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RESEARCH PAPER · Angewandte Chemie International Edition · 2007

A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds

Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

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A Crown Ether as Template for Microporous and Nanostructured Uranium CompoundsOriginalChemInform Abstract: A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds.0Preparation, Structures, and Photocatalytic Properties of Three New Uranyl−Organic Assembly Compounds218An Open-Framework Thorium Sulfate Hydrate with 11.5 Å Voids42Two novel uranyl–organic frameworks with cyclohexane-1,3-dicarboxylate ligands40Novel layered uranyl arsenates, Ag6[(UO2)2(As2O7)(As4O13)] and AI6[(UO2)2(AsO4)2(As2O7)] (AI–Ag and Na): first observation of a linear As4O136− anion and structure type evolution25Protonated 3-amino-1,2,4-triazole templated luminescent lanthanide isophthalates with a rare (3,6)-connected topology31Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Amine-templated uranyl selenates with chiral [(UO2)2(SeO4)3(H2O)]2– layers: topology, isomerism, structural relationships31Crystal chemistry of anhydrous Li uranyl phosphates and arsenates. II. Tubular fragments and cation–cation interactions in the 3D framework structures of Li6[(UO2)12(PO4)8(P4O13)], Li5[(UO2)13(AsO4)9(As2O7)], Li[(UO2)4(AsO4)3] and Li3[(UO2)7(AsO4)5O)]38Crystal structures of crown and aza-crown ether complexes with zirconium, hafnium, niobium, and tantalum fluorometallates7NDTB‐1: A Supertetrahedral Cationic Framework That Removes TcO4− from Solution270NDTB‐1: A Supertetrahedral Cationic Framework That Removes TcO4− from Solution37Amine templated two- and three-dimensional uranyl sulfates24Cubic and rhombohedral heterobimetallic networks constructed from uranium, transition metals, and phosphonoacetate: new methods for constructing porous materials113Partially ordered organic-inorganic nanocomposites in the system UO2SeO4-H2O-NH3(CH2)9NH36Actinyl Compounds with Hexavalent Elements (S, Cr, Se, Mo) – Structural Diversity, Nanoscale Chemistry, and Cellular Automata Modeling69Crystal Chemistry of the Potassium and Rubidium Uranyl Borate Families Derived from Boric Acid Fluxes49Technetium‐99 MAS NMR Spectroscopy of a Cationic Framework Material that Traps TcO4− Ions57Technetium‐99 MAS NMR Spectroscopy of a Cationic Framework Material that Traps TcO4− Ions11Crystal and molecular structure of a crystal solvate of cesium tris(pivaloyltrifluoroacetonato)dioxouranate, Cs[UO2(Bu t COCHCOCF3)3]·1.5C6H6·H2O2Differential Ion Exchange in Elliptical Uranyl Diphosphonate Nanotubules106Differential Ion Exchange in Elliptical Uranyl Diphosphonate Nanotubules9Advances in actinide solid-state and coordination chemistry37Uranyl−Organic Assemblies with Acetate-Bearing Phenyl- and Cyclohexyl-Based Ligands45Nanoscale Chemistry of Uranyl Selenates1Recent progress in actinide borate chemistry94Structural Complexity of Barium Uranyl Arsenates: Synthesis, Structure, and Topology of Ba4[(UO2)2(As2O7)3], Ba3[(UO2)2(AsO4)2(As2O7)], and Ba5Ca[(UO2)8(AsO4)4O8]11Peptide-based solids: porosity and zeolitic behavior58Metal-Controlled Assembly of Uranyl Diphosphonates toward the Design of Functional Uranyl Nanotubules77Synthesis and structural study of new potassium uranyl selenates K2(H5O2)(H3O)[(UO2)2(SeO4)4(H2O)2](H2O)4 and K3(H3O)[(UO2)2(SeO4)4(H2O)2](H2O)57Complex clover cross-sectioned nanotubules exist in the structure of the first uranium borate phosphate28Polytypism and oxo-tungstate polyhedra polymerization in novel complex uranyl tungstates13Unprecedented layer topology in the crystal structure of a new organically templated uranyl selenite-selenate19Synthesis and structural studies of a new potassium uranyl selenate K(H5O2)[(UO2)2(SeO4)3(H2O)] with strongly deformed layers8Effect of molecular vibrations on the selectivity character of pyridino-18-crown-6 derivatives towards potassium ion10Selectivity, Kinetics, and Efficiency of Reversible Anion Exchange with TcO4− in a Supertetrahedral Cationic Framework176Structural topology and dimensional reduction in uranyl oxysalts: eight novel phases in the methylamine–(UO2)(NO3)2–H2SeO4–H2O system24Influence of the Organic Species and Oxoanion in the Synthesis of two Uranyl Sulfate Hydrates, (H3O)2[(UO2)2(SO4)3(H2O)]·7H2O and (H3O)2[(UO2)2(SO4)3(H2O)]·4H2O, and a Uranyl Selenate‐Selenite [C5H6N][(UO2)(SeO4)(HSeO3)]15Nanoscale Hemispheres in Novel Mixed-Valent Uranyl Chromate(V,VI), (C3NH10)10[(UO2)13(Cr125+O42)(Cr6+O4)6(H2O)6](H2O)618A calorimetric and thermodynamic investigation of potassium uranyl tungstate K2[(UO2)(W2O8)]7Tetraalkylammonium cations as templates in the construction of two cadmium( ii ) metal–organic frameworks29Crystal Chemistry of Uranium Oxides and Minerals27Organic templates promoted photocatalytic and photoluminescent properties between two coordination polymers19Controlled Synthesis of Thorium and Uranium Oxide Nanocrystals73Hybrid Uranyl Arsonate Coordination Nanocages18Reactivity of U3+ Metallocene Allyl Complexes Leads to a Nanometer-Sized Uranium Carbonate, [(C5Me5)2U]6(μ-κ1:κ2-CO3)623Symmetry reduction in uranyl compounds with [(UO2)2(TO4)3]2- (T = Se, S, Mo) layers: crystal structures of the new guanidinium uranyl selenate and methylammonium uranyl sulfate17The role of potassium atoms in the formation of uranyl selenates: the crystal structure and synthesis of two novel compounds9Novel type of molecular connectivity in one-dimensional uranyl compounds: [K@(18-crown-6)(H2O)][(UO2)(SeO4)(NO3)], a new potassium uranyl selenate with 18-crown-6 ether11Isolated Uranyl Chromate and Polychromate Units in Crown Ether Templated Compounds18Chemical and Structural Evolution in the Th–SeO 3 2– /SeO 4 2– System: from Simple Selenites to Cluster-Based Selenate Compounds29Hybrid Materials Based on Multifunctional Phosphonic Acids4Hybrid One‐Dimensional 15‐Crown‐5‐ether‐uranyl‐selenate Polymers in [K@(C10H20O5)][(UO2)(SeO4)(HSeO4)(H2O)]: Synthesis and Characterization9Topologically and geometrically flexible structural units in seven new organically templated uranyl selenates and selenite–selenates22Semiconductive Nanotube Array Constructed from Giant [PbII18I54(I2)9] Wheel Clusters104Semiconductive Nanotube Array Constructed from Giant [PbII18I54(I2)9] Wheel Clusters20Crown-ether-templated uranyl selenates: novel family of mixed organic-inorganic actinide compounds9Microporous uranyl chromates successively formed by evaporation from acidic solution9Probing the Influence of Acidity and Temperature to Th(IV) on Hydrolysis, Nucleation, and Structural Topology16Synthesis and Study of the First Zeolitic Uranium Borate22Complex Inorganic Actinide Materials1A Large Family of Centrosymmetric and Chiral f-Element-Bearing Iodate Selenates Exhibiting Coordination Number and Dimensional Reductions26Crown Ethers and Their Alkali Metal Ion Complexes as Assembler Groups in Uranyl–Organic Coordination Polymers with cis-1,3-, cis-1,2-, and trans-1,2-Cyclohexanedicarboxylates34Uranyl Sulfate Nanotubules Templated by N-phenylglycine16In Situ Reduction from Uranyl Ion into a Tetravalent Uranium Trimer and Hexamer Featuring Ion-Exchange Properties and the Alexandrite Effect16Structural unit charge density and molecular cation templating effects on orientational geometric isomerism and interlayer spacing in 2-D uranyl sulfates11High-Pressure Synthesis, Structural, and Spectroscopic Studies of the Ni–U–O System15Complex Uranyl Dichromates Templated by Aza-Crowns3Pd/PTABS: Catalyst for Efficient C−H (Hetero)Arylation of 1,3,4‐Oxadiazoles Using Bromo(Hetero)Arenes18Tubelike Uranyl–Phenylenediacetate Assemblies from Screening of Ligand Isomers and Structure-Directing Counterions28Topological analysis of the layered uranyl compounds bearing slabs with UO2:TO4ratio of 2:35Hybrid Uranyl–Phosphonate Coordination Nanocage8Uranyl Tricarballylate Triperiodic and Nanotubular Species. Counterion Control of Nanotube Diameter13Organically Templated Layered Uranyl Molybdate [C3H9NH+]4[(UO2)3(MoO4)5] Structurally Based on Mineral-Related Modular Units6Structural topology of uranyl chromate-dichromates: Preparation and crystal structures of [dabcoH2][(UO2)(CrO4)(Cr2O7)](H2O)2, [dmedaH2][(UO2)(CrO4)(Cr2O7)](H2O) and [pyH]4[(UO2)(CrO4)2(Cr2O7)]2Successive Crystallization of Organically Templated Uranyl Sulfates: Synthesis and Crystal Structures of [pyH](H3O)[(UO2)3(SO4)4(H2O)2], [pyH]2[(UO2)6(SO4)7(H2O)], and [pyH]2[(UO2)2(SO4)3]3A chalcogenide-cluster-based semiconducting nanotube array with oriented photoconductive behavior25Framework Uranyl Silicates: Crystal Chemistry and a New Route for the Synthesis10Organically Templated Uranyl Sulfates and Selenates: Structural Complexity and Crystal Chemical Restrictions for Isotypic Compounds Formation7Nanotube Structure of AsPS4–xSex (x = 0, 1)2Results of 25-Year Studies of Uranium Compounds at the Department of Crystallography of St. Petersburg State University3

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  1. ChemInform Abstract: A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds.

    ChemInform · 2008-04-02

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

    Read original paper ↗ ·

  2. Preparation, Structures, and Photocatalytic Properties of Three New Uranyl−Organic Assembly Compounds

    Inorganic Chemistry · 2008-04-30

    Zuolei Liao, Guodong Li, Minghui Bi, Jie‐Sheng Chen

    Read original paper ↗ ·

  3. An Open-Framework Thorium Sulfate Hydrate with 11.5 Å Voids

    Inorganic Chemistry · 2008-09-24

    Richard E. Wilson, S. Skanthakumar, Karah E. Knope, Christopher L. Cahill, L. Soderholm

    Read original paper ↗ ·

  4. Two novel uranyl–organic frameworks with cyclohexane-1,3-dicarboxylate ligands

    CrystEngComm · 2008-11-19

    P. Thuéry

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  5. Novel layered uranyl arsenates, Ag6[(UO2)2(As2O7)(As4O13)] and AI6[(UO2)2(AsO4)2(As2O7)] (AI–Ag and Na): first observation of a linear As4O136− anion and structure type evolution

    Journal of Materials Chemistry · 2009-01-01

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

    Read original paper ↗ ·

  6. Protonated 3-amino-1,2,4-triazole templated luminescent lanthanide isophthalates with a rare (3,6)-connected topology

    CrystEngComm · 2009-01-01

    Pei‐Xiu Yin, Zhaoji Li, Jian Zhang, Lei Zhang, Qipu Lin, Ye‐Yan Qin, Yuan‐Gen Yao

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  7. Alternative approaches to structure description

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  8. Anion-topology approach

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  9. Basic concepts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  10. Copyright Page

    Unknown journal · 2009-01-22

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  11. Dedication

    Unknown journal · 2009-01-22

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  12. Dimensional reduction in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  13. Graph theory applied to low-dimensional structural units in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  14. Preface

    Unknown journal · 2009-01-22

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  15. Structural Crystallography of Inorganic Oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  16. Topology of framework structures in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  17. Amine-templated uranyl selenates with chiral [(UO2)2(SeO4)3(H2O)]2– layers: topology, isomerism, structural relationships

    Zeitschrift für Kristallographie · 2009-05-01

    Sergey V. Krivovichev, Vladislav V. Gurzhiy, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  18. Crystal chemistry of anhydrous Li uranyl phosphates and arsenates. II. Tubular fragments and cation–cation interactions in the 3D framework structures of Li6[(UO2)12(PO4)8(P4O13)], Li5[(UO2)13(AsO4)9(As2O7)], Li[(UO2)4(AsO4)3] and Li3[(UO2)7(AsO4)5O)]

    Journal of Solid State Chemistry · 2009-08-09

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

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  19. Crystal structures of crown and aza-crown ether complexes with zirconium, hafnium, niobium, and tantalum fluorometallates

    Journal of Structural Chemistry · 2009-12-01

    Marina S. Fonarı, Nina G. Furmanova, Yu. A. Simonov

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  20. NDTB‐1: A Supertetrahedral Cationic Framework That Removes TcO4− from Solution

    Angewandte Chemie International Edition · 2009-12-28

    Shuao Wang, Evgeny V. Alekseev, Juan Diwu, William H. Casey, Brian L. Phillips, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  21. NDTB‐1: A Supertetrahedral Cationic Framework That Removes TcO4− from Solution

    Angewandte Chemie · 2009-12-28

    Shuao Wang, Evgeny V. Alekseev, Juan Diwu, William H. Casey, Brian L. Phillips, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  22. Amine templated two- and three-dimensional uranyl sulfates

    Dalton Transactions · 2010-01-01

    Mohan Singh Bharara, Anne E. V. Gorden

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  23. Cubic and rhombohedral heterobimetallic networks constructed from uranium, transition metals, and phosphonoacetate: new methods for constructing porous materials

    Chemical Communications · 2010-01-01

    A.N. Alsobrook, Brad G. Hauser, Joseph T. Hupp, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  24. Partially ordered organic-inorganic nanocomposites in the system UO2SeO4-H2O-NH3(CH2)9NH3

    Radiochemistry · 2010-02-01

    Sergey V. Krivovichev, Vladislav V. Gurzhiy, Peter Carman Burns, Ivan Gundarovich Tananaev, Boris F. Myasoedov

    Read original paper ↗ ·

  25. Actinyl Compounds with Hexavalent Elements (S, Cr, Se, Mo) – Structural Diversity, Nanoscale Chemistry, and Cellular Automata Modeling

    European Journal of Inorganic Chemistry · 2010-05-25

    Sergey V. Krivovichev

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  26. Crystal Chemistry of the Potassium and Rubidium Uranyl Borate Families Derived from Boric Acid Fluxes

    Inorganic Chemistry · 2010-06-18

    Shuao Wang, Evgeny V. Alekseev, Jared T. Stritzinger, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  27. Technetium‐99 MAS NMR Spectroscopy of a Cationic Framework Material that Traps TcO4− Ions

    Angewandte Chemie International Edition · 2010-07-15

    Ping Yu, Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, David T Hobbs, Thomas E. Albrecht‐Schmitt, Brian L. Phillips, William H. Casey

    Read original paper ↗ ·

  28. Technetium‐99 MAS NMR Spectroscopy of a Cationic Framework Material that Traps TcO4− Ions

    Angewandte Chemie · 2010-07-15

    Ping Yu, Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, David T Hobbs, Thomas E. Albrecht‐Schmitt, Brian L. Phillips, William H. Casey

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  29. Crystal and molecular structure of a crystal solvate of cesium tris(pivaloyltrifluoroacetonato)dioxouranate, Cs[UO2(Bu t COCHCOCF3)3]·1.5C6H6·H2O

    Radiochemistry · 2010-08-01

    Georgii V. Sidorenko, Mikhail S. Grigoriev, Vladislav V. Gurzhiy, Sergey V. Krivovichev, D.N. Suglobov

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  30. Differential Ion Exchange in Elliptical Uranyl Diphosphonate Nanotubules

    Angewandte Chemie International Edition · 2010-10-12

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  31. Differential Ion Exchange in Elliptical Uranyl Diphosphonate Nanotubules

    Angewandte Chemie · 2010-10-12

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  32. Advances in actinide solid-state and coordination chemistry

    MRS Bulletin · 2010-11-01

    Peter Carman Burns, Yasuhisa Ikeda, Ken Czerwinski

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  33. Uranyl−Organic Assemblies with Acetate-Bearing Phenyl- and Cyclohexyl-Based Ligands

    Crystal Growth & Design · 2010-12-09

    P. Thuéry

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  34. Nanoscale Chemistry of Uranyl Selenates

    Springer eBooks · 2011-01-01

    Sergey V. Krivovichev, Vladislav V. Gurzhiy, Ivan Gundarovich Tananaev, Boris F. Myasoedov

    Read original paper ↗ ·

  35. Recent progress in actinide borate chemistry

    Chemical Communications · 2011-01-01

    Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  36. Structural Complexity of Barium Uranyl Arsenates: Synthesis, Structure, and Topology of Ba4[(UO2)2(As2O7)3], Ba3[(UO2)2(AsO4)2(As2O7)], and Ba5Ca[(UO2)8(AsO4)4O8]

    Crystal Growth & Design · 2011-05-30

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

    Read original paper ↗ ·

  37. Peptide-based solids: porosity and zeolitic behavior

    Journal of Materials Chemistry · 2011-11-02

    Rui Afonso, Adélio Miguel Magalhães Mendes, Luı́s Gales

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  38. Metal-Controlled Assembly of Uranyl Diphosphonates toward the Design of Functional Uranyl Nanotubules

    Inorganic Chemistry · 2011-11-03

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  39. Synthesis and structural study of new potassium uranyl selenates K2(H5O2)(H3O)[(UO2)2(SeO4)4(H2O)2](H2O)4 and K3(H3O)[(UO2)2(SeO4)4(H2O)2](H2O)5

    Radiochemistry · 2011-12-01

    Vladislav V. Gurzhiy, Olga S. Tyumentseva, Sergey V. Krivovichev, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  40. Complex clover cross-sectioned nanotubules exist in the structure of the first uranium borate phosphate

    Chemical Communications · 2012-01-01

    Shijun Wu, Shuao Wang, Juan Diwu, Wulf Depmeier, Thomas Malcherek, Evgeny V. Alekseev, Thomas E. Albrecht‐Schmitt

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  41. Polytypism and oxo-tungstate polyhedra polymerization in novel complex uranyl tungstates

    Dalton Transactions · 2012-01-01

    Andrey Seliverstov, Evgeny V. Suleimanov, Evgeny V. Chuprunov, Н. В. Сомов, Elena M. Zhuchkova, Maxim I. Lelet, Konstantin Rozov, Wulf Depmeier, Sergey V. Krivovichev, Evgeny V. Alekseev

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  42. Unprecedented layer topology in the crystal structure of a new organically templated uranyl selenite-selenate

    Mendeleev Communications · 2012-01-01

    Vadim M. Kovrugin, Vladislav V. Gurzhiy, Sergey V. Krivovichev, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  43. Synthesis and structural studies of a new potassium uranyl selenate K(H5O2)[(UO2)2(SeO4)3(H2O)] with strongly deformed layers

    Radiochemistry · 2012-02-01

    Vladislav V. Gurzhiy, Olga S. Tyumentseva, Sergey V. Krivovichev, Ivan Gundarovich Tananaev, Boris F. Myasoedov

    Read original paper ↗ ·

  44. Effect of molecular vibrations on the selectivity character of pyridino-18-crown-6 derivatives towards potassium ion

    Chemical Physics Letters · 2012-03-10

    Yin Li, Péter Huszthy, Sándor Kunsági‐Máté

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  45. Selectivity, Kinetics, and Efficiency of Reversible Anion Exchange with TcO4− in a Supertetrahedral Cationic Framework

    Advanced Functional Materials · 2012-03-20

    Shuao Wang, Ping Yu, Bryant A. Purse, Matthew J. Orta, Juan Diwu, William H. Casey, Brian L. Phillips, Evgeny V. Alekseev, Wulf Depmeier, David T Hobbs, Thomas E. Albrecht‐Schmitt

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  46. Structural topology and dimensional reduction in uranyl oxysalts: eight novel phases in the methylamine–(UO2)(NO3)2–H2SeO4–H2O system

    Structural Chemistry · 2012-05-05

    Vadim M. Kovrugin, Vladislav V. Gurzhiy, Sergey V. Krivovichev

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  47. Influence of the Organic Species and Oxoanion in the Synthesis of two Uranyl Sulfate Hydrates, (H3O)2[(UO2)2(SO4)3(H2O)]·7H2O and (H3O)2[(UO2)2(SO4)3(H2O)]·4H2O, and a Uranyl Selenate‐Selenite [C5H6N][(UO2)(SeO4)(HSeO3)]

    Zeitschrift für anorganische und allgemeine Chemie · 2012-08-08

    Laurent J. Jouffret, Ernest M. Wylie, Peter Carman Burns

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  48. Nanoscale Hemispheres in Novel Mixed-Valent Uranyl Chromate(V,VI), (C3NH10)10[(UO2)13(Cr125+O42)(Cr6+O4)6(H2O)6](H2O)6

    Inorganic Chemistry · 2012-08-20

    Oleg I. Siidra, Еvgeny V. Nazarchuk, Anatoly A. Petrunin, Roman A. Kayukov, Sergey V. Krivovichev

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  49. A calorimetric and thermodynamic investigation of potassium uranyl tungstate K2[(UO2)(W2O8)]

    The Journal of Chemical Thermodynamics · 2012-10-08

    Maxim I. Lelet, Olga V. Ogurtsova, Evgeny V. Suleimanov, Charles A. Geiger, Wulf Depmeier, Evgeny V. Alekseev

    Read original paper ↗ ·

  50. Tetraalkylammonium cations as templates in the construction of two cadmium( ii ) metal–organic frameworks

    CrystEngComm · 2012-11-12

    Jian‐Di Lin, Shuai‐Hua Wang, Li‐Zhen Cai, Fa‐Kun Zheng, Guo‐Cong Guo, Jin‐Shun Huang

    Read original paper ↗ ·
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