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RESEARCH PAPER · ChemSusChem · 2014

In Situ Studies of Solvothermal Synthesis of Energy Materials

Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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In Situ Studies of Solvothermal Synthesis of Energy MaterialsOriginalSupercritical fluid methods for synthesizing cathode materials towards lithium ion battery applications30Controlling Allotropism in Ruthenium Nanoparticles: A Pulsed-Flow Supercritical Synthesis and in Situ Synchrotron X-ray Diffraction Study41In situ powder X-ray diffraction study of the hydro-thermal formation of LiMn 2 O 4 nanocrystallites10Characterization of Gas‐Solid Reactions using In Situ Powder X‐ray Diffraction38Mechanisms for Iron Oxide Formation under Hydrothermal Conditions: An in Situ Total Scattering Study92Morphology-controlled growth of special nanostructure CuInS2 thin films on an FTO substrate and their application in thin film solar cells18In situ powder X-ray diffraction study of magnetic CoFe 2 O 4 nanocrystallite synthesis57In situ total X-ray scattering study of the formation mechanism and structural defects in anatase TiO 2 nanoparticles under hydrothermal conditions59Matching the organic and inorganic counterparts during nucleation and growth of copper-based nanoparticles – in situ spectroscopic studies39Synthesis and formation mechanism of VO 2 (A) nanoplates with intrinsic peroxidase-like activity49The formation mechanism of bimetallic PtRu alloy nanoparticles in solvothermal synthesis31Porous Co3O4/CuO Composite Assembled from Nanosheets as High‐Performance Anodes for Lithium‐Ion Batteries49Beamline P02.1 at PETRA III for high-resolution and high-energy powder diffraction289Solvothermal Growth of Bismuth Chalcogenide Nanoplatelets by the Oriented Attachment Mechanism: An in Situ PXRD Study56Formation Mechanisms of Pt and Pt3Gd Nanoparticles under Solvothermal Conditions: An in Situ Total X-ray Scattering Study40Hydrothermal Synthesis and in Situ Powder X-ray Diffraction Study of Bismuth-Substituted Ceria Nanoparticles28In Situ X-Ray Diffraction Measurement Method for Investigating the Oxides Films on Austenitic Stainless Steel in Simulated Pressurized Water Reactor Primary Water4In situ X-ray diffraction environments for high-pressure reactions72Controlling the crystallisation of oxide materials by solvothermal chemistry: tuning composition, substitution and morphology of functional solids34Crystal structure, microstructure and electrochemical properties of hydrothermally synthesised LiMn 2 O 414The chemistry of nucleation119Unraveling structural and magnetic information during growth of nanocrystalline SrFe 12 O 1936Hydrothermal Synthesis of CoSb2O4: In Situ Powder X-ray Diffraction, Crystal Structure, and Electrochemical Properties29Unraveling the Hydrogenation of TiO2 and Graphene Oxide/TiO2 Composites in Real Time by in Situ Synchrotron X-ray Powder Diffraction and Pair Distribution Function Analysis21Hydrothermal Synthesis of TiO2@SnO2 Hybrid Nanoparticles in a Continuous‐Flow Dual‐Stage Reactor10Guide to by-products formed in organic solvents under solvothermal conditions44Synthesis of indium tin oxide (ITO) nanoparticles in supercritical methanol21Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction53Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction14Revealing Complexity of Nanoparticle Synthesis in Solution by in Situ Hard X-ray Spectroscopy─Today and Beyond52Morphology-dependent electrochemistry of FeOOH nanostructures51In SituStudies of the Crystallization of Metal-Organic Frameworks10Versatile, Fast, and Easy One‐Step Method for the Synthesis of Hydrophilic Lanthanide‐Doped Nanoparticles6The ZIF system zinc(II) 4,5-dichoroimidazolate: theoretical and experimental investigations of the polymorphism and crystallization mechanisms7Nucleation and Crystal Growth of a {V14Sb8O42} Cluster from a {V15Sb6O42} Polyoxovanadate: In Situ XRD Studies28Towards atomistic understanding of polymorphism in the solvothermal synthesis of ZrO2nanoparticles52Interlayer-expanded MoS 2381Formation pathways of metal–organic frameworks proceeding through partial dissolution of the metastable phase27Hydrothermal and Solvothermal Syntheses239In situ neutron diffraction study of the formation of Ho 2 Ge 2 O 7 pyrochlore at high temperature and pressure13Structural variety in ytterbium dicarboxylate frameworks and in situ study diffraction of their solvothermal crystallisation14Mechanistic Aspects in the Formation, Growth and Surface Functionalization of Metal Oxide Nanoparticles in Organic Solvents125Quantitative 3D evolution of colloidal nanoparticle oxidation in solution150High energy X-rays for following metal-organic framework formation: Identifying intermediates in interpenetrated MOF-5 crystallisation26Insight into Nucleation and Growth of Bi2–xSbxTe3 (x = 0–2) Nanoplatelets in Hydrothermal Synthesis11Time-Resolved Powder X-ray Diffraction of the Solvothermal Crystallization of Cobalt Gallate Spinel Photocatalyst Reveals Transient Layered Double Hydroxides20Continuous Hydrothermal Synthesis of Inorganic Nanoparticles: Applications and Future Directions614In situ monitoring metal-ligand exchange processes by optical spectroscopy and X-ray diffraction analysis: a review22Synchrotron X-ray Analytical Techniques for Studying Materials Electrochemistry in Rechargeable Batteries582Understanding the polychalcogenides as building blocks to solid state materials: Speciation of polychalcogenides in solutions10Combinatorial appraisal of transition states for in situ pair distribution function analysis19Formation of a new type of uranium( iv ) poly-oxo cluster {U 38 } based on a controlled release of water via esterification reaction44Kinetics during hydrothermal synthesis of nanosized K x Na 1−x NbO 316Formation Mechanisms of Nanocrystalline MnO 2 Polymorphs under Hydrothermal Conditions78In Situ, Time-Resolved, and Mechanistic Studies of Metal–Organic Framework Nucleation and Growth610Pitfalls and reproducibility ofin situsynchrotron powder X-ray diffraction studies of solvothermal nanoparticle formation31Elucidation of the Formation Mechanism of Metal–Organic Frameworks via in-Situ Raman and FTIR Spectroscopy under Solvothermal Conditions81Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity20Facile Low Temperature Hydrothermal Synthesis of BaTiO3 Nanoparticles Studied by In Situ X-ray Diffraction21VO2(A) nanorods: One-pot synthesis, formation mechanism and thermal transformation to VO2(M)39Lepidocrocite-Type Titanate Formation from Isostructural Prestructures under Hydrothermal Reactions: Observation by Synchrotron X-ray Total Scattering Analyses51The 2019 materials by design roadmap322Alkali Counterions Impact Crystallization Kinetics of Apatite Nanocrystals from Amorphous Calcium Phosphate in Water at High pH18Hydrothermal reactor for in-situ synchrotron radiation powder diffraction at SPring-8 BL02B2 for quantitative design for nanoparticle10Control of Metal–Organic Framework Crystallization by Metastable Intermediate Pre‐equilibrium Species66Control of Metal–Organic Framework Crystallization by Metastable Intermediate Pre‐equilibrium Species4Introduction7Chemical Approaches to Carbon‐Based Metal‐Free Catalysts142Mechanisms for Tungsten Oxide Nanoparticle Formation in Solvothermal Synthesis: From Polyoxometalates to Crystalline Materials51Piloting melt synthesis and manufacturing processes to produce c‐lifepo4: preface5In Situ Synchrotron X‐ray Characterization Shining Light on the Nucleation and Growth Kinetics of Colloidal Nanoparticles53In Situ Synchrotron X‐ray Characterization Shining Light on the Nucleation and Growth Kinetics of Colloidal Nanoparticles4A kinetic and mechanistic study into the transformation of calcium sulfate hemihydrate to dihydrate40Laboratory setup for rapid in situ powder X-ray diffraction elucidating Ni particle formation in supercritical methanol10Quantitative Review of Olivine Carbonation Kinetics: Reactivity Trends, Mechanistic Insights, and Research Frontiers96Looking into the Black Box of Solid‐State Synthesis74From NaZn4Sb3 to HT-Na1–xZn4–ySb3: Panoramic Hydride Synthesis, Structural Diversity, and Thermoelectric Properties28Mapping the redox chemistry of common solvents in solvothermal synthesis through in situ X-ray diffraction22There's no place like real-space: elucidating size-dependent atomic structure of nanomaterials using pair distribution function analysis149Unraveling Structure and Dynamics in Porous Frameworks via Advanced In Situ Characterization Techniques134A Fast, Low‐Temperature Synthesis Method for Hexagonal YMnO3: Kinetics, Purity, Size and Shape as Studied by In Situ X‐ray Diffraction6In Situ Monitoring of Particle Formation with Spectroscopic and Analytical Techniques Under Solvothermal Conditions11Controllable preparation and formation mechanisms of BaTiO3/titanate nanocomposites from solvothermally synthesized K0.8Li0.27Ti1.73O4 crystal3Perovskite Oxides Prepared by Hydrothermal and Solvothermal Synthesis: A Review of Crystallisation, Chemistry, and Compositions152The interplay between thermodynamics and kinetics in the solid-state synthesis of layered oxides264Cation exchange in metal-organic frameworks (MOFs): The hard-soft acid-base (HSAB) principle appraisal187Quantitative Precipitation of Uranyl or Plutonyl Nitrate with N-(1-Adamantyl)acetamide in Nitric Acid Aqueous Solution9From platinum atoms in molecules to colloidal nanoparticles: A review on reduction, nucleation and growth mechanisms108Formation and growth mechanism for niobium oxide nanoparticles: atomistic insight from in situ X-ray total scattering23Hydrothermal synthesis of hexagonal YMnO 3 and YbMnO 3 below 250 °C5Kinetic origins of the metastable zone width in the manganese oxide Pourbaix diagram20Unravelling the complex formation mechanism of HfO 2 nanocrystals using in situ pair distribution function analysis17Insights from In Situ Studies on the Early Stages of Platinum Nanoparticle Formation17Structures and Role of the Intermediate Phases on the Crystallization of BaTiO3 from an Aqueous Synthesis Route19Characterization of Nanomaterials with Total Scattering and Pair Distribution Function Analysis: Examples from Metal Oxide Nanochemistry9Structural Changes during the Growth of Atomically Precise Metal Oxido Nanoclusters from Combined Pair Distribution Function and Small‐Angle X‐ray Scattering Analysis38Structural Changes during the Growth of Atomically Precise Metal Oxido Nanoclusters from Combined Pair Distribution Function and Small‐Angle X‐ray Scattering Analysis4In situ scattering studies of material formation during wet-chemical syntheses1Nucleation and Coalescence of BaTiO3 Using a Continuous Flow Reactor with Water–Ethanol Mixed Solvents10Panoramic (in beam) studies of materials synthesis1Local structure determination using total scattering data12Powder diffraction58Total scattering and pair distribution function analysis for studies of nanomaterials2In Situ Studies of the Formation of Tungsten and Niobium Oxide Nanoparticles: Towards Automated Analysis of Reaction Pathways from PDF Analysis using the Pearson Correlation Coefficient18Solvothermal synthesis of zirconia nanomaterials: Latest developments and future45In situ X‐ray Scattering of the Crystallisation of Basic Magnesium Chlorides using a Laboratory Instrument1Solvothermal synthesis and applications of micro/nano carbons: A review245Challenges and innovative strategies related to synthesis and electrocatalytic/energy storage applications of metal sulfides and its derivatives29Real-Time Crystallization of LiCoO2from β-Co(OH)2and Co3O4: Synthetic Pathways and Structural Evolution22Solvothermal and hydrothermal methods for preparative solid-state chemistry5Advancements and Challenges in Synthesizing Colloidal Semiconductor Nanocrystals by Hot-Injection Method9Cobalt–iron layered double hydroxide nanosheet-wrapped nitrogen-doped graphite felt as an oxygen-evolving electrode19Formation of intermetallic PdIn nanoparticles: influence of surfactants on nanoparticle atomic structure5In situ X-ray diffraction study of the solvothermal formation mechanism of gallium oxide nanoparticles13Nanoscale designing of metal organic framework moieties as efficient tools for environmental decontamination21Synthesis and real-time monitoring of the morphological evolution of luminescent Eu(TCPP) MOFs12Influence of precursor structure on the formation of tungsten oxide polymorphs0Influence of precursor structure on the formation of tungsten oxide polymorphs1A reactor for time-resolved X-ray studies of nucleation and growth during solvothermal synthesis21An in situ study to shed light on the formation of goethite spindles by pseudomorphic transformation of intermediate phases5In situ neutron diffraction to investigate the solid-state synthesis of Ni-rich cathode materials7Design of nanoarchitecture for synergistic interactions to realize nanoflower-like Ni3S4 supported on graphene sheets as high-performance supercapacitor electrodes3Mapping the Complete Reaction Energy Landscape of a Metal–Organic Framework Phase Transformation11Influence of the Precursor Structure on the Formation of Tungsten Oxide Polymorphs14Pair Distribution Function from Liquid Jet Nanoparticle Suspension using Femtosecond X‐ray Pulses3Recent progress in γ-Fe2O3-based catalysts: An overview of the synthesis and applications in environmental remediation43A System‐Level Feasibility Study of a Lead‐Free Ultrasonically Powered Light Delivery Implant for Optogenetics4Passivation-Free, Liquid-Metal-Based Electrosynthesis of Aluminum Metal–Organic Frameworks Mediated by Light Metal Activation12Prospects for the application of nanostructures of bismuth oxychloride (BiOCl) towards the degradation of organic compounds in an aqueous solution3Recent trends in nanozyme research and their potential therapeutic applications86Stabilizing tetragonal ZrO 2 nanocrystallites in solvothermal synthesis10The Chemistry of Spinel Ferrite Nanoparticle Nucleation, Crystallization, and Growth103Unveiling the Potential of Covalent Organic Frameworks for Energy Storage: Developments, Challenges, and Future Prospects137Enhanced catalytic reduction of 4-nitrophenol using bimetallic MOFs: a one-pot synthesis approach0Nanostructural Modification of Fe2O3 Nanoparticles: Carbon Coating for Enhanced Magnetic Behavior4Dependence of photocatalytic efficiency of titania-carbon nanotube nanocomposites on optoelectrical properties and colloidal stability2Heterostructure interface-engineered 3D/2D CoMn 2 O 4 /CoFe 2 O 4 /NF core/shell Bi-functional electrocatalytic nanomaterials for efficient overall water splitting application in alkaline media6Mechanistic insights into solvent-guided growth and structure of MoO 2 nanoparticles in solvothermal synthesis5What goes on in sub-critical solvothermal synthesis of metal ion complexes?2Exploring the potential energy storage capability of NiCdS2 nanocomposites: insights through promising electrochemical, impedance and dielectric analysis16Tunable Multicolor in Heterojunction Ln(BTB) Fast Prepared by Liquid Plasma with In Situ Spectral Monitoring for Anticounterfeiting Application7Reliability of pair distribution function analysis in in situ experiments1Direct Correlation of the Crystalline Phases of La 0.9 Sr 0.1 Co 1– y Fe y O 3−δ with the Partial Oxidation of Methane via In Situ Neutron and Synchrotron Diffraction5Ratiometric fluorescence sensors utilizing lanthanide coordination polymers for detecting foodborne hazards: Mechanisms, design strategies, applications, and future perspectives11Comprehensive insight into Cu-based catalysts for CO2 hydrogenation to methanol9Uncovering Polyoxometalate Speciation in Hydrothermal Systems by Combining Computational Simulation with X-ray Total Scattering5A review of recent advances in Ce3+-activated garnet phosphors for blue-chip-pumped pc-WLEDs81Linking Transition Metal Molybdate Formation to Polyoxometalate and Chloride Complex Speciation: An In Situ X‐Ray Total Scattering Study0Synthesis and Characterizations of Nanomaterials for Electronic Devices0Recent progress of crystalline-amorphous heterointerface: design, mechanism and application15

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  5. Mechanisms for Iron Oxide Formation under Hydrothermal Conditions: An in Situ Total Scattering Study

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  46. Time-Resolved Powder X-ray Diffraction of the Solvothermal Crystallization of Cobalt Gallate Spinel Photocatalyst Reveals Transient Layered Double Hydroxides

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