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RESEARCH PAPER · Journal of the American Chemical Society · 2012

Time-Resolved in Situ Neutron Diffraction under Supercritical Hydrothermal Conditions: A Study of the Synthesis of KTiOPO4

Kang Min Ok, Dong Woo Lee, Ronald I. Smith, Dermot M. O'Hare

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Time-Resolved in Situ Neutron Diffraction under Supercritical Hydrothermal Conditions: A Study of the Synthesis of KTiOPO4OriginalFrom an Open Framework to a Layered and a Hexagonal Tungsten Oxide Structure: Controlled Transformation Reactions of an Extended Solid-State Material, Cs3Ga7(SeO3)12 to Ga(OH)(SeO3) and KGa3(SeO4)2(OH)613In Situ Studies of Solvothermal Synthesis of Energy Materials159Evolution of atomic structure during nanoparticle formation57Mechanisms for Iron Oxide Formation under Hydrothermal Conditions: An in Situ Total Scattering Study92The chemistry of nucleation119Hydrothermal Synthesis of CoSb2O4: In Situ Powder X-ray Diffraction, Crystal Structure, and Electrochemical Properties29Application of the Dimensional Reduction Formalism to Pb12[Li2(P2O7)2(P4O13)2](P4O13): a Phosphate Containing Three Types of Isolated P–O Groups21Toward the Rational Design of Novel Noncentrosymmetric Materials: Factors Influencing the Framework Structures601Application of the dimensional reduction formalism to Pb 9−x Ba x [Li 2 (P 2 O 7 ) 2 (P 4 O 13 ) 2 ] (x = 0, 2, 6, 7): a series of phosphates with two types of isolated polyphosphate groups13From a Metastable Layer to a Stable Ring: A Kinetic Study for Transformation Reactions of Li2Mo3TeO12 to Polyoxometalates12Pitfalls and reproducibility ofin situsynchrotron powder X-ray diffraction studies of solvothermal nanoparticle formation31A New Cadmium‐Based Pb2Cd3(PO4)2(P2O7) with Two Types of Isolated P–O Groups18Synthesis, structure and characterization of three new Mg-containing phosphates with deep-UV cut-off edges9Time-Resolved In Situ Neutron Diffraction Study of Cu22Fe8Ge4S32 Germanite: A Guide for the Synthesis of Complex Chalcogenides5A2BBi2(PO4)2(P2O7) (A = K, Rb, B = Pb, Cd): the Effect of Cation Sizes on Structural Evolution10A2(TeO)P2O7 (A = K, Rb, Cs): Three new tellurite-pyrophosphates with large birefringence17Order and Disorder: Toward the Thermodynamically Stable α-BaMoO2F4 from the Metastable Polymorph31Synthesis, Structure, Characterization, and Calculation of a Noncentrosymmetric Fluorine-Containing Indium Iodate, Ba[InF3(IO3)2]10In situ scattering studies of material formation during wet-chemical syntheses1In Situ and In Operando Neutron Diffraction of Transition Metal Oxides for Electrochemical Storage1Design Principles for Noncentrosymmetric Materials23Mapping the Complete Reaction Energy Landscape of a Metal–Organic Framework Phase Transformation11Novel antimony phosphates with enlarged birefringence induced by lone pair cations4The enhanced bandgap and birefringence of rare-earth phosphates XPO 4 (X = Sc, Y, La, and Lu): a first-principles investigation7The Chemistry of Spinel Ferrite Nanoparticle Nucleation, Crystallization, and Growth103Unraveling Materials Synthesis Mechanisms Using In Situ Transmission Electron Microscopy and Neutron Scattering5Topology-Guided Discovery of BaIn 2 Si 7 P 12 : A Quaternary Diamond-like Framework Phosphide with Giant Second-Harmonic Generation and High Laser-Induced Damage Threshold24Neutron Diffraction for Structural Characterisation of Inorganic Materials0

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  1. From an Open Framework to a Layered and a Hexagonal Tungsten Oxide Structure: Controlled Transformation Reactions of an Extended Solid-State Material, Cs3Ga7(SeO3)12 to Ga(OH)(SeO3) and KGa3(SeO4)2(OH)6

    Inorganic Chemistry · 2013-10-21

    Hyun Sun Ahn, Dong Woo Lee, Kang Min Ok

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  2. In Situ Studies of Solvothermal Synthesis of Energy Materials

    ChemSusChem · 2014-03-05

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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  3. Evolution of atomic structure during nanoparticle formation

    IUCrJ · 2014-04-13

    Christoffer Tyrsted, Nina Lock, Kirsten M. Ø. Jensen, Mogens Christensen, Espen Drath Bøjesen, Hermann Emerich, G. Vaughan, Simon J. L. Billinge, Bo B. Iversen

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  4. Mechanisms for Iron Oxide Formation under Hydrothermal Conditions: An in Situ Total Scattering Study

    ACS Nano · 2014-09-25

    Kirsten M. Ø. Jensen, H.L. Andersen, Christoffer Tyrsted, Espen Drath Bøjesen, Ann‐Christin Dippel, Nina Lock, Simon J. L. Billinge, Bo B. Iversen, Mogens Christensen

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  5. The chemistry of nucleation

    CrystEngComm · 2016-01-01

    Espen Drath Bøjesen, Bo B. Iversen

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  6. Hydrothermal Synthesis of CoSb2O4: In Situ Powder X-ray Diffraction, Crystal Structure, and Electrochemical Properties

    Crystal Growth & Design · 2016-01-05

    Peter Nørby, Martin Roelsgaard, Martin Søndergaard, Bo B. Iversen

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  7. Application of the Dimensional Reduction Formalism to Pb12[Li2(P2O7)2(P4O13)2](P4O13): a Phosphate Containing Three Types of Isolated P–O Groups

    Inorganic Chemistry · 2016-07-11

    Xiangyu Zhang, Hongping Wu, Ying Wang, Xiaoyu Dong, Shujuan Han, Shilie Pan

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  8. Toward the Rational Design of Novel Noncentrosymmetric Materials: Factors Influencing the Framework Structures

    Accounts of Chemical Research · 2016-11-14

    Kang Min Ok

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  9. Application of the dimensional reduction formalism to Pb 9−x Ba x [Li 2 (P 2 O 7 ) 2 (P 4 O 13 ) 2 ] (x = 0, 2, 6, 7): a series of phosphates with two types of isolated polyphosphate groups

    Dalton Transactions · 2017-01-01

    Xiangyu Zhang, Hongping Wu, Qiong Liu, Xiaoyu Dong, Yunlei Chen, Zhihua Yang, Xiaodong Wen, Shilie Pan

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  10. From a Metastable Layer to a Stable Ring: A Kinetic Study for Transformation Reactions of Li2Mo3TeO12 to Polyoxometalates

    Chemistry - A European Journal · 2017-12-07

    Seung‐Jin Oh, Seong‐Ji Lim, Tae‐Soo You, Kang Min Ok

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  11. Pitfalls and reproducibility ofin situsynchrotron powder X-ray diffraction studies of solvothermal nanoparticle formation

    Journal of Applied Crystallography · 2018-03-28

    H.L. Andersen, Espen Drath Bøjesen, Steinar Birgisson, Mogens Christensen, Bo B. Iversen

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  12. A New Cadmium‐Based Pb2Cd3(PO4)2(P2O7) with Two Types of Isolated P–O Groups

    European Journal of Inorganic Chemistry · 2019-01-24

    Wenqiang Chen, Qun Jing, Qiaoqiao Zhang, Ming‐Hsien Lee, Xuefang Lu, Ping Wei, Zhaohui Chen

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  13. Synthesis, structure and characterization of three new Mg-containing phosphates with deep-UV cut-off edges

    New Journal of Chemistry · 2020-01-01

    Zhen Qian, Hongping Wu, Hongwei Yu, Zhanggui Hu, Jiyang Wang, Yicheng Wu

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  14. Time-Resolved In Situ Neutron Diffraction Study of Cu22Fe8Ge4S32 Germanite: A Guide for the Synthesis of Complex Chalcogenides

    Chemistry of Materials · 2020-09-21

    Laura Paradis-Fortin, Pierric Lemoine, Carmelo Prestipino, Pavan Kumar Ventrapati, Bernard Raveau, Vivian Nassif, Stéphane Cordier, Emmanuel Guilmeau

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  15. A2BBi2(PO4)2(P2O7) (A = K, Rb, B = Pb, Cd): the Effect of Cation Sizes on Structural Evolution

    European Journal of Inorganic Chemistry · 2020-09-24

    Lu Qi, Zhaohui Chen, Lu Li, Qun Jing, Na Li, Zhongqi Jiang, Xiaoyu Dong, Ming‐Hsien Lee

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  16. A2(TeO)P2O7 (A = K, Rb, Cs): Three new tellurite-pyrophosphates with large birefringence

    Journal of Alloys and Compounds · 2021-02-02

    Min Zhao, Weimin Dong, Yuandong Wu, Dajiang Mei, Shaoguo Wen, Thomas Doert

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  17. Order and Disorder: Toward the Thermodynamically Stable α-BaMoO2F4 from the Metastable Polymorph

    Chemistry of Materials · 2021-02-25

    Hongil Jo, Min Hyung Lee, Kang Min Ok

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  18. Synthesis, Structure, Characterization, and Calculation of a Noncentrosymmetric Fluorine-Containing Indium Iodate, Ba[InF3(IO3)2]

    Crystal Growth & Design · 2021-06-24

    Xiaoqing Jiang, Hongping Wu, Hongwei Yu, Zhanggui Hu, Jiyang Wang, Yicheng Wu

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  19. In situ scattering studies of material formation during wet-chemical syntheses

    Elsevier eBooks · 2021-08-04

    Susanne Linn Skjærvø, Mikkel Juelsholt, Kirsten M. Ø. Jensen

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  20. In Situ and In Operando Neutron Diffraction of Transition Metal Oxides for Electrochemical Storage

    Unknown journal · 2022-04-08

    Christophe Didier, Zhanhu Guo, Bohang Song, Ashfia Huq, Vanessa Kate Peterson

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  21. Design Principles for Noncentrosymmetric Materials

    Annual Review of Materials Research · 2023-07-03

    Xudong Huai, T. Thao Tran

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  22. Mapping the Complete Reaction Energy Landscape of a Metal–Organic Framework Phase Transformation

    ACS Materials Letters · 2023-08-17

    Sylvia L. Hanna, Michael L. Barsoum, Tekalign Terfa Debela, Christos D. Malliakas, Madeleine A. Gaidimas, Julia G. Knapp, Kent O. Kirlikovali, Christopher H. Hendon, Vinayak P. Dravid, Omar K. Farha

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  23. Novel antimony phosphates with enlarged birefringence induced by lone pair cations

    Dalton Transactions · 2024-01-01

    Mei Hu, Jialong Wang, Nuerbiye Tuerhong, Zhiyuan Zhang, Qun Jing, Zhaohui Chen, Yonglei Yang, Ming‐Hsien Lee

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  24. The enhanced bandgap and birefringence of rare-earth phosphates XPO 4 (X = Sc, Y, La, and Lu): a first-principles investigation

    Physical Chemistry Chemical Physics · 2024-01-01

    Nuerbiye Tuerhong, Hongheng Chen, Mei Hu, X.Y. Cui, Haiming Duan, Qun Jing, Zhaohui Chen

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  25. The Chemistry of Spinel Ferrite Nanoparticle Nucleation, Crystallization, and Growth

    ACS Nano · 2024-03-25

    H.L. Andersen, Cecilia Granados‐Miralles, Kirsten M. Ø. Jensen, Matilde Saura Muzquiz, Mogens Christensen

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  26. Unraveling Materials Synthesis Mechanisms Using In Situ Transmission Electron Microscopy and Neutron Scattering

    Chemical Reviews · 2025-09-06

    Jacob Smith, Hwangsun Kim, Ke An, Yan Chen, Ondrej Dyck, Kate Reidy, Miaofang Chi

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  27. Topology-Guided Discovery of BaIn 2 Si 7 P 12 : A Quaternary Diamond-like Framework Phosphide with Giant Second-Harmonic Generation and High Laser-Induced Damage Threshold

    Journal of the American Chemical Society · 2026-02-16

    Jiazheng Zhou, Yu Chu, Xin Su, Ling Luo, Miriding Mutailipu, Shilie Pan, Junjie Li

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  28. Neutron Diffraction for Structural Characterisation of Inorganic Materials

    Royal Society of Chemistry eBooks · 2026-09-23

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