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RESEARCH PAPER · Review of Scientific Instruments · 1999

Novel apparatus for the in situ study of hydrothermal crystallizations using time-resolved neutron diffraction

Richard I. Walton, Robin J. Francis, P. Shiv Halasyamani, Dermot O’Hare, Ronald I. Smith, Robert Done, Robin J. Humphreys

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42 direct citing works

Novel apparatus for the in situ study of hydrothermal crystallizations using time-resolved neutron diffractionOriginalAn in situ time-resolved neutron diffraction study of the hydrothermal crystallisation of barium titanate11Watching solids crystallise using in situ powder diffraction124An in Situ Energy-Dispersive X-ray Diffraction Study of the Hydrothermal Crystallization of Zeolite A. 2. Effect of Deuteration on Crystallization Kinetics36Following the hydrothermal crystallisation of zeolites using time-resolved in situ powder neutron diffraction42Real Time Observation of the Hydrothermal Crystallization of Barium Titanate Using in Situ Neutron Powder Diffraction152Intercalation chemistry of layered double hydroxides: recent developments and applications1196Neutron powder diffraction of minerals at high pressures and temperatures: some recent technical developments and scientific applications19Subcritical solvothermal synthesis of condensed inorganic materials409Recent results from the in situ study of hydrothermal crystallisations using time-resolved X-ray and neutron diffraction methods33Synthesis and Structure of Low-Dimensional Gallium Fluorodiphosphates Seen during the Crystallization of the Three-Dimensional Microporous Gallium Fluorophosphate ULM-334A review of sample environments in neutron scattering76Sample containment for neutron and high-energy x-ray scattering studies of hydrogen fluoride and related molecular species11The use of neutron scattering in the study of ceramics11High pressurein situx-ray absorption spectroscopy cell for studying simultaneously the liquid phase and the solid/liquid interface68Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time-resolved, In-situ X-ray Powder Diffraction57Neutron Scattering and Diffraction Studies of Fluids and Fluid-Solid Interactions62Time-resolved Neutron Diffraction Studies with Emphasis on Water Ices and Gas Hydrates28Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time‐Resolved, in situ X‐Ray Powder Diffraction15A flow-through hydrothermal cell for in situ neutron diffraction studies of phase transformations13Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study18Probing ore deposits formation: New insights and challenges from synchrotron and neutron studies65A thermosyphon-driven hydrothermal flow-through cell forin situand time-resolved neutron diffraction studies14A large volume cell for in situ neutron diffraction studies of hydrothermal crystallizations10New large volume hydrothermal reaction cell for studying chemical processes under supercritical hydrothermal conditions using time-resolved in situ neutron diffraction14Synthesis, Structure, and Crystallization Study of a Layered Lithium Thiophene-Dicarboxylate39In situ neutron diffraction under high pressure—Providing an insight into working catalysts23Single-pass flow-through reaction cell for high-temperature and high-pressurein situneutron diffraction studies of hydrothermal crystallization processes7Time-Resolved in Situ Neutron Diffraction under Supercritical Hydrothermal Conditions: A Study of the Synthesis of KTiOPO428In Situ Study of Catalytic Processes: Neutron Diffraction of a Methanol Synthesis Catalyst at Industrially Relevant Pressure75In‐situ‐Untersuchung von katalytischen Prozessen bei industriell relevanten Drücken: Neutronenbeugung an einem Methanolsynthesekatalysator19Crystallisation Kinetics of Metal Organic Frameworks From in situ Time-Resolved X-ray Diffraction59In Situ Studies of Solvothermal Synthesis of Energy Materials159Pursuing the Crystallization of Mono- and Polymetallic Nanosized Crystalline Inorganic Compounds by Low-Temperature Wet-Chemistry and Colloidal Routes80Determination of toluene hydrogenation kinetics with neutron diffraction8Unraveling structural and magnetic information during growth of nanocrystalline SrFe 12 O 1936A Fast, Low‐Temperature Synthesis Method for Hexagonal YMnO3: Kinetics, Purity, Size and Shape as Studied by In Situ X‐ray Diffraction6In situ scattering studies of material formation during wet-chemical syntheses1High temperature hydrothermal synthesis of inorganic compounds5In Situ and In Operando Neutron Diffraction of Transition Metal Oxides for Electrochemical Storage1Stepwise Reduction of Ruthenium and Growth of Magnetic Structure During Hydrothermal Crystallisation of SrRu 2 O 6 from KRuO 40Stepwise Reduction of Ruthenium and Growth of Magnetic Structure During Hydrothermal Crystallisation of SrRu 2 O 6 from KRuO 40

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  1. An in situ time-resolved neutron diffraction study of the hydrothermal crystallisation of barium titanate

    Chemical Communications · 2000-01-01

    Richard I. Walton, Franck Millange, Dermot O’Hare, Ronald I. Smith, Iain J. Clark, Derek C. Sinclair

    Read original paper ↗ ·

  2. Watching solids crystallise using in situ powder diffraction

    Chemical Communications · 2000-01-01

    Richard I. Walton, Dermot O’Hare

    Read original paper ↗ ·

  3. An in Situ Energy-Dispersive X-ray Diffraction Study of the Hydrothermal Crystallization of Zeolite A. 2. Effect of Deuteration on Crystallization Kinetics

    The Journal of Physical Chemistry B · 2000-12-12

    Richard I. Walton, Dermot O’Hare

    Read original paper ↗ ·

  4. Following the hydrothermal crystallisation of zeolites using time-resolved in situ powder neutron diffraction

    Microporous and Mesoporous Materials · 2001-11-01

    Richard I. Walton, Ronald I. Smith, Dermot O’Hare

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  5. Real Time Observation of the Hydrothermal Crystallization of Barium Titanate Using in Situ Neutron Powder Diffraction

    Journal of the American Chemical Society · 2001-11-07

    Richard I. Walton, Franck Millange, Ronald I. Smith, Thomas C. Hansen, Dermot O’Hare

    Read original paper ↗ ·

  6. Intercalation chemistry of layered double hydroxides: recent developments and applications

    Journal of Materials Chemistry · 2002-01-01

    Aamir I. Khan, Dermot O’Hare

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  7. Neutron powder diffraction of minerals at high pressures and temperatures: some recent technical developments and scientific applications

    European Journal of Mineralogy · 2002-03-22

    Simon A. T. Redfern

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  8. Subcritical solvothermal synthesis of condensed inorganic materials

    Chemical Society Reviews · 2002-06-13

    Richard I. Walton

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  9. Recent results from the in situ study of hydrothermal crystallisations using time-resolved X-ray and neutron diffraction methods

    Faraday Discussions · 2002-07-30

    Richard I. Walton, Alexander J. Norquist, Ronald I. Smith, Dermot O’Hare

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  10. Synthesis and Structure of Low-Dimensional Gallium Fluorodiphosphates Seen during the Crystallization of the Three-Dimensional Microporous Gallium Fluorophosphate ULM-3

    Chemistry of Materials · 2002-09-14

    Franck Millange, Richard I. Walton, Nathalie Guillou, Thierry Loiseau, Dermot O’Hare, Gérard Férey

    Read original paper ↗ ·

  11. A review of sample environments in neutron scattering

    Zeitschrift für Kristallographie - Crystalline Materials · 2003-02-01

    I. F. Bailey

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  12. Sample containment for neutron and high-energy x-ray scattering studies of hydrogen fluoride and related molecular species

    Review of Scientific Instruments · 2003-09-25

    John F. Turner, Sylvia E. McLain, Timothy H. Free, Chris J. Benmore, Kenneth W. Herwig, Joan E. Siewenie

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  13. The use of neutron scattering in the study of ceramics

    Journal of Materials Science · 2004-10-23

    S. M. Bennington

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  14. High pressurein situx-ray absorption spectroscopy cell for studying simultaneously the liquid phase and the solid/liquid interface

    Review of Scientific Instruments · 2005-04-29

    Jan‐Dierk Grunwaldt, Michael Ramin, Markus Rohr, Alexej Michailovski, Greta Ricarda Patzke, Alfons Baiker

    Read original paper ↗ ·

  15. Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time-resolved, In-situ X-ray Powder Diffraction

    Structure and bonding · 2005-11-08

    Gareth R. Williams, Aamir I. Khan, Dermot O’Hare

    Read original paper ↗ ·

  16. Neutron Scattering and Diffraction Studies of Fluids and Fluid-Solid Interactions

    Reviews in Mineralogy and Geochemistry · 2006-01-01

    D. R. Cole, Kenneth W. Herwig, Eugene Mamontov, John Z. Larese

    Read original paper ↗ ·

  17. Time-resolved Neutron Diffraction Studies with Emphasis on Water Ices and Gas Hydrates

    Reviews in Mineralogy and Geochemistry · 2006-01-01

    W. F. Kuhs, Thomas C. Hansen

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  18. Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time‐Resolved, in situ X‐Ray Powder Diffraction

    ChemInform · 2006-05-23

    Gareth R. Williams, Aamir I. Khan, Dermot O’Hare

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  19. A flow-through hydrothermal cell for in situ neutron diffraction studies of phase transformations

    Physica B Condensed Matter · 2006-07-18

    Brian O’Neill, Christophe Tenailleau, Yung Nogthai, Andrew J. Studer, Joël Brugger, Allan Pring

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  20. Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study

    Chemistry of Materials · 2006-07-18

    Gareth R. Williams, Alexander J. Norquist, Dermot O’Hare

    Read original paper ↗ ·

  21. Probing ore deposits formation: New insights and challenges from synchrotron and neutron studies

    Radiation Physics and Chemistry · 2009-04-07

    Joël Brugger, Allan Pring, Frank Reith, C.G. Ryan, Barbara E. Etschmann, Weihua Liu, Brian O’Neill, Yung Ngothai

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  22. A thermosyphon-driven hydrothermal flow-through cell forin situand time-resolved neutron diffraction studies

    Journal of Applied Crystallography · 2010-03-25

    Fang Xia, Brian O’Neill, Yung Ngothai, Jason Peak, Christophe Tenailleau, Barbara E. Etschmann, Gujie Qian, Joël Brugger, Andrew J. Studer, Scott R. Olsen, Allan Pring

    Read original paper ↗ ·

  23. A large volume cell for in situ neutron diffraction studies of hydrothermal crystallizations

    Review of Scientific Instruments · 2010-10-01

    Fang Xia, Gujie Qian, Joël Brugger, Andrew J. Studer, Scott R. Olsen, Allan Pring

    Read original paper ↗ ·

  24. New large volume hydrothermal reaction cell for studying chemical processes under supercritical hydrothermal conditions using time-resolved in situ neutron diffraction

    Review of Scientific Instruments · 2010-12-01

    Kang Min Ok, Dermot O’Hare, Ronald I. Smith, Mohammed Chowdhury, Hanna Fikremariam

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  25. Synthesis, Structure, and Crystallization Study of a Layered Lithium Thiophene-Dicarboxylate

    Crystal Growth & Design · 2012-01-19

    Racha El Osta, Michel Frigoli, Jérôme Marrot, Manuela E. Medina, Richard I. Walton, Franck Millange

    Read original paper ↗ ·

  26. In situ neutron diffraction under high pressure—Providing an insight into working catalysts

    Nuclear Instruments and Methods in Physics Research Section A Accelerators Spectrometers Detectors and Associated Equipment · 2012-01-20

    Timur Kandemir, Dirk Wallacher, Thomas C. Hansen, Klaus‐Dieter Liss, Raoul Naumann d’Alnoncourt, Robert Schlögl, Malte Behrens

    Read original paper ↗ ·

  27. Single-pass flow-through reaction cell for high-temperature and high-pressurein situneutron diffraction studies of hydrothermal crystallization processes

    Journal of Applied Crystallography · 2012-03-15

    Fang Xia, Joël Brugger, Gujie Qian, Yung Ngothai, Brian O’Neill, Zhao Jing, Stewart Pullen, Scott R. Olsen, Allan Pring

    Read original paper ↗ ·

  28. Time-Resolved in Situ Neutron Diffraction under Supercritical Hydrothermal Conditions: A Study of the Synthesis of KTiOPO4

    Journal of the American Chemical Society · 2012-10-17

    Kang Min Ok, Dong Woo Lee, Ronald I. Smith, Dermot O’Hare

    Read original paper ↗ ·

  29. In Situ Study of Catalytic Processes: Neutron Diffraction of a Methanol Synthesis Catalyst at Industrially Relevant Pressure

    Angewandte Chemie International Edition · 2013-04-10

    Timur Kandemir, Frank Girgsdies, Thomas C. Hansen, Klaus‐Dieter Liss, Igor Kasatkin, Edward L. Kunkes, Gregor Wowsnick, Nikolas Jacobsen, Robert Schlögl, Malte Behrens

    Read original paper ↗ ·

  30. In‐situ‐Untersuchung von katalytischen Prozessen bei industriell relevanten Drücken: Neutronenbeugung an einem Methanolsynthesekatalysator

    Angewandte Chemie · 2013-04-10

    Timur Kandemir, Frank Girgsdies, Thomas C. Hansen, Klaus‐Dieter Liss, Igor Kasatkin, Edward L. Kunkes, Gregor Wowsnick, Nikolas Jacobsen, Robert Schlögl, Malte Behrens

    Read original paper ↗ ·

  31. Crystallisation Kinetics of Metal Organic Frameworks From in situ Time-Resolved X-ray Diffraction

    Powder Diffraction · 2013-09-01

    Racha El Osta, Mark Feyand, Norbert Stock, Franck Millange, Richard I. Walton

    Read original paper ↗ ·

  32. In Situ Studies of Solvothermal Synthesis of Energy Materials

    ChemSusChem · 2014-03-05

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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  33. Pursuing the Crystallization of Mono- and Polymetallic Nanosized Crystalline Inorganic Compounds by Low-Temperature Wet-Chemistry and Colloidal Routes

    Chemical Reviews · 2015-09-25

    Stefano Diodati, Paolo Dolcet, Maurizio Casarin, Silvia Gross

    Read original paper ↗ ·

  34. Determination of toluene hydrogenation kinetics with neutron diffraction

    Physical Chemistry Chemical Physics · 2016-01-01

    Marta Falkowska, Sarayute Chansai, Haresh Manyar, Lynn F. Gladden, Daniel T. Bowron, Tristan G. A. Youngs, Christopher Hardacre

    Read original paper ↗ ·

  35. Unraveling structural and magnetic information during growth of nanocrystalline SrFe 12 O 19

    Journal of Materials Chemistry C · 2016-01-01

    Cecilia Granados‐Miralles, Matilde Saura Muzquiz, Espen Drath Bøjesen, Kirsten M. Ø. Jensen, H.L. Andersen, Mogens Christensen

    Read original paper ↗ ·

  36. A Fast, Low‐Temperature Synthesis Method for Hexagonal YMnO3: Kinetics, Purity, Size and Shape as Studied by In Situ X‐ray Diffraction

    Chemistry - A European Journal · 2020-03-04

    Kenneth P. Marshall, Anders B. Blichfeld, Susanne Linn Skjærvø, Ola G. Grendal, Wouter van Beek, Sverre M. Selbach, Tor Grande, Mari‐Ann Einarsrud

    Read original paper ↗ ·

  37. In situ scattering studies of material formation during wet-chemical syntheses

    Elsevier eBooks · 2021-08-04

    Susanne Linn Skjærvø, Mikkel Juelsholt, Kirsten M. Ø. Jensen

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  38. High temperature hydrothermal synthesis of inorganic compounds

    Elsevier eBooks · 2022-03-29

    Joseph W. Kolis, Colin D. McMillen

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  39. In Situ and In Operando Neutron Diffraction of Transition Metal Oxides for Electrochemical Storage

    Unknown journal · 2022-04-08

    Christophe Didier, Zhanhu Guo, Bohang Song, Ashfia Huq, Vanessa Kate Peterson

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  40. Stepwise Reduction of Ruthenium and Growth of Magnetic Structure During Hydrothermal Crystallisation of SrRu 2 O 6 from KRuO 4

    Angewandte Chemie International Edition · 2025-11-17

    Mark Crossman, Craig I. Hiley, Helen Y. Playford, Chris M. Goodway, Ronald I. Smith, Thomas C. Hansen, Richard I. Walton

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  41. Stepwise Reduction of Ruthenium and Growth of Magnetic Structure During Hydrothermal Crystallisation of SrRu 2 O 6 from KRuO 4

    Angewandte Chemie · 2025-11-28

    Mark Crossman, Craig I. Hiley, Helen Y. Playford, Chris M. Goodway, Ronald I. Smith, Thomas C. Hansen, Richard I. Walton

    Read original paper ↗ ·
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