hybrid Compounds of Uranium and Thorium

    Inorganic Chemistry · 2010-07-27

    Padmini Ramaswamy, Ramanath Prabhu, Srinivasan Natarajan

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  48. Uranyl Bearing Hybrid Materials: Synthesis, Speciation, and Solid-State Structures

    Chemical Reviews · 2012-08-10

    Michael B. Andrews, Christopher L. Cahill

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  49. Hydrothermal synthesis and structural characterisation of [H 2 DABCO] 3 [Cu 16 Cl 22 ]: a new copper( i ) chloride framework

    CrystEngComm · 2012-10-19

    Edward R. Williams, Mark T. Weller

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  50. Bisactinyl halogenated complexes: relativistic density functional theory calculation and experimental synthesis

    RSC Advances · 2012-11-14

    Qing‐Jiang Pan, Yong-Ming Wang, Run-Xue Wang, Hongyue Wu, Weiting Yang, Zhong‐Ming Sun, Hong‐Xing Zhang

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