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RESEARCH PAPER · Inorganic Chemistry · 2003

Exploration of Composition Space in Templated Uranium Sulfates

M.B. Doran, Alexander J. Norquist, Dermot O’Hare

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Exploration of Composition Space in Templated Uranium SulfatesOriginal18 Scandium, yttrium, the lanthanides and the actinides11The effects of hydrofluoric acid addition on the hydrothermal synthesis of templated uranium sulfates46(C8H26N4)0.5[(UO2)2(SO4)3(H2O)]·2H2O, an organically templated uranyl sulfate with a novel layer type22Solvothermal Synthesis of Paramagnetic Molecular Clusters83Comparative study of the flexibility of structural complexes in uranyl sulfates, chromates, and molybdates28Structural variation in organically templated uranium sulfate fluorides42(C3H12N2)2[UO2(H2O)2(SO4)2]2·2H2O: an organically templated uranium sulfate with a novel dimer type14The Role of Amine Sulfates in Hydrothermal Uranium Chemistry63[H2en]2{La2M(SO4)6(H2O)2} (M=Co, Ni): First organically templated 3d–4f mixed metal sulfates38Actinides: Inorganic & Coordination ChemistryBased in part on the article Actinides: Inorganic & Coordination Chemistry by Grigorii L. Soloveichik which appeared in the Encyclopedia of Inorganic Chemistry, First Edition .1Actinides: Inorganic & Coordination ChemistryBased in part on the article Actinides: Inorganic & Coordination Chemistry by Grigorii L. Soloveichik which appeared in the Encyclopedia of Inorganic Chemistry, First Edition .0Hydrothermal Synthesis of Delafossite-Type Oxides245Organically-templated metal sulfates, selenites and selenates194High-Pressure- and Low-Temperature-Induced Changes in [(CH3)2NH(CH2)2NH3][SbCl5]39Directed Synthesis of Noncentrosymmetric Molybdates Using Composition Space Analysis72Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates23Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)26Composition space analysis of templated molybdates25One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands32Coordination of U(IV) and U(VI) sulfate hydrate in aqueous solution3Synthetic Approaches for Noncentrosymmetric Molybdates59Syntheses, structures, characterizations and charge-density matching of novel amino-templated uranyl selenates45NEPTUNYL COMPOUNDS: POLYHEDRON GEOMETRIES, BOND-VALENCE PARAMETERS, AND STRUCTURAL HIERARCHY77Pyrazolato-bridged 1-D Co(II) coordination polymer and dinuclear Ni(II) and Cu(II) complexes: Syntheses, crystal structures and magnetic properties32A three-dimensional copper(II) coordination polymer featuring the 2,3-dioxyquinoxalinate(-2) ligand: Preparation, structural characterization and magnetic study9Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Amine-templated uranyl selenates with chiral [(UO2)2(SeO4)3(H2O)]2– layers: topology, isomerism, structural relationships31Glycine-Templated Manganese Sulfate with New Topology and Canted Antiferromagnetism35Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?18Uranyl selenates with organic templates: Principles of structure and characteristics of self-organization23Hydrothermal Synthesis and Crystal Structures of Actinide Compounds2Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization18A Slow Leak Synthetic Route to Organically Templated Gallium Sulfates8Synthesis, spectroscopic and structural properties of uranyl complexes based on bipyridine N-oxide ligands20Synthesis, characterization and magnetic properties of four new organically templated metal sulfates [C5H14N2][MII(H2O)6](SO4)2, (MII = Mn, Fe, Co, Ni)35Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates38Understanding an Order–Disorder Phase Transition in Ionothermally Synthesized Gallium Phosphates9Beyond Charge Density Matching: The Role of C–H···O Interactions in the Formation of Templated Vanadium Tellurites16N,N-Dimethylethane-1,2-diaminium bis(3-hydroxybenzoate)0A series of new rare earth sulfates based on lanthanide contraction and dual organic-amine templating effects12Isopropylammonium Layered Uranyl Chromates: Syntheses and Crystal Structures of [(CH3)2CHNH3]3[(UO2)3(CrO4)2O(OH)3] and[(CH3)2CHNH3]2[(UO2)2(CrO4)3(H2O)]30Uranyl Bearing Hybrid Materials: Synthesis, Speciation, and Solid-State Structures418Amine templating effect absent in uranyl sulfates synthesized with 1,4-n-butyldiamine14Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks26Crystal Chemistry of Uranium Oxides and Minerals27Cr(VI) Trioxide as a Starting Material for the Synthesis of Novel Zero-, One-, and Two-Dimensional Uranyl Dichromates and Chromate-Dichromates28The structural transformation of monoclinic [(R)-C5H14N2][Cu(SO4)2(H2O)4]·2H2O into orthorhombic [(R)-C5H14N2]2[Cu(H2O)6](SO4)3: crystal structures and thermal behavior3Crystal structures and characterization of two divalent metal selenates templated by dabco, (C6H14N2)[MII(H2O)6](SeO4)2 (MII: NiII, ZnII)11K2Na8(UO2)8Mo4O24[(S,Mo)O4], the first uranium molybdosulfate: synthesis, crystal structure, and comparison to related compounds5Triazolyl–Based Copper–Molybdate Hybrids: From Composition Space Diagram to Magnetism and Catalytic Performance41Hydro(solvo)thermal synthetic strategy towards azido/formato-mediated molecular magnetic materials90Topologically and geometrically flexible structural units in seven new organically templated uranyl selenates and selenite–selenates22Coherent Fusion of Water Array and Protonated Amine in a Metal–Sulfate-Based Coordination Polymer for Proton Conduction18Phase Transition Originating from Disorder–Order Transformation Coupled with Reorientation in the Organic–Inorganic Hybrid Compound (C4H14N2)[Cd2(H2O)6(SO4)3]7Inorganic Synthesis of Actinides3Formation of co-racemic uranyl chromate constructed from chiral layers of different topology10Polyamine functionalised ion exchange resins: Synthesis, characterisation and uranyl uptake101Structural unit charge density and molecular cation templating effects on orientational geometric isomerism and interlayer spacing in 2-D uranyl sulfates11Synthesis, characterization and temperature-triggered phase transition of organic-inorganic hybrid compound: (C6H18N2)(HSO4)211Synthesis and Crystal Structures of New Layered Uranyl Compounds Containing Dimers [(UO2)2O8] of Edge-Linked Pentagonal Bipyramids7Probing the existence of uranyl trisulfate structures in the AMEX solvent extraction process27Effect of solution acidity on the structure of amino acid-bearing uranyl compounds7Ligand Mediated Morphology of the Two‐Dimensional Uranyl Aqua Sulfates [UO2(X)(SO4)(H2O)] [X = Cl– or (CH3)3NCH2COO]6Templated vanadium tellurites: Identifying the effects of low density attractions on inorganic layer topology4Chemically induced symmetry breaking in the crystal structure of guanidinium uranyl sulfate10Topological analysis of the layered uranyl compounds bearing slabs with UO2:TO4ratio of 2:35Dimensional evolution in hydrated K + -bearing uranyl sulfates: from 2D-sheets to 3D-frameworks12Organically Templated Layered Uranyl Molybdate [C3H9NH+]4[(UO2)3(MoO4)5] Structurally Based on Mineral-Related Modular Units6Insights from quantum chemical calculations into inner and outer-sphere complexation of plutonium( iv ) by monoamide and carbamide extractants3Effect of Ionothermal Conditions on the Crystallization of Organically Templated Uranyl Sulfate Compounds6Effect of solution acidity on the crystallization of polychromates in uranyl-bearing systems: synthesis and crystal structures of Rb2[(UO2)(Cr2O7)(NO3)2] and two new polymorphs of Rb2Cr3O105Molecular modeling of organic phases after plutonium extraction0Homopiperazine (Hexahydro-1,4-diazepine)5Nitrogen-Containing Molecules: Natural and Synthetic Products Including Coordination Compounds1Secondary Role of Aliphatic and Heterocyclic Amines in the Formation of Low-Temperature Amine-Bearing U, Np, and Pu(VI) Chromates2Hydrogen bond network and bond valence analysis on uranyl sulfate compounds with organic-based interstitial cations5Exploring the Role of Organic Functional Groups in the Ionothermal Synthesis of Uranyl Phosphate Materials3Mixed-Valence NpV/AnVI Molybdate Complexes with Single-Charge Outer-Sphere Cations2Organically Templated Uranyl Sulfates and Selenates: Structural Complexity and Crystal Chemical Restrictions for Isotypic Compounds Formation7Results of 25-Year Studies of Uranium Compounds at the Department of Crystallography of St. Petersburg State University3

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  1. 18 Scandium, yttrium, the lanthanides and the actinides

    Annual Reports Section A (Inorganic Chemistry) · 2004-01-01

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  2. The effects of hydrofluoric acid addition on the hydrothermal synthesis of templated uranium sulfates

    Dalton Transactions · 2004-01-01

    M.B. Doran, Ben E. Cockbain, Alexander J. Norquist, Dermot O’Hare

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  3. (C8H26N4)0.5[(UO2)2(SO4)3(H2O)]·2H2O, an organically templated uranyl sulfate with a novel layer type

    Acta Crystallographica Section E Structure Reports Online · 2004-06-26

    M.B. Doran, Alexander J. Norquist, Clair L. Stuart, Dermot O’Hare

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  4. Solvothermal Synthesis of Paramagnetic Molecular Clusters

    European Journal of Inorganic Chemistry · 2004-07-01

    R.H. Laye, Eric J. L. McInnes

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  5. Comparative study of the flexibility of structural complexes in uranyl sulfates, chromates, and molybdates

    Radiochemistry · 2004-09-01

    Sergey V. Krivovichev

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  6. Structural variation in organically templated uranium sulfate fluorides

    Dalton Transactions · 2005-01-01

    M.B. Doran, Ben E. Cockbain, Dermot O’Hare

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  7. (C3H12N2)2[UO2(H2O)2(SO4)2]2·2H2O: an organically templated uranium sulfate with a novel dimer type

    Acta Crystallographica Section E Structure Reports Online · 2005-04-16

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  8. The Role of Amine Sulfates in Hydrothermal Uranium Chemistry

    Inorganic Chemistry · 2005-05-01

    Alexander J. Norquist, M.B. Doran, Dermot O’Hare

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  9. [H2en]2{La2M(SO4)6(H2O)2} (M=Co, Ni): First organically templated 3d–4f mixed metal sulfates

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  10. Actinides: Inorganic & Coordination ChemistryBased in part on the article Actinides: Inorganic & Coordination Chemistry by Grigorii L. Soloveichik which appeared in the Encyclopedia of Inorganic Chemistry, First Edition .

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  11. Actinides: Inorganic & Coordination ChemistryBased in part on the article Actinides: Inorganic & Coordination Chemistry by Grigorii L. Soloveichik which appeared in the Encyclopedia of Inorganic Chemistry, First Edition .

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  12. Hydrothermal Synthesis of Delafossite-Type Oxides

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    William C. Sheets, Emmanuelle Mugnier, Antoine Barnabé, Tobin Jay Marks, Kenneth Reinhard Poeppelmeier

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  13. Organically-templated metal sulfates, selenites and selenates

    Chemical Society Reviews · 2006-01-01

    C. N. R. Rao, J. N. Behera, Meenakshi Dan-Hardi

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  14. High-Pressure- and Low-Temperature-Induced Changes in [(CH3)2NH(CH2)2NH3][SbCl5]

    The Journal of Physical Chemistry B · 2006-05-12

    M. Bujak, Ross John Angel

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  15. Directed Synthesis of Noncentrosymmetric Molybdates Using Composition Space Analysis

    Inorganic Chemistry · 2006-06-10

    Thomas R. Veltman, Adam K. Stover, Amy Narducci Sarjeant, Kang Min Ok, P. Shiv Halasyamani, Alexander J. Norquist

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  16. Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates

    Journal of Solid State Chemistry · 2006-12-13

    Murielle Rivenet, Nicolas Vigier, Pascal Roussel, F. Abraham

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  17. Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)

    Elsevier eBooks · 2007-01-01

    Sergey V. Krivovichev, Peter Carman Burns

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  18. Composition space analysis of templated molybdates

    Solid State Sciences · 2007-04-11

    J.H. Nelson, Alexander R. Johnston, Amy Narducci Sarjeant, Alexander J. Norquist

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  19. One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands

    Inorganic Chemistry · 2007-11-01

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  20. Coordination of U(IV) and U(VI) sulfate hydrate in aqueous solution

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    Christoph Hennig, Satoru Tsushima, Vinzenz Brendler, Atsushi Ikeda‐Ohno, Andreas C. Scheinost, Gert Bernhard

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  21. Synthetic Approaches for Noncentrosymmetric Molybdates

    Inorganic Chemistry · 2008-09-29

    Desmond J. Hubbard, Alexander R. Johnston, Hernan Sanchez Casalongue, Amy Narducci Sarjeant, Alexander J. Norquist

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  22. Syntheses, structures, characterizations and charge-density matching of novel amino-templated uranyl selenates

    Journal of Solid State Chemistry · 2008-11-21

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  23. NEPTUNYL COMPOUNDS: POLYHEDRON GEOMETRIES, BOND-VALENCE PARAMETERS, AND STRUCTURAL HIERARCHY

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  24. Pyrazolato-bridged 1-D Co(II) coordination polymer and dinuclear Ni(II) and Cu(II) complexes: Syntheses, crystal structures and magnetic properties

    Inorganica Chimica Acta · 2008-12-03

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  25. A three-dimensional copper(II) coordination polymer featuring the 2,3-dioxyquinoxalinate(-2) ligand: Preparation, structural characterization and magnetic study

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  26. Alternative approaches to structure description

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  27. Anion-topology approach

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  28. Basic concepts

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  29. Copyright Page

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  30. Dedication

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  31. Dimensional reduction in inorganic oxysalts

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  32. Graph theory applied to low-dimensional structural units in inorganic oxysalts

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  33. Preface

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  34. Structural Crystallography of Inorganic Oxysalts

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  35. Topology of framework structures in inorganic oxysalts

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  36. Amine-templated uranyl selenates with chiral [(UO2)2(SeO4)3(H2O)]2– layers: topology, isomerism, structural relationships

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  37. Glycine-Templated Manganese Sulfate with New Topology and Canted Antiferromagnetism

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  38. Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?

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  39. Uranyl selenates with organic templates: Principles of structure and characteristics of self-organization

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  40. Hydrothermal Synthesis and Crystal Structures of Actinide Compounds

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  41. Two- and Three-Dimensional Open-Framework Uranium Arsenates: Synthesis, Structure, and Characterization

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  42. A Slow Leak Synthetic Route to Organically Templated Gallium Sulfates

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  43. Synthesis, spectroscopic and structural properties of uranyl complexes based on bipyridine N-oxide ligands

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  44. Synthesis, characterization and magnetic properties of four new organically templated metal sulfates [C5H14N2][MII(H2O)6](SO4)2, (MII = Mn, Fe, Co, Ni)

    Dalton Transactions · 2011-01-01

    Fadhel Hajlaoui, Houcine Naı̈li, S. Yahyaoui, Mark M. Turnbull, Tahar Mhiri, Thierry Bataille

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  45. Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates

    Crystal Growth & Design · 2011-04-18

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  46. Understanding an Order–Disorder Phase Transition in Ionothermally Synthesized Gallium Phosphates

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  47. Beyond Charge Density Matching: The Role of C–H···O Interactions in the Formation of Templated Vanadium Tellurites

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  48. N,N-Dimethylethane-1,2-diaminium bis(3-hydroxybenzoate)

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  49. A series of new rare earth sulfates based on lanthanide contraction and dual organic-amine templating effects

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  50. Isopropylammonium Layered Uranyl Chromates: Syntheses and Crystal Structures of [(CH3)2CHNH3]3[(UO2)3(CrO4)2O(OH)3] and[(CH3)2CHNH3]2[(UO2)2(CrO4)3(H2O)]

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