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RESEARCH PAPER · Journal of the American Chemical Society · 2007

Assembly of a Homochiral, Body-Centered Cubic Network Composed of Vertex-Shared Mg12 Cages: Use of Electrospray Ionization Mass Spectrometry to Monitor Metal Carboxylate Nucleation

J.A. Rood, Bill Boggess, Bruce C. Noll, Kenneth W. Henderson

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Assembly of a Homochiral, Body-Centered Cubic Network Composed of Vertex-Shared Mg12 Cages: Use of Electrospray Ionization Mass Spectrometry to Monitor Metal Carboxylate NucleationOriginalTwo chiral metal–organic frameworks showing unprecedented pcu-type topology based on the vertex-shared bowl-like MNa3 SBUs11Manipulation of molecular aggregation and supramolecular structure using self-assembled lithium mixed-anion complexes17The Designed Assembly of Augmented Diamond Networks From Predetermined Pentanuclear Tetrahedral Units129The Designed Assembly of Augmented Diamond Networks From Predetermined Pentanuclear Tetrahedral Units21Base‐Induced Formation of Two Magnesium Metal‐Organic Framework Compounds with a Bifunctional Tetratopic Ligand345Temperature- and Stoichiometry-Controlled Dimensionality in a Magnesium 4,5-Imidazoledicarboxylate System with Strong Hydrophilic Pore Surfaces116The Use of Halide‐Substituted Anilines for the Formation of Magnesium Imides15Crystal Growth of the Nanoporous Metal–Organic Framework HKUST‐1 Revealed by In Situ Atomic Force Microscopy180Crystal Growth of the Nanoporous Metal–Organic Framework HKUST‐1 Revealed by In Situ Atomic Force Microscopy45Controlling the dimensionalities and structures of homochiral Zn( ii ) and Cd( ii ) compounds of N-(p-tosyl)-S-carboxymethyl- l -cysteinevia tuning the connecting modes of metal ions and chiral linkers by different kinds of ancillary ligands45How Does Your MOF Grow?56Bulk homochirality of a 3-D inorganic framework: ligand control of inorganic network chirality27Microwave synthesis and single-crystal-to-single-crystal transformation of magnesium coordination polymers exhibiting selective gas adsorption and luminescence properties65Thin films of metal–organic frameworks893Self-Assembly of Metal−Organic Coordination Polymers Constructed from a Versatile Multipyridyl Ligand: Diversity of Coordination Modes and Structures131Alteration of Molecular Conformations, Coordination Modes, and Architectures for a Novel 3,8-Diimidazol-1,10-phenanthroline Compound in the Construction of Cadmium(II) and Zinc(II) Homochiral Coordination Polymers Involving an Auxiliary Chiral Camphorate Ligand74A Porous Polyhedral Metal-Organic Framework Based on Zn2(COO)3 and Zn2(COO)4 SBUs55A new eight-connected net with CsCl-type topology built on unique [Co2(μ3-OH)(μ2-OH2)(CO2)3]2 building blocks22A Three-Dimensional Porous Metal−Organic Framework with a Body-Centered Cubic Topology Constructed from 48-Membered Tetraicosanuclear Metallamacrocycle Based on in Situ Ligand Synthesis13Growth Mechanism of Metal–Organic Frameworks: Insights into the Nucleation by Employing a Step‐by‐Step Route399Wachstumsmechanismen Metall‐organischer Gerüststrukturen: Einblicke in die Keimbildung anhand einer schrittweisen Methodik48Variable Lithium Coordination Modes in Two- and Three-Dimensional Lithium Boron Imidazolate Frameworks52Isolated Co15 Clusters and Their Assembly into a 3D Network: Conformation-Directed Synthesis26A homochiral metal-organic framework with amino-functionalized pores20Metal−Organic Coordination Polymers Generated from Chiral Camphoric Acid and Flexible Ligands with Different Spacer Lengths: Syntheses, Structures, and Properties68Crystallographic Evidence for Ionic Molecular Building Blocks in the Assembly of a Two-Dimensional Metal−Organic Framework11Metal‐Containing Polymers: Building Blocks for Functional (Nano)Materials116Homochiral frameworks derived from magnesium, zinc and copper salts of l-tartaric acid37Two Thermostable Three-Dimensional Homochiral Metal−Organic Polymers with Quartz Topology79Factors Dictating the Nuclearity/Aggregation and Acetate Coordination Modes of Lutidine-Coordinated Zinc(II) Acetate Complexes70Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks220Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks512D and 3D lanthanide coordination polymers constructed from benzimidazole-5,6-dicarboxylic acid and sulfate bridged secondary building units75Chiral or achiral camphorate-based complexes controlled by the conformational rigidity of N-donor co-ligands34Hydro(solvo)thermal synthesis of homochiral metal–camphorate coordination polymers13Porous lanthanide oxides via a precursor method: Morphology control through competitive interaction of lanthanide cations with oxalate anions and amino acids5Selective CO2 and H2 adsorption in a chiral magnesium-based metal organic framework (Mg-MOF) with open metal sites151New Metal−Organic Framework with Uninodal 4-Connected Topology Displaying Interpenetration, Self-Catenation, and Second-Order Nonlinear Optical Response75Syntheses, Structures, and Physical Properties of Camphorate Coordination Polymers Controlled by Semirigid Auxiliary Ligands with Variable Coordination Positions and Conformations59Supramolecular Isomerism in Honeycomb Metal−Organic Frameworks Driven by CH···π Interactions: Homochiral Crystallization from an Achiral Ligand through Chiral Inducement88A Method for the Preparation of Highly Porous, Nanosized Crystals of Isoreticular Metal−Organic Frameworks115Facile route for synthesis and controlled growth of SURMOFs on functionalized organic surfaces0Oberflächenchemie Metall‐organischer Gerüste an der Flüssig‐fest‐Grenzfläche43Surface Chemistry of Metal–Organic Frameworks at the Liquid–Solid Interface318Homochiral transition-metal camphorate coordination architectures containing “piperazine–pyridine” ligands26Structural variability of Co(ii) and Ni(ii) entangled metal–organic frameworks: effect of N-donor ligands and metal ions53Structure, adsorption and magnetic properties of chiral metal–organic frameworks bearing linear trinuclear secondary building blocks48Three 2D AgI-framework isomers with helical structures controlled by the chirality of camphor-10-sulfonic acid11Three new two-dimensional metal-organic coordination polymers derived from bis(pyridinecarboxamide)-1,4-benzene ligands and 1,3-benzenedicarboxylate: Syntheses and electrochemical property57Investigation of Reaction Mechanism of Amino Acids and Phosphorus Trichloride by 31 P NMR and ESI-MS/MS2A novel 2D (3,5)-connected coordination framework with Zn2(COO)3 SBU7Fast Nucleation and Growth of ZIF‐8 Nanocrystals Monitored by Time‐Resolved In Situ Small‐Angle and Wide‐Angle X‐Ray Scattering263Fast Nucleation and Growth of ZIF‐8 Nanocrystals Monitored by Time‐Resolved In Situ Small‐Angle and Wide‐Angle X‐Ray Scattering57Revelation of the Molecular Assembly of the Nanoporous Metal Organic Framework ZIF-8175Recent Advances in s-Block Metal Carboxylate Networks222Synthesis, Structures, and Adsorption Properties of Two New LaIII–MgII Heterometallic Polymers13Layer-by-layer evolution and a hysteretic single-crystal to single-crystal transformation cycle of a flexible pillared-layer open framework54Synthesis of Metal-Organic Frameworks (MOFs): Routes to Various MOF Topologies, Morphologies, and Composites5045Crystal growth of nanoporous metal organic frameworks47A porous metal–organic framework (MOF) with unusual 2D→3D polycatenation based on honeycomb layers602D lanthanide–organic frameworks constructed from lanthanide acetate skeletons and benzotriazole-5-carboxylic acid connectors: synthesis, structure, luminescence and magnetic properties24Hydrophobic-exterior layer structures and magnetic properties of trinuclear copper complexes with chiral amino alcoholate ligands42Two chiral Zn(ii) metal–organic frameworks with dinuclear Zn2(COO)3 secondary building units: a 2-D (6,3) net and a 3-D 3-fold interpenetrating (3,5)-connected network15Vertex-directed self-assembly of a high symmetry supermolecular building block using a custom-designed porphyrin98In Situ NMR, Ex Situ XRD and SEM Study of the Hydrothermal Crystallization of Nanoporous Aluminum Trimesates MIL-96, MIL-100, and MIL-110131Synthesis, Structure, and Properties of a Chiral Zinc(II) Metal-Organic Framework Featuring Linear Trinuclear Secondary Building Blocks7Comparative Study of Activation Methods on Tuning Gas Sorption Properties of a Metal–Organic Framework with Nanosized Ligands60Crystal Growth Mechanisms and Morphological Control of the Prototypical Metal–Organic Framework MOF‐5 Revealed by Atomic Force Microscopy89Spectroscopic Evidence for the Structure Directing Role of the Solvent in the Synthesis of Two Iron Carboxylates31Spectroscopic Evidence for the Structure Directing Role of the Solvent in the Synthesis of Two Iron Carboxylates3Construction of metal–organic coordination polymers derived from 4-substituted tetrazole–benzoate ligands: synthesis, structure, luminescence, and magnetic behaviors40A supramoleculear self-assembled flexible open framework based on the coordination of honeycomb layers possessing octahedral and tetrahedral CoII geometries2An unprecedented acylamide-functionalized 2D → 3D microporous metal–organic polycatenation framework exhibiting highly selective CO2 capture34Sonochemical Syntheses of a One‐Dimensional Mg(II) Metal‐Organic Framework: A New Precursor for Preparation of MgO One‐Dimensional Nanostructure21Two new series of rare-earth organic frameworks involving two structural architectures: syntheses, structures and magnetic properties26Two Enantiomorphic MgII/Carboxylate Coordination Polymers Produced from Spontaneous Resolution with an Achiral Bipyridyl Dicarboxylate Ligand18Lanthanide coordination polymers based on Ln2 cluster: Syntheses, crystal structures photoluminescence and magnetic properties6Mn 8 @Na 8 Cube-in-Cube SBBs-Based Heterometallic Coordination Network with Unprecedented (3 9 .4 6 ) 8 Topological Mn 8 (μ 4 -OMe) 6 Cubes3Three new homochiral coordination polymers involving two three-dimensional structural architectures: Syntheses, structures and magnetic properties8Liquid phase stepwise growth of surface mounted metal–organic frameworks for exploratory research and development of applications59A magnesium-carboxylate framework showing luminescent sensing for CS2 and nitroaromatic compounds26A set of alkali and alkaline-earth coordination polymers based on the ligand 2-(1H-benzotriazol-1-yl) acetic acid: Effects the radius of metal ions on structures and properties20Solvent-assisted construction of diverse Mg-TDC coordination polymers20Phase Formation Study of Ca-Terephthalate MOF-Type Materials323D lanthanide metal–organic frameworks constructed from lanthanide formate skeletons and 3,5-bis(4′-carboxy-phenyl)-1,2,4-triazole connectors: synthesis, structure and luminescence11An ionothermally synthesized Mg-based coordination polymer as a precursor for preparing porous carbons18An organic–inorganic hybrid photocatalyst based on sandwich-type tetra-Co-substituted phosphotungstates with high visible light photocatalytic activity20MOF crystal growth: UV resonance Raman investigation of metal–ligand binding in solution and accelerated crystal growth methods16Insights into the Molecular Assembly of Zeolitic Imidazolate Frameworks by ESI-MS70Assembly, Structures, and Properties of a Series of Metal‐Organic Coordination Polymers Derived from a Semi‐rigid Bis‐pyridyl‐bis‐amide Ligand3Chiral chemistry of metal–camphorate frameworks268Hierarchical Assembly of a {Mn II 15 Mn III 4 } Brucite Disc: Step-by-Step Formation and Ferrimagnetism191Advancing Magnesium–Organic Porous Materials through New Magnesium Cluster Chemistry41Determination of the Preassembled Nucleating Units That Are Critical for the Crystal Growth of the Metal–Organic Framework CdIF‐422Determination of the Preassembled Nucleating Units That Are Critical for the Crystal Growth of the Metal–Organic Framework CdIF‐47In SituStudies of the Crystallization of Metal-Organic Frameworks10A Highly Water‐Tolerant Magnesium(II) Coordination Polymer Derived from a Flexible Layered Structure6Chirality in Network Solids1Tuning the luminescence of two 3d–4f metal–organic frameworks for the fast response and highly selective detection of aniline72In-situ IR monitoring of the formation of Zr-fumarate MOF33Molecular simulations of self-assembly processes in metal-organic frameworks: Model dependence18Structural Diversification of Light‐Metal Coordination Polymers Using 4‐(Methylsulfonyl)benzoate with a Charge‐Polarized Neutral Methylsulfonyl Coordination Moiety2Growth of Metal Organic Frameworks (MOFs) layers on functionalized surfaces0A kinetic study of facile fabrication of MIL-101(Cr) metal-organic framework: Effect of synthetic method20Early stage structural development of prototypical zeolitic imidazolate framework (ZIF) in solution77In Situ, Time-Resolved, and Mechanistic Studies of Metal–Organic Framework Nucleation and Growth610Morphology control in modulated synthesis of metal-organic framework CPO-2737Structural Characterization of Molybdenum Oxide Nanoclusters Using Ion Mobility Spectrometry–Mass Spectrometry and Infrared Action Spectroscopy24A Solvent-Stable Zinc(II)–Gadolinium(III) Metal–Organic Framework Assembled with Furan-2,5-Dicarboxylic Acid: Synthesis, Crystal Structure and Magnetic Property7Electrospray Mass Spectrometry Investigation into the Formation of CPO-2712Applications and advances in coordination cages: Metal-Organic Frameworks27Difference in the Formation of Two Structural Types of V-Shaped MII3 Clusters: Diffraction, Mass Spectrometry, and Magnetism9Understanding Time Dependence on Zinc Metal–Organic Framework Growth Using in Situ Liquid Secondary Ion Mass Spectrometry15Machine-Learning-Guided Morphology Engineering of Nanoscale Metal-Organic Frameworks83Synthetic strategies towards chiral coordination polymers72The Structures of Metal–Organic Frameworks1The Structures of Metal–Organic Frameworks1The Structures of Metal–Organic Frameworks3Uncovering growth species of multivariate MOFs in liquid phase by mass spectrometry6Elucidation of the pre-nucleation phase directing metal-organic framework formation50Understanding and controlling the nucleation and growth of metal–organic frameworks186Synthetic and analytical considerations for the preparation of amorphous metal–organic frameworks41Non-classical crystallization in soft and organic materials107Light metal coordination polymers0Hierarchical assembly of a Ti24 metal-organic polyhedron via kinetic trapping of intermediates2Simulating the Self-Assembly of MOF-5 Using Reactive Force Field (ReaxFF)1Site-selective valence isomerism as a unified electronic trigger for magnetism, chirality, and catalysis in Ni–carboxylate MOFs1

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  1. Two chiral metal–organic frameworks showing unprecedented pcu-type topology based on the vertex-shared bowl-like MNa3 SBUs

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  2. Manipulation of molecular aggregation and supramolecular structure using self-assembled lithium mixed-anion complexes

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  3. The Designed Assembly of Augmented Diamond Networks From Predetermined Pentanuclear Tetrahedral Units

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  4. The Designed Assembly of Augmented Diamond Networks From Predetermined Pentanuclear Tetrahedral Units

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  5. Base‐Induced Formation of Two Magnesium Metal‐Organic Framework Compounds with a Bifunctional Tetratopic Ligand

    European Journal of Inorganic Chemistry · 2008-07-05

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  6. Temperature- and Stoichiometry-Controlled Dimensionality in a Magnesium 4,5-Imidazoledicarboxylate System with Strong Hydrophilic Pore Surfaces

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  7. The Use of Halide‐Substituted Anilines for the Formation of Magnesium Imides

    European Journal of Inorganic Chemistry · 2008-07-25

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  8. Crystal Growth of the Nanoporous Metal–Organic Framework HKUST‐1 Revealed by In Situ Atomic Force Microscopy

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  9. Crystal Growth of the Nanoporous Metal–Organic Framework HKUST‐1 Revealed by In Situ Atomic Force Microscopy

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  10. Controlling the dimensionalities and structures of homochiral Zn( ii ) and Cd( ii ) compounds of N-(p-tosyl)-S-carboxymethyl- l -cysteinevia tuning the connecting modes of metal ions and chiral linkers by different kinds of ancillary ligands

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  11. How Does Your MOF Grow?

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  12. Bulk homochirality of a 3-D inorganic framework: ligand control of inorganic network chirality

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  13. Microwave synthesis and single-crystal-to-single-crystal transformation of magnesium coordination polymers exhibiting selective gas adsorption and luminescence properties

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  14. Thin films of metal–organic frameworks

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  15. Self-Assembly of Metal−Organic Coordination Polymers Constructed from a Versatile Multipyridyl Ligand: Diversity of Coordination Modes and Structures

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  16. Alteration of Molecular Conformations, Coordination Modes, and Architectures for a Novel 3,8-Diimidazol-1,10-phenanthroline Compound in the Construction of Cadmium(II) and Zinc(II) Homochiral Coordination Polymers Involving an Auxiliary Chiral Camphorate Ligand

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  17. A Porous Polyhedral Metal-Organic Framework Based on Zn2(COO)3 and Zn2(COO)4 SBUs

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  18. A new eight-connected net with CsCl-type topology built on unique [Co2(μ3-OH)(μ2-OH2)(CO2)3]2 building blocks

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  19. A Three-Dimensional Porous Metal−Organic Framework with a Body-Centered Cubic Topology Constructed from 48-Membered Tetraicosanuclear Metallamacrocycle Based on in Situ Ligand Synthesis

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  20. Growth Mechanism of Metal–Organic Frameworks: Insights into the Nucleation by Employing a Step‐by‐Step Route

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  21. Wachstumsmechanismen Metall‐organischer Gerüststrukturen: Einblicke in die Keimbildung anhand einer schrittweisen Methodik

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  22. Variable Lithium Coordination Modes in Two- and Three-Dimensional Lithium Boron Imidazolate Frameworks

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  23. Isolated Co15 Clusters and Their Assembly into a 3D Network: Conformation-Directed Synthesis

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  24. A homochiral metal-organic framework with amino-functionalized pores

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  25. Metal−Organic Coordination Polymers Generated from Chiral Camphoric Acid and Flexible Ligands with Different Spacer Lengths: Syntheses, Structures, and Properties

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  26. Crystallographic Evidence for Ionic Molecular Building Blocks in the Assembly of a Two-Dimensional Metal−Organic Framework

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  27. Metal‐Containing Polymers: Building Blocks for Functional (Nano)Materials

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  28. Homochiral frameworks derived from magnesium, zinc and copper salts of l-tartaric acid

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  29. Two Thermostable Three-Dimensional Homochiral Metal−Organic Polymers with Quartz Topology

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  30. Factors Dictating the Nuclearity/Aggregation and Acetate Coordination Modes of Lutidine-Coordinated Zinc(II) Acetate Complexes

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  31. Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks

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  32. Time‐Resolved In Situ Diffraction Study of the Solvothermal Crystallization of Some Prototypical Metal–Organic Frameworks

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  33. 2D and 3D lanthanide coordination polymers constructed from benzimidazole-5,6-dicarboxylic acid and sulfate bridged secondary building units

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  34. Chiral or achiral camphorate-based complexes controlled by the conformational rigidity of N-donor co-ligands

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  35. Hydro(solvo)thermal synthesis of homochiral metal–camphorate coordination polymers

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  36. Porous lanthanide oxides via a precursor method: Morphology control through competitive interaction of lanthanide cations with oxalate anions and amino acids

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  37. Selective CO2 and H2 adsorption in a chiral magnesium-based metal organic framework (Mg-MOF) with open metal sites

    Journal of Materials Chemistry · 2010-01-01

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  38. New Metal−Organic Framework with Uninodal 4-Connected Topology Displaying Interpenetration, Self-Catenation, and Second-Order Nonlinear Optical Response

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  39. Syntheses, Structures, and Physical Properties of Camphorate Coordination Polymers Controlled by Semirigid Auxiliary Ligands with Variable Coordination Positions and Conformations

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  40. Supramolecular Isomerism in Honeycomb Metal−Organic Frameworks Driven by CH···π Interactions: Homochiral Crystallization from an Achiral Ligand through Chiral Inducement

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  41. A Method for the Preparation of Highly Porous, Nanosized Crystals of Isoreticular Metal−Organic Frameworks

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  42. Facile route for synthesis and controlled growth of SURMOFs on functionalized organic surfaces

    University Library BOCHUM (Ruhr University Bochum) · 2010-12-17

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  43. Oberflächenchemie Metall‐organischer Gerüste an der Flüssig‐fest‐Grenzfläche

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  44. Surface Chemistry of Metal–Organic Frameworks at the Liquid–Solid Interface

    Angewandte Chemie International Edition · 2010-12-28

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  45. Homochiral transition-metal camphorate coordination architectures containing “piperazine–pyridine” ligands

    CrystEngComm · 2011-01-01

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  46. Structural variability of Co(ii) and Ni(ii) entangled metal–organic frameworks: effect of N-donor ligands and metal ions

    CrystEngComm · 2011-01-01

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  47. Structure, adsorption and magnetic properties of chiral metal–organic frameworks bearing linear trinuclear secondary building blocks

    Dalton Transactions · 2011-01-01

    Zilu Chen, Xianlin Liu, Chuanbing Zhang, Zhong Zhang, Fupei Liang

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  48. Three 2D AgI-framework isomers with helical structures controlled by the chirality of camphor-10-sulfonic acid

    Dalton Transactions · 2011-01-01

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  49. Three new two-dimensional metal-organic coordination polymers derived from bis(pyridinecarboxamide)-1,4-benzene ligands and 1,3-benzenedicarboxylate: Syntheses and electrochemical property

    Journal of Organometallic Chemistry · 2011-01-05

    Xiuli Wang, Bao Mu, Hong‐Yan Lin, Guo‐Cheng Liu

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  50. Investigation of Reaction Mechanism of Amino Acids and Phosphorus Trichloride by 31 P NMR and ESI-MS/MS

    Chinese Journal of Chemistry · 2011-06-01

    Yanchun Cao, Shuxia Cao, Yali Xie, Xiang-Kun Zong, Yufen Zhao

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