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RESEARCH PAPER · Chemical Communications · 2000

Watching solids crystallise using in situ powder diffraction

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Watching solids crystallise using in situ powder diffractionOriginalChemInform Abstract: Watching Solids Crystallize Using in situ Powder Diffraction0Microporous Solids: From Organically Templated Inorganic Skeletons to Hybrid Frameworks...Ecumenism in Chemistry659Nucleation and crystallization of solids from solution81Real Time Observation of the Hydrothermal Crystallization of Barium Titanate Using in Situ Neutron Powder Diffraction152Identification of a Key Precursor Phase for Synthesis of SAPO-34 and Kinetics of Formation Investigated by in Situ X-ray Diffraction73Hydrothermal synthesis and structure of a zinc arsenate–oxalate, [NH3(CH2)3NH2(CH2)3NH3][Zn3(AsO4)(HAsO4)2(C2O4)], and a zinc arsenate, [{NH3(CH3)2NH2(CH3)3NH3}2][Zn6(AsO4)4(HAsO4)3]·H2O, with three-dimensional structures16A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates50A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates6In‐Situtime‐resolved X‐ray diffraction: The current state of the art11An Investigation of the Synthesis of the Layered Perovskite RbCa2Nb3O10 Using Time-Resolved in Situ High-Temperature Powder X-ray Diffraction19Synthesis and Structure of Low-Dimensional Gallium Fluorodiphosphates Seen during the Crystallization of the Three-Dimensional Microporous Gallium Fluorophosphate ULM-334Hydrothermal Synthesis of Nanoporous Metalofluorophosphates. 1. Precursor Solutions of Titanium Fluoride and Fluorophosphate in Water, a 19F and 31P NMR Study16In‐situ Energy‐Dispersive X‐ray Diffraction Studies of Crystal Growth and Compound Conversion Under Solvothermal Conditions47In Situ NMR of SAPO-34 Crystallization120Morpholine, an in Situ 13C NMR pH Meter for Hydrothermal Crystallogenesis of SAPO-3430Hydrothermal Synthesis of Nanoporous Metalofluorophosphates. 2. In Situ and ex Situ 19F and 31P NMR of Nano- and Mesostructured Titanium Phosphates Crystallogenesis26Variable temperature in situ X-ray diffraction study of mechanically activated synthesis of calcium titanate, CaTiO350Sample containment for neutron and high-energy x-ray scattering studies of hydrogen fluoride and related molecular species11Probing Molten Salt Flux Reactions Using Time-Resolved in Situ High-Temperature Powder X-ray Diffraction: A New Synthesis Route to the Mixed-Valence NaTi2O445Local Order of Amorphous Zeolite Precursors from 29Si{H} CPMAS and 27Al and 23Na MQMAS NMR and Evidence for the Nature of Medium-Range Order from Neutron Diffraction49Nanostructured Oxides in Chemistry: Characterization and Properties1035Observation and Reactivity of the Chainlike Species ([Al(PO4)2]3-)n during the X-ray Diffraction Investigation of the Hydrothermal Synthesis of the Super-sodalite Sodium Aluminophosphate MIL-74 (Na2Al7(PO4)12·4trenH3·Na(H2O)16)42In situ spectroscopic investigation of heterogeneous catalysts and reaction media at high pressure110Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques105Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken24Syntheses and applications of nanocatalysts based on nanoporous materials14In-situ XRD as a tool to understanding zeolite crystallization105Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study18Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry62Sequential transformations in assemblies based on octamolybdate clusters and 1,2-bis(4-pyridyl)ethane39Direct measurement of the kinetics of geopolymerisation by in-situ energy dispersive X-ray diffractometry60Hydrothermal Synthesis and Crystal Structure of Novel Alkali Trimolybdates7In situ studies of the crystallisation of microporous materials using synchrotron radiation based X-ray techniques0Geopolymerisation kinetics. 1. In situ energy-dispersive X-ray diffractometry224Watching the crystallisation of complex oxides by in situ X-ray techniques28Crystallization of AlPO4-5 Aluminophosphate Molecular Sieve Prepared in Fluoride Medium: A Multinuclear Solid-State NMR Study61Synthesis and Structural Determination of Four Novel Metal−Organic Frameworks in a Zn−3-Amino-1,2,4-Triazole System51Control of framework stoichiometry in MeGaPO laumontites using 1-methylimidazole as structure-directing agent5Crystallization of magnesium substituted aluminophosphate of type-36 as studied by solid-state NMR spectroscopy16On the Structure of Cobalt-Substituted Aluminophosphate Catalysts and Their Catalytic Performance1Hydrothermal Formation of W/Mo-Oxides: A Multidisciplinary Study of Growth and Shape64Desilication Reactions at Digestion Conditions: An in Situ X-ray Diffraction Study31Control of polymorphism in NaNbO 3 by hydrothermal synthesis71Time and position resolved in situ X-ray diffraction study of the hydrothermal conversion of gypsum monoliths to hydroxyapatite11Kinetics and Mechanisms of the Hydrothermal Crystallization of Calcium Titanate Species47Linking Simultaneous In Situ WAXS/SAXS/Raman with Raman/ATR/UV–vis Spectroscopy: Comprehensive Insight into the Synthesis of Molybdate Catalyst Precursors35The Interplay of Crystallization Kinetics and Morphology in Nanostructured W/Mo Oxide Formation: An in situ Diffraction Study38In Situ Comparison of Ionothermal Kinetics Under Microwave And Conventional Heating36Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques30In situ X-ray diffraction study of the hydrothermal crystallization of hierarchical Bi2WO6 nanostructures42Observation and Isolation of Layered and Framework Ytterbium Hydroxide Phases Using In Situ Energy-Dispersive X-ray Diffraction56Combined Synchrotron XRD/Raman Measurements: In Situ Identification of Polymorphic Transitions during Crystallization Processes39Hydrothermal Synthesis of Bi6S2O15 Nanowires: Structural, in situ EXAFS, and Humidity‐Sensing Studies37Selective Sorption of Organic Molecules by the Flexible Porous Hybrid Metal−Organic Framework MIL-53(Fe) Controlled by Various Host−Guest Interactions122A time-resolved diffraction study of a window of stability in the synthesis of a copper carboxylate metal–organic framework154Oxide Nanomaterials: Synthetic Developments, Mechanistic Studies, and Technological Innovations366Oxidische Nanomaterialien: Von der Synthese über den Mechanismus zur technologischen Innovation25New large volume hydrothermal reaction cell for studying chemical processes under supercritical hydrothermal conditions using time-resolved in situ neutron diffraction14Determination of reaction kinetics and mechanisms of 1.13 NM tobermorite by in-situ neutron diffraction4The application of statistical methodology to the analysis of time-resolved X-ray diffraction data12Structure, Size, and Morphology Control of Nanocrystalline Lithium Cobalt Oxide25In‐Situ Monitoring of the Formation of Crystalline Solids251In‐situ‐Verfolgung der Bildung kristalliner Feststoffe69Real-time synchrotron powder X-ray diffraction study of the antisite defect formation during sub- and supercritical synthesis of LiFePO4and LiFe1−xMnxPO4nanoparticles38Uptake of Liquid Alcohols by the Flexible Fe III Metal–Organic Framework MIL‐53 Observed by Time‐Resolved In Situ X‐ray Diffraction47Formate modulated solvothermal synthesis of ZIF-8 investigated using time-resolved in situ X-ray diffraction and scanning electron microscopy368A furnace and environmental cell for thein situinvestigation of molten salt electrolysis using high-energy X-ray diffraction9In situ EDXRD study of the chemistry of aging of co-precipitated mixed Cu,Zn hydroxycarbonates – consequences for the preparation of Cu/ZnO catalysts57Hydrothermal synthesis map of bismuth titanates31Single-pass flow-through reaction cell for high-temperature and high-pressurein situneutron diffraction studies of hydrothermal crystallization processes7X‐Ray Diffraction and Small Angle X‐Ray Scattering23Time-Resolved in Situ Neutron Diffraction under Supercritical Hydrothermal Conditions: A Study of the Synthesis of KTiOPO428In situ high-temperature X-ray diffraction measurements: Application to the study of heterogeneous catalysts1A comprehensive study of the crystallization mechanism involved in the nonaqueous formation of tungstite33Adsorption of N/S heterocycles in the flexible metal–organic framework MIL-53(FeIII) studied by in situ energy dispersive X-ray diffraction46Diffraction and Spectroscopy of Porous Solids1Synthetic Methodologies0Crystallisation Kinetics of Metal Organic Frameworks From in situ Time-Resolved X-ray Diffraction59From an Open Framework to a Layered and a Hexagonal Tungsten Oxide Structure: Controlled Transformation Reactions of an Extended Solid-State Material, Cs3Ga7(SeO3)12 to Ga(OH)(SeO3) and KGa3(SeO4)2(OH)613Insight into the mechanism of modulated syntheses: in situ synchrotron diffraction studies on the formation of Zr-fumarate MOF158In Situ Studies of Solvothermal Synthesis of Energy Materials159Controlling Allotropism in Ruthenium Nanoparticles: A Pulsed-Flow Supercritical Synthesis and in Situ Synchrotron X-ray Diffraction Study41Evolution of atomic structure during nanoparticle formation57In Situ Powder Diffraction Study of the Hydrothermal Synthesis of ZnO Nanoparticles49In situ powder X-ray diffraction study of the hydro-thermal formation of LiMn 2 O 4 nanocrystallites10Mechanisms for Iron Oxide Formation under Hydrothermal Conditions: An in Situ Total Scattering Study92Chemical Reactions followed byin situNeutron Powder Diffraction57Hydrothermal Synthesis and in Situ Powder X-ray Diffraction Study of Bismuth-Substituted Ceria Nanoparticles28Pursuing the Crystallization of Mono- and Polymetallic Nanosized Crystalline Inorganic Compounds by Low-Temperature Wet-Chemistry and Colloidal Routes80Development of a new in situ analysis technique applying luminescence of local coordination sensors: principle and application for monitoring metal-ligand exchange processes23The chemistry of nucleation119The chemistry of ZnWO 4 nanoparticle formation41Unraveling structural and magnetic information during growth of nanocrystalline SrFe 12 O 1936In SituStudies of the Crystallization of Metal-Organic Frameworks10Simultaneous Differential Scanning Calorimetry-Synchrotron X-ray Powder Diffraction: A Powerful Technique for Physical Form Characterization in Pharmaceutical Materials39In Situ Studies on Phase Transitions of Tris(acetylacetonato)-Aluminum(III) Al(acac)321In situ neutron diffraction study of the formation of Ho 2 Ge 2 O 7 pyrochlore at high temperature and pressure13In-situ high temperature X-ray diffraction study on the phase transition process of polymetallic sulfide ore4Mechanistic Aspects in the Formation, Growth and Surface Functionalization of Metal Oxide Nanoparticles in Organic Solvents125Panoramic Synthesis as an Effective Materials Discovery Tool: The System Cs/Sn/P/Se as a Test Case46In situ monitoring metal-ligand exchange processes by optical spectroscopy and X-ray diffraction analysis: a review22A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions33100 yearsin situdiffraction5Very fast crystallisation of MFe2O4 spinel ferrites (M = Co, Mn, Ni, Zn) under low temperature hydrothermal conditions: a time-resolved structural investigation34Formation Mechanisms of Nanocrystalline MnO 2 Polymorphs under Hydrothermal Conditions78Pitfalls and reproducibility ofin situsynchrotron powder X-ray diffraction studies of solvothermal nanoparticle formation31Lepidocrocite-Type Titanate Formation from Isostructural Prestructures under Hydrothermal Reactions: Observation by Synchrotron X-ray Total Scattering Analyses51A prototype handheld X-ray diffraction instrument5Analytical Techniques for Probing Small-Scale Layers that Preserve Information on Gas–Solid Interactions15Hydrothermal reactor for in-situ synchrotron radiation powder diffraction at SPring-8 BL02B2 for quantitative design for nanoparticle10In situ Monitoring of the Formation of [Bis(acetylacetonato)manganese(II)] Complexes10Solid-State NMR Studies of Zeolites and Zeotype Materials Synthesis0Looking into the Black Box of Solid‐State Synthesis74A Fast, Low‐Temperature Synthesis Method for Hexagonal YMnO3: Kinetics, Purity, Size and Shape as Studied by In Situ X‐ray Diffraction6In Situ Monitoring of Particle Formation with Spectroscopic and Analytical Techniques Under Solvothermal Conditions11Mechanistic insight of KBiQ 2 (Q = S, Se) using panoramic synthesis towards synthesis-by-design27In situ scattering studies of material formation during wet-chemical syntheses1Panoramic (in beam) studies of materials synthesis1Solvothermal and hydrothermal methods for preparative solid-state chemistry5Detailed insights into the formation pathway of CdS and ZnS in solution: a multi-modal in situ characterisation approach9Further Sustainable and/or Unconventional Low-temperature Wet-chemical Synthetic Methods1Stepwise Reduction of Ruthenium and Growth of Magnetic Structure During Hydrothermal Crystallisation of SrRu 2 O 6 from KRuO 40Stepwise Reduction of Ruthenium and Growth of Magnetic Structure During Hydrothermal Crystallisation of SrRu 2 O 6 from KRuO 40Neutron Diffraction for Structural Characterisation of Inorganic Materials0

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  1. ChemInform Abstract: Watching Solids Crystallize Using in situ Powder Diffraction

    ChemInform · 2001-02-13

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  2. Microporous Solids: From Organically Templated Inorganic Skeletons to Hybrid Frameworks...Ecumenism in Chemistry

    Chemistry of Materials · 2001-09-25

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  3. Nucleation and crystallization of solids from solution

    Current Opinion in Solid State and Materials Science · 2001-10-01

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  4. Real Time Observation of the Hydrothermal Crystallization of Barium Titanate Using in Situ Neutron Powder Diffraction

    Journal of the American Chemical Society · 2001-11-07

    Richard I. Walton, Franck Millange, Ronald I. Smith, Thomas C. Hansen, Dermot M. O'Hare

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  5. Identification of a Key Precursor Phase for Synthesis of SAPO-34 and Kinetics of Formation Investigated by in Situ X-ray Diffraction

    The Journal of Physical Chemistry B · 2001-11-22

    Ørnulv B. Vistad, Duncan E. Akporiaye, Karl Petter Lillerud

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  6. Hydrothermal synthesis and structure of a zinc arsenate–oxalate, [NH3(CH2)3NH2(CH2)3NH3][Zn3(AsO4)(HAsO4)2(C2O4)], and a zinc arsenate, [{NH3(CH3)2NH2(CH3)3NH3}2][Zn6(AsO4)4(HAsO4)3]·H2O, with three-dimensional structures

    Journal of the Chemical Society Dalton Transactions · 2002-01-01

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  7. A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates

    Angewandte Chemie International Edition · 2002-04-02

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  8. A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates

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  9. In‐Situtime‐resolved X‐ray diffraction: The current state of the art

    Synchrotron Radiation News · 2002-07-01

    Ann E. Terry, G. Vaughan, Åke Kvick, Richard I. Walton, Alexander J. Norquist, Dermot M. O'Hare

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  10. An Investigation of the Synthesis of the Layered Perovskite RbCa2Nb3O10 Using Time-Resolved in Situ High-Temperature Powder X-ray Diffraction

    Chemistry of Materials · 2002-09-05

    Margret J. Geselbracht, Richard I. Walton, E. Sarah Cowell, Franck Millange, Dermot M. O'Hare

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  11. Synthesis and Structure of Low-Dimensional Gallium Fluorodiphosphates Seen during the Crystallization of the Three-Dimensional Microporous Gallium Fluorophosphate ULM-3

    Chemistry of Materials · 2002-09-14

    Franck Millange, Richard I. Walton, Nathalie Guillou, Thierry Loiseau, Dermot M. O'Hare, Gérard Férey

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  12. Hydrothermal Synthesis of Nanoporous Metalofluorophosphates. 1. Precursor Solutions of Titanium Fluoride and Fluorophosphate in Water, a 19F and 31P NMR Study

    Chemistry of Materials · 2002-11-22

    Christian Serre, Tristan Corbière, Chantal Lorentz, Françis Taulelle, Gérard Férey

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  13. In‐situ Energy‐Dispersive X‐ray Diffraction Studies of Crystal Growth and Compound Conversion Under Solvothermal Conditions

    European Journal of Inorganic Chemistry · 2003-01-20

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  14. In Situ NMR of SAPO-34 Crystallization

    Chemistry of Materials · 2003-03-29

    Ørnulv B. Vistad, Duncan E. Akporiaye, Françis Taulelle, Karl Petter Lillerud

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  15. Morpholine, an in Situ 13C NMR pH Meter for Hydrothermal Crystallogenesis of SAPO-34

    Chemistry of Materials · 2003-03-29

    Ørnulv B. Vistad, Duncan E. Akporiaye, Françis Taulelle, Karl Petter Lillerud

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  16. Hydrothermal Synthesis of Nanoporous Metalofluorophosphates. 2. In Situ and ex Situ 19F and 31P NMR of Nano- and Mesostructured Titanium Phosphates Crystallogenesis

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  17. Variable temperature in situ X-ray diffraction study of mechanically activated synthesis of calcium titanate, CaTiO3

    Materials Research Bulletin · 2003-05-27

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  18. Sample containment for neutron and high-energy x-ray scattering studies of hydrogen fluoride and related molecular species

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  19. Probing Molten Salt Flux Reactions Using Time-Resolved in Situ High-Temperature Powder X-ray Diffraction: A New Synthesis Route to the Mixed-Valence NaTi2O4

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  20. Local Order of Amorphous Zeolite Precursors from 29Si{H} CPMAS and 27Al and 23Na MQMAS NMR and Evidence for the Nature of Medium-Range Order from Neutron Diffraction

    The Journal of Physical Chemistry B · 2004-05-21

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  21. Nanostructured Oxides in Chemistry: Characterization and Properties

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  22. Observation and Reactivity of the Chainlike Species ([Al(PO4)2]3-)n during the X-ray Diffraction Investigation of the Hydrothermal Synthesis of the Super-sodalite Sodium Aluminophosphate MIL-74 (Na2Al7(PO4)12·4trenH3·Na(H2O)16)

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  23. In situ spectroscopic investigation of heterogeneous catalysts and reaction media at high pressure

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  24. Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques

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  25. Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken

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  27. In-situ XRD as a tool to understanding zeolite crystallization

    Current Opinion in Colloid & Interface Science · 2006-01-28

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  28. Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study

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  29. Hydrothermal Synthesis of Molybdenum Oxide Based Materials: Strategy and Structural Chemistry

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  30. Sequential transformations in assemblies based on octamolybdate clusters and 1,2-bis(4-pyridyl)ethane

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  31. Direct measurement of the kinetics of geopolymerisation by in-situ energy dispersive X-ray diffractometry

    Journal of Materials Science · 2006-12-08

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  32. Hydrothermal Synthesis and Crystal Structure of Novel Alkali Trimolybdates

    Zeitschrift für anorganische und allgemeine Chemie · 2006-12-11

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  33. In situ studies of the crystallisation of microporous materials using synchrotron radiation based X-ray techniques

    Studies in surface science and catalysis · 2007-01-01

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  34. Geopolymerisation kinetics. 1. In situ energy-dispersive X-ray diffractometry

    Chemical Engineering Science · 2007-02-03

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  35. Watching the crystallisation of complex oxides by in situ X-ray techniques

    Applied Catalysis A General · 2007-03-04

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  36. Crystallization of AlPO4-5 Aluminophosphate Molecular Sieve Prepared in Fluoride Medium: A Multinuclear Solid-State NMR Study

    The Journal of Physical Chemistry B · 2007-05-27

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  37. Synthesis and Structural Determination of Four Novel Metal−Organic Frameworks in a Zn−3-Amino-1,2,4-Triazole System

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  38. Control of framework stoichiometry in MeGaPO laumontites using 1-methylimidazole as structure-directing agent

    Microporous and Mesoporous Materials · 2007-11-09

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  39. Crystallization of magnesium substituted aluminophosphate of type-36 as studied by solid-state NMR spectroscopy

    Microporous and Mesoporous Materials · 2008-03-05

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  40. On the Structure of Cobalt-Substituted Aluminophosphate Catalysts and Their Catalytic Performance

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  41. Hydrothermal Formation of W/Mo-Oxides: A Multidisciplinary Study of Growth and Shape

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  42. Desilication Reactions at Digestion Conditions: An in Situ X-ray Diffraction Study

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  43. Control of polymorphism in NaNbO 3 by hydrothermal synthesis

    Chemical Communications · 2008-11-12

    Deena R. Modeshia, Richard J. Darton, Sharon Elizabeth Ashbrook, Richard I. Walton

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  44. Time and position resolved in situ X-ray diffraction study of the hydrothermal conversion of gypsum monoliths to hydroxyapatite

    Dalton Transactions · 2009-01-01

    Robin D. Fisher, Richard I. Walton

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  45. Kinetics and Mechanisms of the Hydrothermal Crystallization of Calcium Titanate Species

    Crystal Growth & Design · 2009-03-10

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  46. Linking Simultaneous In Situ WAXS/SAXS/Raman with Raman/ATR/UV–vis Spectroscopy: Comprehensive Insight into the Synthesis of Molybdate Catalyst Precursors

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  47. The Interplay of Crystallization Kinetics and Morphology in Nanostructured W/Mo Oxide Formation: An in situ Diffraction Study

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  48. In Situ Comparison of Ionothermal Kinetics Under Microwave And Conventional Heating

    The Journal of Physical Chemistry C · 2009-11-02

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  49. Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques

    Physical Chemistry Chemical Physics · 2009-11-13

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  50. In situ X-ray diffraction study of the hydrothermal crystallization of hierarchical Bi2WO6 nanostructures

    Nanoscale · 2010-01-01

    Ying Zhou, Е. А. Антонова, Wolfgang Bensch, Greta Ricarda Patzke

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