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RESEARCH PAPER · Review of Scientific Instruments · 2005

High pressurein situx-ray absorption spectroscopy cell for studying simultaneously the liquid phase and the solid/liquid interface

Jan‐Dierk Grunwaldt, Michael Ramin, Markus Rohr, Alexej Michailovski, Greta Ricarda Patzke, Alfons Baiker

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High pressurein situx-ray absorption spectroscopy cell for studying simultaneously the liquid phase and the solid/liquid interfaceOriginalIn situ spectroscopic investigation of heterogeneous catalysts and reaction media at high pressure110Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques105Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken24Behavior of homogeneous and immobilized zinc-based catalysts in cycloaddition of CO2 to propylene oxide62Solvothermal Synthesis and Crystal Structures of Alkali Molybdates15An EXAFS study of the formation of a nanoporous metal–organic framework: evidence for the retention of secondary building units during synthesis157In Situ Extended X-ray Absorption Fine Structure Study during Selective Alcohol Oxidation over Pd/Al2O3 in Supercritical Carbon Dioxide53EXAFS measurements of a working catalyst in the liquid phase: An in situ study of a Ni2P hydrodesulfurization catalyst89Heterogeneous strong base catalysis in supercritical carbon dioxide by mesoporous alumina and sulfated mesoporous alumina10Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry62Identification of the surface species responsible for N2O formation from the chemisorption of NO on Rh/alumina29Design and operation of a high pressure reaction cell for in situ X-ray absorption spectroscopy51Morphological and Kinetic Studies on Hexagonal Tungstates55Targeted Synthesis of Nanostructured Oxide Materials2Design of a high-temperature and high-pressure liquid flow cell for x-ray absorption fine structure measurements under catalytic reaction conditions28Hydrothermal Formation of W/Mo-Oxides: A Multidisciplinary Study of Growth and Shape64In situ XAS study of the Mn(III)(salen)Br catalyzed synthesis of cyclic organic carbonates from epoxides and CO236Transition metal phosphide hydroprocessing catalysts: A review792Gold-catalyzed aerobic oxidation of dibenzylamine: Homogeneous or heterogeneous catalysis?48Chapter 6 Characterization of Catalysts in Reactive Atmospheres by X‐ray Absorption Spectroscopy98Time Resolved IR and X-Ray Simultaneous Spectroscopy: New Opportunities for the Analysis of Fast Chemical-Physical Phenomena in Materials Science18New agitated and thermostatized cell forin situmonitoring of fast reactions by synchrotron SAXS2In situobservation of Ni–Mo–S phase formed on NiMo/Al2O3catalyst sulfided at high pressure by means of Ni and MoK-edge EXAFS spectroscopy12High‐pressure Methods and Equipment3Asymmetric CC Bond‐Formation Reaction with Pd: How to Favor Heterogeneous or Homogeneous Catalysis?15In Situ X-ray Diffraction and Absorption Studies of the Growth and Phase Transformation of Yttrium Hydroxide Nanotubes to Their Oxide Counterparts16Hydrothermal and Solvothermal Syntheses56Interplay Between Size and Crystal Structure of Molybdenum Dioxide Nanoparticles—Synthesis, Growth Mechanism, and Electrochemical Performance92A large-volume gas cell for high-energy X-ray reflectivity investigations of interfaces under pressure10Identification of the Active Species Generated from Supported Pd Catalysts in Heck Reactions: An in situ Quick Scanning EXAFS Investigation103A flow-through reaction cell forin situX-ray diffraction and absorption studies of heterogeneous powder–liquid reactions and phase transformations11In Situ X‐ray Absorption Spectroscopy/Energy‐Dispersive X‐ray Diffraction Studies on the Hydrothermal Formation of Bi2W1–xMoxO6 Nanomaterials32Study of the Chemical Mechanism Involved in the Formation of Tungstite in Benzyl Alcohol by the Advanced QEXAFS Technique34A portable powder-liquid high corrosion-resistant reaction cell for in situ X-ray diffraction and absorption studies of heterogeneous powder-liquid reactions and phase transformations0QEXAFS in Catalysis Research: Principles, Data Analysis, and Applications8In Situ Studies of Solvothermal Synthesis of Energy Materials159Puzzling Mechanism behind a Simple Synthesis of Cobalt and Cobalt Oxide Nanoparticles: In Situ Synchrotron X-ray Absorption and Diffraction Studies70Aliovalent Ni in MoO2Lattice— Probing the Structure and Valence of Ni and Its Implication on the Electrochemical Performance29X-Ray Absorption Fine Structure Analysis of Catalytic Nanomaterials2Revealing Complexity of Nanoparticle Synthesis in Solution by in Situ Hard X-ray Spectroscopy─Today and Beyond52Cell Designs for In Situ and Operando Studies22Metal Nanocatalysts7Hydrothermal and Solvothermal Syntheses239Mechanistic Aspects in the Formation, Growth and Surface Functionalization of Metal Oxide Nanoparticles in Organic Solvents125A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions33CAT-ACT—A new highly versatile x-ray spectroscopy beamline for catalysis and radionuclide science at the KIT synchrotron light facility ANKA134On the mechanism of rapid metal exchange between thiolate-protected gold and gold/silver clusters: a time-resolved in situ XAFS study35Measurements inside a reactor of spatial and temporal profiles on liquid and solid phases through spectroscopic analysis0A versatile liquid-jet/sessile droplet system for operando studies of reactions in liquid dispersions and solutions by X-ray absorption spectroscopy10In situ XAS study of the local structure and oxidation state evolution of palladium in a reduced graphene oxide supported Pd( ii ) carbene complex during an undirected C–H acetoxylation reaction23High‐Pressure High‐Temperature Transparent Fixed‐Bed Reactor for Operando Gas‐Liquid Reaction Follow‐up7Development of photochemical and electrochemical cells for operando X-ray absorption spectroscopy during photocatalytic and electrocatalytic reactions10Mechanistic insights into the selective oxidation of 5-(hydroxymethyl)furfural over silver-based catalysts22In Situ Monitoring of Particle Formation with Spectroscopic and Analytical Techniques Under Solvothermal Conditions11Toward an Intensified Process of Biomass-Derived Monomers: The Influence of 5-(Hydroxymethyl)furfural Byproducts on the Gold-Catalyzed Synthesis of 2,5-Furandicarboxylic Acid45In situ scattering studies of material formation during wet-chemical syntheses1Electronic and Chemical Properties: X‐Ray Absorption and Photoemission1Continuous-flow reactor setup for operando x-ray absorption spectroscopy of high pressure heterogeneous liquid–solid catalytic processes6Versatile in situ/operando Setup for Studying Catalysts by X‐Ray Absorption Spectroscopy under Demanding and Dynamic Reaction Conditions for Energy Storage and Conversion25Design of Single-Atom Catalysts and Tracking Their Fate Using Operando and Advanced X-ray Spectroscopic Tools291In situ and operando study of catalysts during high-temperature high-pressure catalysis in a fixed-bed plug flow reactor with x-ray absorption spectroscopy7In situ catalytic cells for x-ray absorption spectroscopy measurement8An in situ study to shed light on the formation of goethite spindles by pseudomorphic transformation of intermediate phases5Multi-technique operando methods and instruments for simultaneous assessment of thermal catalysis structure, performance, dynamics, and kinetics18Synchrotron radiation XAFS applications in the in situ measurement for energy catalysis2A versatile pressure-cell design for studying ultrafast molecular-dynamics in supercritical fluids using coherent multi-pulse x-ray scattering8Real-Time Multiscale Imaging of Heterogeneous Multistage Reactions: Insights into Nanoscale TiO2 Synthesis9Design and use of a flow cell for observing evolving solid-fluid interfaces in a scanning electron microscope0

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68 direct citing papers saved. Showing the first 50 here; use Browse Matching Papers in the map for all loaded papers.

  1. In situ spectroscopic investigation of heterogeneous catalysts and reaction media at high pressure

    Physical Chemistry Chemical Physics · 2005-01-01

    Jan‐Dierk Grunwaldt, Alfons Baiker

    Read original paper ↗ ·

  2. Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques

    Angewandte Chemie International Edition · 2005-08-02

    Alexej Michailovski, Jan‐Dierk Grunwaldt, Alfons Baiker, Ragnar Kiebach, Wolfgang Bensch, Greta Ricarda Patzke

    Read original paper ↗ ·

  3. Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken

    Angewandte Chemie · 2005-08-02

    Alexej Michailovski, Jan‐Dierk Grunwaldt, Alfons Baiker, Ragnar Kiebach, Wolfgang Bensch, Greta Ricarda Patzke

    Read original paper ↗ ·

  4. Behavior of homogeneous and immobilized zinc-based catalysts in cycloaddition of CO2 to propylene oxide

    Journal of Catalysis · 2005-08-10

    Michael Ramin, Jan‐Dierk Grunwaldt, Alfons Baiker

    Read original paper ↗ ·

  5. Solvothermal Synthesis and Crystal Structures of Alkali Molybdates

    Helvetica Chimica Acta · 2005-09-01

    Alexej Michailovski, J. Willems, Norbert Stock, Greta Ricarda Patzke

    Read original paper ↗ ·

  6. An EXAFS study of the formation of a nanoporous metal–organic framework: evidence for the retention of secondary building units during synthesis

    Chemical Communications · 2006-01-01

    Suzy Surblé, Franck Millange, Christian Serre, Gérard Férey, Richard I. Walton

    Read original paper ↗ ·

  7. In Situ Extended X-ray Absorption Fine Structure Study during Selective Alcohol Oxidation over Pd/Al2O3 in Supercritical Carbon Dioxide

    The Journal of Physical Chemistry B · 2006-05-01

    Jan‐Dierk Grunwaldt, Matteo Caravati, Alfons Baiker

    Read original paper ↗ ·

  8. EXAFS measurements of a working catalyst in the liquid phase: An in situ study of a Ni2P hydrodesulfurization catalyst

    Journal of Catalysis · 2006-05-17

    T KAWAI, Kyoko Kitamura Bando, Yong-Kul Lee, Shigeo Ted Oyama, Wang‐Jae Chun, Kiyotaka Asakura

    Read original paper ↗ ·

  9. Heterogeneous strong base catalysis in supercritical carbon dioxide by mesoporous alumina and sulfated mesoporous alumina

    Catalysis Surveys from Asia · 2006-11-09

    Tsunetake Seki, Makoto Onaka

    Read original paper ↗ ·

  10. Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry

    Chemistry - A European Journal · 2006-11-17

    Alexej Michailovski, Greta Ricarda Patzke

    Read original paper ↗ ·

  11. Identification of the surface species responsible for N2O formation from the chemisorption of NO on Rh/alumina

    Physical Chemistry Chemical Physics · 2006-11-21

    Mark A. Newton, Andrew J. Dent, Steven G. Fiddy, Bhrat Jyoti, John Evans

    Read original paper ↗ ·

  12. Design and operation of a high pressure reaction cell for in situ X-ray absorption spectroscopy

    Catalysis Today · 2006-11-22

    Simon R. Bare, Ning Yang, Shelly D. Kelly, George E. Mickelson, Frank S. Modica

    Read original paper ↗ ·

  13. Morphological and Kinetic Studies on Hexagonal Tungstates

    Chemistry of Materials · 2006-12-20

    Alexej Michailovski, Ragnar Kiebach, Wolfgang Bensch, Jan‐Dierk Grunwaldt, Alfons Baiker, Sridhar Komarneni, Greta Ricarda Patzke

    Read original paper ↗ ·

  14. Targeted Synthesis of Nanostructured Oxide Materials

    MRS Proceedings · 2007-01-01

    Greta Ricarda Patzke, Ying Zhou

    Read original paper ↗ ·

  15. Design of a high-temperature and high-pressure liquid flow cell for x-ray absorption fine structure measurements under catalytic reaction conditions

    Review of Scientific Instruments · 2008-01-01

    Toshihide Kawai, Wang‐Jae Chun, Kiyotaka Asakura, Yuichiro Koike, Masaharu Nomura, Kyoko Kitamura Bando, Shigeo Ted Oyama, Hitoshi Sumiya

    Read original paper ↗ ·

  16. Hydrothermal Formation of W/Mo-Oxides: A Multidisciplinary Study of Growth and Shape

    Chemistry of Materials · 2008-04-17

    Ragnar Kiebach, Nicole Pienack, Wolfgang Bensch, Jan‐Dierk Grunwaldt, Alexej Michailovski, Alfons Baiker, Thomas Fox, Ying Zhou, Greta Ricarda Patzke

    Read original paper ↗ ·

  17. In situ XAS study of the Mn(III)(salen)Br catalyzed synthesis of cyclic organic carbonates from epoxides and CO2

    Journal of Molecular Catalysis A Chemical · 2008-10-16

    Fabian Jutz, Jan‐Dierk Grunwaldt, Alfons Baiker

    Read original paper ↗ ·

  18. Transition metal phosphide hydroprocessing catalysts: A review

    Catalysis Today · 2008-11-07

    Shigeo Ted Oyama, Travis Gott, Haiyan Y. Zhao, Yong-Kul Lee

    Read original paper ↗ ·

  19. Gold-catalyzed aerobic oxidation of dibenzylamine: Homogeneous or heterogeneous catalysis?

    Journal of Molecular Catalysis A Chemical · 2008-11-13

    Linda Aschwanden, Tamás Mallát, Jan‐Dierk Grunwaldt, Frank Krumeich, Alfons Baiker

    Read original paper ↗ ·

  20. Chapter 6 Characterization of Catalysts in Reactive Atmospheres by X‐ray Absorption Spectroscopy

    Advances in catalysis · 2009-01-01

    Simon R. Bare, Thorsten Ressler

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  21. Time Resolved IR and X-Ray Simultaneous Spectroscopy: New Opportunities for the Analysis of Fast Chemical-Physical Phenomena in Materials Science

    Acta Physica Polonica A · 2009-02-01

    A. Marcelli, D. Hampai, Wei Xu, Luca Malfatti, Plinio Innocenzi

    Read original paper ↗ ·

  22. New agitated and thermostatized cell forin situmonitoring of fast reactions by synchrotron SAXS

    Journal of Synchrotron Radiation · 2009-09-24

    Marı́a Paulis, Audrey Bonnefond, Matej Mičušík, José R. Leiza

    Read original paper ↗ ·

  23. In situobservation of Ni–Mo–S phase formed on NiMo/Al2O3catalyst sulfided at high pressure by means of Ni and MoK-edge EXAFS spectroscopy

    Journal of Synchrotron Radiation · 2010-03-18

    Naoto Koizumi, Yusuke Hamabe, Sungbong Jung, Yasuhiro Suzuki, Shohei Yoshida, Muneyoshi Yamada

    Read original paper ↗ ·

  24. High‐pressure Methods and Equipment

    Unknown journal · 2010-06-28

    Nils Theyssen, Katherine Scovell, Martyn Poliakoff

    Read original paper ↗ ·

  25. Asymmetric CC Bond‐Formation Reaction with Pd: How to Favor Heterogeneous or Homogeneous Catalysis?

    Chemistry - A European Journal · 2010-07-21

    Sven Reimann, Jan‐Dierk Grunwaldt, Tamás Mallát, Alfons Baiker

    Read original paper ↗ ·

  26. In Situ X-ray Diffraction and Absorption Studies of the Growth and Phase Transformation of Yttrium Hydroxide Nanotubes to Their Oxide Counterparts

    The Journal of Physical Chemistry C · 2010-09-20

    James A. Dorman, Yuanbing Mao, John Bargar, Jane P. Chang

    Read original paper ↗ ·

  27. Hydrothermal and Solvothermal Syntheses

    Elsevier eBooks · 2010-11-12

    Shouhua Feng, Li Guanghua

    Read original paper ↗ ·

  28. Interplay Between Size and Crystal Structure of Molybdenum Dioxide Nanoparticles—Synthesis, Growth Mechanism, and Electrochemical Performance

    Small · 2010-12-20

    Dorota Koziej, Marta D. Rossell, Bettina Ludi, Andreas Hintennach, Petr Novák, Jan‐Dierk Grunwaldt, Markus Niederberger

    Read original paper ↗ ·

  29. A large-volume gas cell for high-energy X-ray reflectivity investigations of interfaces under pressure

    Journal of Synchrotron Radiation · 2011-01-25

    Federica Venturini, Sebastian Schöder, W. F. Kuhs, V. Honkimäki, L Mélési, H. Reichert, H. Schober, Frédéric Thomas

    Read original paper ↗ ·

  30. Identification of the Active Species Generated from Supported Pd Catalysts in Heck Reactions: An in situ Quick Scanning EXAFS Investigation

    Journal of the American Chemical Society · 2011-02-23

    Sven Reimann, Jan Stötzel, R. Frahm, Wolfgang Kleist, Jan‐Dierk Grunwaldt, Alfons Baiker

    Read original paper ↗ ·

  31. A flow-through reaction cell forin situX-ray diffraction and absorption studies of heterogeneous powder–liquid reactions and phase transformations

    Journal of Synchrotron Radiation · 2011-11-14

    Pilar Ferrer, Iván da Silva, Juan Rubio‐Zuazo, Belén F. Alfonso, Camino Trobajo, Sergei A. Khainakov, José R. Garcı́a, Santiago García‐Granda, German Rafael Castro

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  32. In Situ X‐ray Absorption Spectroscopy/Energy‐Dispersive X‐ray Diffraction Studies on the Hydrothermal Formation of Bi2W1–xMoxO6 Nanomaterials

    European Journal of Inorganic Chemistry · 2012-01-03

    Ying Zhou, Е. А. Антонова, Yuanhua Lin, Jan‐Dierk Grunwaldt, Wolfgang Bensch, Greta Ricarda Patzke

    Read original paper ↗ ·

  33. Study of the Chemical Mechanism Involved in the Formation of Tungstite in Benzyl Alcohol by the Advanced QEXAFS Technique

    Chemistry - A European Journal · 2012-01-16

    Inga Olliges‐Stadler, Jan Stötzel, Dorota Koziej, Marta D. Rossell, Jan‐Dierk Grunwaldt, Maarten Nachtegaal, R. Frahm, Markus Niederberger

    Read original paper ↗ ·

  34. A portable powder-liquid high corrosion-resistant reaction cell for in situ X-ray diffraction and absorption studies of heterogeneous powder-liquid reactions and phase transformations

    Journal of Physics Conference Series · 2013-03-22

    Pilar Ferrer, Iván da Silva, Catherine Heyman, Juan Rubio‐Zuazo, German Rafael Castro

    Read original paper ↗ ·

  35. QEXAFS in Catalysis Research: Principles, Data Analysis, and Applications

    Unknown journal · 2013-06-10

    Anatoly I. Frenkel, Syed Khalid, Jonathan C. Hanson, Maarten Nachtegaal

    Read original paper ↗ ·

  36. In Situ Studies of Solvothermal Synthesis of Energy Materials

    ChemSusChem · 2014-03-05

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

    Read original paper ↗ ·

  37. Puzzling Mechanism behind a Simple Synthesis of Cobalt and Cobalt Oxide Nanoparticles: In Situ Synchrotron X-ray Absorption and Diffraction Studies

    Chemistry of Materials · 2014-03-11

    Malwina Staniuk, Ofer Hirsch, Niklaus Kränzlin, Rahel Böhlen, Wouter van Beek, Paula M. Abdala, Dorota Koziej

    Read original paper ↗ ·

  38. Aliovalent Ni in MoO2Lattice— Probing the Structure and Valence of Ni and Its Implication on the Electrochemical Performance

    Chemistry of Materials · 2014-07-16

    Ofer Hirsch, Guobo Zeng, Li Jun Luo, Malwina Staniuk, Paula M. Abdala, Wouter van Beek, Felix Rechberger, Martin Süess, Markus Niederberger, Dorota Koziej

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  39. X-Ray Absorption Fine Structure Analysis of Catalytic Nanomaterials

    Springer eBooks · 2015-12-04

    Wang‐Jae Chun, Satoru Takakusagi, Yohei Uemura, Kyoko Kitamura Bando, Kiyotaka Asakura

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  40. Revealing Complexity of Nanoparticle Synthesis in Solution by in Situ Hard X-ray Spectroscopy─Today and Beyond

    Chemistry of Materials · 2016-04-08

    Dorota Koziej

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  41. Cell Designs for In Situ and Operando Studies

    Springer eBooks · 2016-10-19

    Dmitry E. Doronkin, Henning Lichtenberg, Jan‐Dierk Grunwaldt

    Read original paper ↗ ·

  42. Metal Nanocatalysts

    Springer eBooks · 2016-10-19

    Yuanyuan Li, Anatoly I. Frenkel

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  43. Hydrothermal and Solvothermal Syntheses

    Elsevier eBooks · 2017-01-01

    Shouhua Feng, G.-H. Li

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  44. Mechanistic Aspects in the Formation, Growth and Surface Functionalization of Metal Oxide Nanoparticles in Organic Solvents

    Chemistry - A European Journal · 2017-04-05

    Rupali Deshmukh, Markus Niederberger

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  45. A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions

    Review of Scientific Instruments · 2017-10-01

    Niclas Heidenreich, U. Rütt, Milan Köppen, A. Ken Inge, S. Beier, Ann‐Christin Dippel, Ralf Suren, Norbert Stock

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  46. CAT-ACT—A new highly versatile x-ray spectroscopy beamline for catalysis and radionuclide science at the KIT synchrotron light facility ANKA

    Review of Scientific Instruments · 2017-11-01

    Anna Zimina, Kathy Dardenne, Melissa A. Denecke, Dmitry E. Doronkin, E. Huttel, Henning Lichtenberg, S. Mangold, T. Prüßmann, Jörg Rothe, T. Spangenberg, Ralph Steininger, Tonya Vitova, Hörst Geckeis, Jan‐Dierk Grunwaldt

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  47. On the mechanism of rapid metal exchange between thiolate-protected gold and gold/silver clusters: a time-resolved in situ XAFS study

    Physical Chemistry Chemical Physics · 2018-01-01

    Bei Zhang, Оlga V. Safonova, Stephan Pollitt, Giovanni Salassa, Annelies Sels, Rania Kazan, Yuming Wang, Günther Rupprechter, Noelia Barrabés, Thomas Bürgi

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  48. Measurements inside a reactor of spatial and temporal profiles on liquid and solid phases through spectroscopic analysis

    Unknown journal · 2018-07-17

    Marisa De Sousa Duarte

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  49. A versatile liquid-jet/sessile droplet system for operando studies of reactions in liquid dispersions and solutions by X-ray absorption spectroscopy

    Reaction Chemistry & Engineering · 2019-01-01

    Sin-Yuen Chang, Thokozile A. Kathyola, Elizabeth A. Willneff, Colin J. Willis, P. Wilson, Peter John Dowding, Giannantonio Cibin, Anna Kroner, Elizabeth J. Shotton, Sven L. M. Schroeder

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  50. In situ XAS study of the local structure and oxidation state evolution of palladium in a reduced graphene oxide supported Pd( ii ) carbene complex during an undirected C–H acetoxylation reaction

    Catalysis Science & Technology · 2019-01-01

    Ning Yuan, Maitham H. Majeed, Éva G. Bajnóczi, Axel R. Persson, Reine Wallenberg, A. Ken Inge, Niclas Heidenreich, Norbert Stock, Xiaodong Zou, Ola F. Wendt, Ingmar Persson

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