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RESEARCH PAPER · Journal of Materials Chemistry · 2007

Synthesis of nanocrystals and morphology control of hydrothermally prepared LiFePO4

Brian L. Ellis, Wang Hay Kan, W. R. M. Makahnouk, Linda F. Nazar

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Synthesis of nanocrystals and morphology control of hydrothermally prepared LiFePO4OriginalMorphology and Electrochemistry of Hydrothermally Prepared LiMnPO41Nanostructured electrode materials for electrochemical energy storage and conversion638Surface structures and crystal morphologies of LiFePO4: relevance to electrochemical behaviour256Characterization of the surface of positive electrodes for Li-ion batteries using 7Li MAS NMR20Hydrothermal synthesis of LiFePO4 with small particle size and its electrochemical properties40Rapid microwave-solvothermal synthesis of phospho-olivine nanorods and their coating with a mixed conducting polymer for lithium ion batteries193The Importance of Nanotechnology in Developing Better Energy Storage Materials for Automotive Transport1Synthesis of Nanowire and Hollow LiFePO4 Cathodes for High-Performance Lithium Batteries178The Design of a LiFePO4/Carbon Nanocomposite With a Core–Shell Structure and Its Synthesis by an In Situ Polymerization Restriction Method878The Design of a LiFePO4/Carbon Nanocomposite With a Core–Shell Structure and Its Synthesis by an In Situ Polymerization Restriction Method91Comparison of Microwave Assisted Solvothermal and Hydrothermal Syntheses of LiFePO4/C Nanocomposite Cathodes for Lithium Ion Batteries234Materials for High-energy Density Batteries4Storage performance of LiFePO 4 nanoplates264Aging of the LiNi[sub 1∕2]Mn[sub 1∕2]O[sub 2] Positive Electrode Interface in Electrolyte59Nanoscale design to enable the revolution in renewable energy431Solid Solution Phases in the Olivine-Type LiMnPO[sub 4]/MnPO[sub 4] System41Dimensionally Modulated, Single-Crystalline LiMPO4 (M= Mn, Fe, Co, and Ni) with Nano-Thumblike Shapes for High-Power Energy Storage169Solvothermal Synthesis of LiFePO4 Hierarchically Dumbbell-Like Microstructures by Nanoplate Self-Assembly and Their Application as a Cathode Material in Lithium-Ion Batteries193Copper-substituted, lithium rich iron phosphate as cathode material for lithium secondary batteries21Hydrothermal preparation of LiFePO4 nanocrystals mediated by organic acid136LiFePO4 thin films grown by pulsed laser deposition: Effect of the substrate on the film structure and morphology28Crystal Structure and Electrochemical Properties of A2MPO4F Fluorophosphates (A = Na, Li; M = Fe, Mn, Co, Ni)341Solid-State Materials for Clean Energy: Insights from Atomic-Scale Modeling28Microwave solid-state synthesis and electrochemical properties of carbon-free Li3V2(PO4)3 as cathode materials for lithium batteries49Directed growth of nanoarchitectured LiFePO4 electrode by solvothermal synthesis and their cathode properties73Hydrothermal synthesis of nanostructured MnO2 under magnetic field for rechargeable lithium batteries14Engineering nanostructured electrodes and fabrication of film electrodes for efficient lithium ion intercalation268Melt Casting LiFePO[sub 4]33Melt Casting LiFePO[sub 4]39Morphology-controlled solvothermal synthesis of LiFePO4 as a cathode material for lithium-ion batteries201Nanostructured Electrode Materials for Lithium-Ion Batteries4Rapid one-pot synthesis of LiMPO4 (M = Fe, Mn) colloidal nanocrystals by supercritical ethanol process68Positive Electrode Materials for Li-Ion and Li-Batteries1697Template-Free Hydrothermal Synthesis of Nanoembossed Mesoporous LiFePO4 Microspheres for High-Performance Lithium-Ion Batteries221In situ growth of LiFePO4 nanorod arrays under hydrothermal condition39Preparation of LiFePO4 Mesocrystals Consisting of Nanorods through Organic-Mediated Parallel Growth from a Precursor Phase40Recent atomistic modelling studies of energy materials: batteries included45Relationship between surface chemistry and electrochemical behavior of LiNi1/2Mn1/2O2 positive electrode in a lithium-ion battery48Understanding the Shifts in the Redox Potentials of Olivine LiM1−yMyPO4 (M = Fe, Mn, Co, and Mg) Solid Solution Cathodes199Mechanism for Hydrothermal Synthesis of LiFePO4 Platelets as Cathode Material for Lithium-Ion Batteries150Self-assembly of LiFePO4 nanodendrites in a novel system of ethylene glycol–water45Small capacity decay of lithium iron phosphate (LiFePO4) synthesized continuously in supercritical water: Comparison with solid-state method45Morphological solution for enhancement of electrochemical kinetic performance of LiFePO456Microwave-Solvothermal Synthesis of Nanostructured Li 2 MSiO 4 /C (M = Mn and Fe) Cathodes for Lithium-Ion Batteries342Recent Progress in Nanostructured Cathode Materials for Lithium Secondary Batteries278Surfactant assisted synthesis of lamellar nanostructured LiFePO4 at 388K17Development and challenges of LiFePO 4 cathode material for lithium-ion batteries1301Olivine LiFePO 4 : development and future372Iron and Manganese Pyrophosphates as Cathodes for Lithium-Ion Batteries141Preparation and characterization of high-rate and long-cycle LiFePO4/C nanocomposite as cathode material for lithium-ion battery25Roles of nanosize in lithium reactive nanomaterials for lithium ion batteries415Ammonia Assisted Hydrothermal Synthesis of Monodisperse LiFePO4∕C Microspheres as Cathode Material for Lithium Ion Batteries40Biotemplating of phosphate hierarchical rechargeable LiFePO4/C spirulina microstructures78Crystal Structure and Electrochemical Performances of Proton-Substituted Li2MnO3 and the Nanocomposites Treated by LiMnO28Facile synthesis of LiMnPO4 olivines with a plate-like morphology from a dittmarite-type KMnPO4·H2O precursor29Influence of particle size on solid solution formation and phase interfaces in Li0.5FePO4 revealed by 31P and 7Li solid state NMR spectroscopy31LiMnPO4 Nanoparticles Prepared through the Reaction between Li3PO4 and Molten Aqua-complex of MnSO428One-Pot Synthesis of Multi-Morphous LiFePO4 Nanoparticles in Polyol Medium27Materials Challenges and Opportunities of Lithium Ion Batteries1065Monodisperse Porous LiFePO4 Microspheres for a High Power Li-Ion Battery Cathode673General synthesis and morphology control of LiMnPO4 nanocrystals via microwave-hydrothermal route47Hydrothermal synthesis of ultra-thin LiFePO4 platelets for Li-ion batteries23Hierarchical Carbon‐Coated LiFePO4 Nanoplate Microspheres with High Electrochemical Performance for Li‐Ion Batteries185Anisotropic Phase Boundary Morphology in Nanoscale Olivine Electrode Particles119Microwave-Assisted Solvothermal Synthesis and Characterization of Metastable LiFe1−x(VO)xPO4 Cathodes36Real-time synchrotron powder X-ray diffraction study of the antisite defect formation during sub- and supercritical synthesis of LiFePO4and LiFe1−xMnxPO4nanoparticles38Electronic Conductivity and Defect Chemistry of Heterosite FePO440Raman spectroscopy of carbon-coated LiCoPO4 and LiFePO4 olivines158Synthesis and electrochemical characterization of LiNi0.5Mn1.5O4 by one-step precipitation method with ammonium carbonate as precipitating agent42Citric Acid- and Ammonium-Mediated Morphological Transformations of Olivine LiFePO4 Particles79Tailoring Native Defects in LiFePO 4 : Insights from First-Principles Calculations189Synthesis of Nano-LiMnPO4 from MnPO4·H2O Prepared by Mechanochemistry31Plate-type LiFePO4 nanocrystals by low temperature polyol-assisted solvothermal reaction and its electrochemical properties24Electrochemical Analysis of Conductive Polymer‐Coated LiFePO4 Nanocrystalline Cathodes with Controlled Morphology42Topochemical Synthesis of Sodium Metal Phosphate Olivines for Sodium-Ion Batteries309Enhancement of F-doping on the electrochemical behavior of carbon-coated LiFePO4 nanoparticles prepared by hydrothermal route104Lithium Intercalation Cathode Materials for Lithium‐Ion Batteries12Synthesis and electrode performance of carbon coated Na2FePO4F for rechargeable Na batteries270A general solution-chemistry route to the synthesis LiMPO4 (M=Mn, Fe, and Co) nanocrystals with [010] orientation for lithium ion batteries52Synthesis of spindle-shaped nanoporous C–LiFePO4 composite and its application as a cathodes material in lithium ion batteries17Synthesis of the LiFePO4/C core–shell nanocomposite using a nano-FePO4/polythiophene as an iron source26Titanium phosphates as positive electrode in lithium-ion batteries: composition, phase purity and electrochemical performance25High-Rate LiFePO4 Electrode Material Synthesized by Chemical Grinding Method0A Comparison of Crystal Structures and Electrode Performance between Na2FePO4F and Na2Fe0.5Mn0.5PO4F Synthesized by Solid-State Method for Rechargeable Na-Ion Batteries84Bio-synthesis participated mechanism of mesoporous LiFePO4/C nanocomposite microspheres for lithium ion battery42Design of nanostructured materials for advanced lithium ion batteries2Ethylene glycol-assisted nanocrystallization of LiFePO4 for a rechargeable lithium-ion battery cathode39Hydrothermally synthesized LiFePO4 crystals with enhanced electrochemical properties: simultaneous suppression of crystal growth along [010] and antisite defect formation156Preparation of LiFePO4/Carbon/PANI-CSA Composite and Its Properties as High-Capacity Cathodes for Lithium Ion Batteries20Solvothermal synthesis of electroactive lithium iron tavorites and structure of Li2FePO4F54Synthesis of LiFePO4Nanoparticles and Crystal Formation Mechanism during Solvothermal Reaction20Synthesis of LiFePO4Using Fe3+Precursors in Polyol Medium5Low-temperature synthesis of LiFePO4 nanocrystals by solvothermal route23First-principles studies of the effects of impurities on the ionic and electronic conduction in LiFePO472Self-Assembled LiFePO4/C Nano/Microspheres by Using Phytic Acid as Phosphorus Source108Synthesis Processes for Li-Ion Battery Electrodes – From Solid State Reaction to Solvothermal Self-Assembly Methods4Nano-layered LiFePO4 particles converted from nano-layered ferrous phenylphosphonate templates11Hydrothermal and Solvothermal Process Towards Development of LiMPO4 (M = Fe, Mn) Nanomaterials for Lithium‐Ion Batteries349Fabrication of promising LiFePO4/C composite with a core–shell structure by a moderate in situ carbothermal reduction method35Low temperature hydrothermal synthesis and electrochemical performances of LiFePO4 microspheres as a cathode material for lithium-ion batteries7Synthesis of Electrochemically Active LiMnPO4 via MnPO4·H2O with Different Morphology Prepared By Facile Precipitation17New Method of Postmodifying the Particle Size and Morphology of LiFePO4 via Supercritical Carbon Dioxide17Self-assembly of highly uniform LiFePO4 hierarchical nanostructures by surfactant molecules in a new mixture medium10Formation Mechanism of LiFePO4 Sticks Grown by a Microwave‐Assisted Liquid‐Phase Process23The effect of ammonia concentration on the morphology and electrochemical properties of LiFePO4 synthesized by ammonia assisted hydrothermal route47LiFePO 4 Nanocrystals: Liquid-Phase Reduction Synthesis and Their Electrochemical Performance34Effect of Acticarbon on the Electrochemical Characteristics of LiFePO4 Battery Powder by Microwave Hydrothermal0Simultaneous enhancement of electronic and Li+ ion conductivity in LiFePO453Surfactant-assisted synthesis of hybrid lithium iron phosphate nanoparticles for enhancing electrochemical performance10介孔球形LiFePO4的低温水热合成及其电化学性能1Crystal Orientation Tuning of LiFePO4Nanoplates for High Rate Lithium Battery Cathode Materials370Synchrotron X-rays and neutrons as essential tools in Li battery research: Examples of oxide, phosphate and silicate-based positive electrodes5Hydrothermal synthesis of Li4Ti5O12/C nanostructured composites: Morphology and electrochemical performance26Continuous synthesis of lithium iron phosphate (LiFePO4) nanoparticles in supercritical water: Effect of mixing tee52V2O5/single-walled carbon nanotube hybrid mesoporous films as cathodes with high-rate capacities for rechargeable lithium ion batteries51Novel Synthesis of Submicrometric LiNi0.5Mn1.5O4 by Electrospinning Method2Immobilization of nanosized LiFePO4 spheres by 3D coralloid carbon structure with large pore volume and thin walls for high power lithium-ion batteries42A rapid, one-pot microwave-solvothermal synthesis of a hierarchical nanostructured graphene/LiFePO4 hybrid as a high performance cathode for lithium ion batteries50An economic and scalable approach to synthesize high power LiFePO4/C nanocomposites from nano-FePO4 precipitated from an impinging jet reactor19Direct evidence of antisite defects in LiFe0.5Mn0.5PO4via atomic-level HAADF-EELS29High performance LiFePO4 microsphere composed of nanofibers with an alcohol-thermal approach46Hydrothermal synthetic strategies of inorganic semiconducting nanostructures548Improving the performance of a LiFePO4 cathode based on electrochemically cleaved graphite oxides with high hydrophilicity and good conductivity35Morphology Control of LiMnPO4 Cathodes by a Careful Choice of Additives0Nanostructured Electrode Materials for Lithium-ion Battery0Novel morphology-controlled synthesis of homogeneous LiFePO4 for Li-ion batteries using an organic phosphate source15Waste minimization and recovery of valuable metals from spent lithium-ion batteries – a review63X-ray diffraction study of LiFePO4 synthesized by hydrothermal method25Long-term cycle stability at a high current for nanocrystalline LiFePO 4 coated with a conductive polymer9Temperature Dependence of Aliovalent-Vanadium Doping in LiFePO4 Cathodes95Large discharge capacities at high current rates for carbon-coated LiMnPO4 nanocrystalline cathodes66Nano particle LiFePO4 prepared by solvothermal process58A core–shell LiFePO4/C nanocomposite prepared via a sol–gel method assisted by citric acid45Nanoscaled LiFePO4 synthesized solvothermally by wettish precursor0Energy Storage: Rechargeable Lithium Batteries1In-situ X-ray absorption spectroscopy analysis of capacity fade in nanoscale-LiCoO262One-pot synthesis of mixed-valence MoO x on carbon nanotube as an anode material for lithium ion batteries36Development of sulfur-polyacrylonitrile/graphene composite cathode for lithium batteries1Rapid synthesis of LiFePO4 nanoparticles by microwave-assisted hydrothermal method7Defects in Hydrothermally Synthesized LiFePO4 and LiFe1-xMnxPO4 Cathode Materials113Size and shape control of LiFePO4 nanocrystals for better lithium ion battery cathode materials141Low cost synthesis of LiFePO4/C cathode materials with Fe2O322Polyanionic (Phosphates, Silicates, Sulfates) Frameworks as Electrode Materials for Rechargeable Li (or Na) Batteries1210Novel rapid synthesis method of LiFePO4/C cathode material by high-frequency induction heating18NMR monitoring of electrode/electrolyte interphase in the case of air-exposed and carbon coated LiFePO 420Hydrothermal synthesis of Li2MnSiO4: Mechanism and influence of precursor concentration on electrochemical properties4Synthesis of LiFePO4/C nanocomposites via ionic liquid assisted hydrothermal method13Cathode Materials Produced by Spray Flame Synthesis for Lithium Ion Batteries2Defect chemistry of phospho-olivine nanoparticles synthesized by a microwave-assisted solvothermal process12Synthesis of Microspherical LiFePO4-Carbon Composites for Lithium-Ion Batteries20

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  1. Morphology and Electrochemistry of Hydrothermally Prepared LiMnPO4

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  3. Surface structures and crystal morphologies of LiFePO4: relevance to electrochemical behaviour

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  4. Characterization of the surface of positive electrodes for Li-ion batteries using 7Li MAS NMR

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  5. Hydrothermal synthesis of LiFePO4 with small particle size and its electrochemical properties

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  6. Rapid microwave-solvothermal synthesis of phospho-olivine nanorods and their coating with a mixed conducting polymer for lithium ion batteries

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  7. The Importance of Nanotechnology in Developing Better Energy Storage Materials for Automotive Transport

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  8. Synthesis of Nanowire and Hollow LiFePO4 Cathodes for High-Performance Lithium Batteries

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  9. The Design of a LiFePO4/Carbon Nanocomposite With a Core–Shell Structure and Its Synthesis by an In Situ Polymerization Restriction Method

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  10. The Design of a LiFePO4/Carbon Nanocomposite With a Core–Shell Structure and Its Synthesis by an In Situ Polymerization Restriction Method

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  11. Comparison of Microwave Assisted Solvothermal and Hydrothermal Syntheses of LiFePO4/C Nanocomposite Cathodes for Lithium Ion Batteries

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  12. Materials for High-energy Density Batteries

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  13. Storage performance of LiFePO 4 nanoplates

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  14. Aging of the LiNi[sub 1∕2]Mn[sub 1∕2]O[sub 2] Positive Electrode Interface in Electrolyte

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  16. Solid Solution Phases in the Olivine-Type LiMnPO[sub 4]/MnPO[sub 4] System

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  17. Dimensionally Modulated, Single-Crystalline LiMPO4 (M= Mn, Fe, Co, and Ni) with Nano-Thumblike Shapes for High-Power Energy Storage

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  18. Solvothermal Synthesis of LiFePO4 Hierarchically Dumbbell-Like Microstructures by Nanoplate Self-Assembly and Their Application as a Cathode Material in Lithium-Ion Batteries

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  19. Copper-substituted, lithium rich iron phosphate as cathode material for lithium secondary batteries

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  20. Hydrothermal preparation of LiFePO4 nanocrystals mediated by organic acid

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  21. LiFePO4 thin films grown by pulsed laser deposition: Effect of the substrate on the film structure and morphology

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  22. Crystal Structure and Electrochemical Properties of A2MPO4F Fluorophosphates (A = Na, Li; M = Fe, Mn, Co, Ni)

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  23. Solid-State Materials for Clean Energy: Insights from Atomic-Scale Modeling

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  24. Microwave solid-state synthesis and electrochemical properties of carbon-free Li3V2(PO4)3 as cathode materials for lithium batteries

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  28. Melt Casting LiFePO[sub 4]

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  32. Rapid one-pot synthesis of LiMPO4 (M = Fe, Mn) colloidal nanocrystals by supercritical ethanol process

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  34. Template-Free Hydrothermal Synthesis of Nanoembossed Mesoporous LiFePO4 Microspheres for High-Performance Lithium-Ion Batteries

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  35. In situ growth of LiFePO4 nanorod arrays under hydrothermal condition

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  36. Preparation of LiFePO4 Mesocrystals Consisting of Nanorods through Organic-Mediated Parallel Growth from a Precursor Phase

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  37. Recent atomistic modelling studies of energy materials: batteries included

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  38. Relationship between surface chemistry and electrochemical behavior of LiNi1/2Mn1/2O2 positive electrode in a lithium-ion battery

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  39. Understanding the Shifts in the Redox Potentials of Olivine LiM1−yMyPO4 (M = Fe, Mn, Co, and Mg) Solid Solution Cathodes

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  40. Mechanism for Hydrothermal Synthesis of LiFePO4 Platelets as Cathode Material for Lithium-Ion Batteries

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  41. Self-assembly of LiFePO4 nanodendrites in a novel system of ethylene glycol–water

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  42. Small capacity decay of lithium iron phosphate (LiFePO4) synthesized continuously in supercritical water: Comparison with solid-state method

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  43. Morphological solution for enhancement of electrochemical kinetic performance of LiFePO4

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  44. Microwave-Solvothermal Synthesis of Nanostructured Li 2 MSiO 4 /C (M = Mn and Fe) Cathodes for Lithium-Ion Batteries

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  45. Recent Progress in Nanostructured Cathode Materials for Lithium Secondary Batteries

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  46. Surfactant assisted synthesis of lamellar nanostructured LiFePO4 at 388K

    Applied Surface Science · 2010-10-11

    Chao Liu, Dongxia Ma, Xiujie Ji, Shanshan Zhao, Li Song

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  47. Development and challenges of LiFePO 4 cathode material for lithium-ion batteries

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    Li-Xia Yuan, Zhaohui Wang, Wu-Xing Zhang, Xianluo Hu, Jitao Chen, Yun-Hui Huang, John Bannister Goodenough

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  48. Olivine LiFePO 4 : development and future

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    Yonggang Wang, Ping He, Haoshen S. Zhou

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  49. Iron and Manganese Pyrophosphates as Cathodes for Lithium-Ion Batteries

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    Hui Zhou, S. Upreti, Natasha A. Chernova, Geoffroy Hautier, Gerbrand Ceder, M. Stanley Whittingham

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  50. Preparation and characterization of high-rate and long-cycle LiFePO4/C nanocomposite as cathode material for lithium-ion battery

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