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RESEARCH PAPER · Microporous and Mesoporous Materials · 2001

Following the hydrothermal crystallisation of zeolites using time-resolved in situ powder neutron diffraction

Richard I. Walton, Ronald I. Smith, Dermot O’Hare

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Following the hydrothermal crystallisation of zeolites using time-resolved in situ powder neutron diffractionOriginalReal Time Observation of the Hydrothermal Crystallization of Barium Titanate Using in Situ Neutron Powder Diffraction152Neutron scattering methods for the study of zeolites37A review of sample environments in neutron scattering77In Situ NMR of SAPO-34 Crystallization120Sample containment for neutron and high-energy x-ray scattering studies of hydrogen fluoride and related molecular species11Investigation of the Crystallization Stages of LTA‐Type Zeolite by Complementary Characterization Techniques81Local Order of Amorphous Zeolite Precursors from 29Si{H} CPMAS and 27Al and 23Na MQMAS NMR and Evidence for the Nature of Medium-Range Order from Neutron Diffraction49Recent developments in metal–organic framework chemistry: design, discovery, permanent porosity and flexibility575Transmission Electron Microscopy Study of the Formation of FAU-Type Zeolite at Room Temperature213Observation and Reactivity of the Chainlike Species ([Al(PO4)2]3-)n during the X-ray Diffraction Investigation of the Hydrothermal Synthesis of the Super-sodalite Sodium Aluminophosphate MIL-74 (Na2Al7(PO4)12·4trenH3·Na(H2O)16)42Room temperature synthesis: an efficient way for studying the zeolite formation7Metal−Organic Frameworks from Homometallic Chains of Nickel(II) and 1,4-Cyclohexanedicarboxylate Connectors: Ferrimagnet−Ferromagnet Transformation125In-situ XRD as a tool to understanding zeolite crystallization105Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study18In-situ ultrasonic methods for monitoring the hydrothermal synthesis of LTA-type zeolite from colloidal solutions9A Comparative Investigation of Co2+ and Mn2+ Incorporation into Aluminophosphates by in Situ XAS and DFT Computation8Crystallization of AlPO4-5 Aluminophosphate Molecular Sieve Prepared in Fluoride Medium: A Multinuclear Solid-State NMR Study61Study of the microstructure of amorphous aluminosilicate gel before and after its hydrothermal treatment47Examining the Self-Assembly of Microporous Material AlPO4-11 by Dry-Gel Conversion76The influences of the way of preparation of Me-aluminosilicates (Me=Li, Na, K, Rb and Cs) on the products5Neutron Scattering4Crystallization of magnesium substituted aluminophosphate of type-36 as studied by solid-state NMR spectroscopy16Investigation of Crystallization of Molecular Sieve AlPO4-5 by the Dry Gel Conversion Method41Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques30Kinetic Analysis of Isothermal Crystallization of Potassium Aluminosilicate Ceramics (Leucite and Kalsilite) from Amorphous Potassium Aluminosilicate Precursors8Influence of reaction conditions on the properties of sodium alumino silicate synthesized by simultaneous addition of precursors0A time-resolved diffraction study of a window of stability in the synthesis of a copper carboxylate metal–organic framework154Nascent zeolite frameworks grown from amorphous gels – identification and prospects for crystal engineering3Alkali Hydrothermal Synthesis of Zeolite A Using Oxide By-products11Synthesis, Structure, and Crystallization Study of a Layered Lithium Thiophene-Dicarboxylate39Neutron Scattering2Copper Phosphonatoethanesulfonates: Temperature Dependent in Situ Energy Dispersive X-ray Diffraction Study and Influence of the pH on the Crystal Structures38Neutron Scattering forIn‐situCharacterization of Heterogeneous Catalysis2In Situ Studies of Solvothermal Synthesis of Energy Materials159Präparationsprinzipien mikroporöser Materialien: Vom building block zum hierarchisch aufgebauten porösen System5In SituStudies of the Crystallization of Metal-Organic Frameworks10Solid-State NMR Studies of Zeolites and Zeotype Materials Synthesis0In situ scattering studies of material formation during wet-chemical syntheses1Panoramic (in beam) studies of materials synthesis1In Situ and In Operando Neutron Diffraction of Transition Metal Oxides for Electrochemical Storage1Solvothermal and hydrothermal methods for preparative solid-state chemistry5Direct Correlation of the Crystalline Phases of La 0.9 Sr 0.1 Co 1– y Fe y O 3−δ with the Partial Oxidation of Methane via In Situ Neutron and Synchrotron Diffraction5

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42 direct citing papers saved.

  1. Real Time Observation of the Hydrothermal Crystallization of Barium Titanate Using in Situ Neutron Powder Diffraction

    Journal of the American Chemical Society · 2001-11-07

    Richard I. Walton, Franck Millange, Ronald I. Smith, Thomas C. Hansen, Dermot M. O'Hare

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  2. Neutron scattering methods for the study of zeolites

    Current Opinion in Solid State and Materials Science · 2002-10-01

    H. Jobic

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  3. A review of sample environments in neutron scattering

    Zeitschrift für Kristallographie - Crystalline Materials · 2003-02-01

    I. F. Bailey

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  4. In Situ NMR of SAPO-34 Crystallization

    Chemistry of Materials · 2003-03-29

    Ørnulv B. Vistad, Duncan E. Akporiaye, Françis Taulelle, Karl Petter Lillerud

    Read original paper ↗ ·

  5. Sample containment for neutron and high-energy x-ray scattering studies of hydrogen fluoride and related molecular species

    Review of Scientific Instruments · 2003-09-25

    John F. Turner, Sylvia E. McLain, Timothy H. Free, Chris J. Benmore, Kenneth W. Herwig, Joan E. Siewenie

    Read original paper ↗ ·

  6. Investigation of the Crystallization Stages of LTA‐Type Zeolite by Complementary Characterization Techniques

    European Journal of Inorganic Chemistry · 2003-12-01

    M. Smaïhi, Olivier Barida, Valentin Valtchev

    Read original paper ↗ ·

  7. Local Order of Amorphous Zeolite Precursors from 29Si{H} CPMAS and 27Al and 23Na MQMAS NMR and Evidence for the Nature of Medium-Range Order from Neutron Diffraction

    The Journal of Physical Chemistry B · 2004-05-21

    Huaixin Yang, Richard I. Walton, Sasa Antonijevic, Stephen Wimperis, Alex C. Hannon

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  8. Recent developments in metal–organic framework chemistry: design, discovery, permanent porosity and flexibility

    Microporous and Mesoporous Materials · 2004-06-21

    Matthew J. Rosseinsky

    Read original paper ↗ ·

  9. Transmission Electron Microscopy Study of the Formation of FAU-Type Zeolite at Room Temperature

    The Journal of Physical Chemistry B · 2004-09-11

    Valentin Valtchev, Krassimir N. Bozhilov

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  10. Observation and Reactivity of the Chainlike Species ([Al(PO4)2]3-)n during the X-ray Diffraction Investigation of the Hydrothermal Synthesis of the Super-sodalite Sodium Aluminophosphate MIL-74 (Na2Al7(PO4)12·4trenH3·Na(H2O)16)

    The Journal of Physical Chemistry B · 2004-11-24

    Thierry Loiseau, L. Beitone, Franck Millange, Françis Taulelle, Dermot M. O'Hare, Gérard Férey

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  11. Room temperature synthesis: an efficient way for studying the zeolite formation

    Studies in surface science and catalysis · 2005-01-01

    Valentin Valtchev, Krassimir N. Bozhilov, M. Smaïhi, Lubomira Tosheva

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  12. Metal−Organic Frameworks from Homometallic Chains of Nickel(II) and 1,4-Cyclohexanedicarboxylate Connectors: Ferrimagnet−Ferromagnet Transformation

    Inorganic Chemistry · 2006-01-18

    Mohamedally Kurmoo, Hitoshi Kumagai, Motoko Akita-Tanaka, Katsuya Inoue, Seishi Takagi

    Read original paper ↗ ·

  13. In-situ XRD as a tool to understanding zeolite crystallization

    Current Opinion in Colloid & Interface Science · 2006-01-28

    Poul Norby

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  14. Incorporation of Li into MnOOH: An In Situ X-ray and Neutron Diffraction Study

    Chemistry of Materials · 2006-07-18

    Gareth R. Williams, Alexander J. Norquist, Dermot M. O'Hare

    Read original paper ↗ ·

  15. In-situ ultrasonic methods for monitoring the hydrothermal synthesis of LTA-type zeolite from colloidal solutions

    Studies in surface science and catalysis · 2007-01-01

    Hasan Baser, T. Selvam, Jimmy Ofili, Ralph Herrmann, Wilhelm Schwieger

    Read original paper ↗ ·

  16. A Comparative Investigation of Co2+ and Mn2+ Incorporation into Aluminophosphates by in Situ XAS and DFT Computation

    The Journal of Physical Chemistry A · 2007-02-02

    Mei Dong, Guofu Wang, Zhangfeng Qin, Jianguo Wang, Tao Liu, Shuping Yuan, Haijun Jiao

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  17. Crystallization of AlPO4-5 Aluminophosphate Molecular Sieve Prepared in Fluoride Medium: A Multinuclear Solid-State NMR Study

    The Journal of Physical Chemistry B · 2007-05-27

    Jun Xu, Lei Chen, Danlin Zeng, Jun Yang, Minjin Zhang, Chaohui Ye, Feng Deng

    Read original paper ↗ ·

  18. Study of the microstructure of amorphous aluminosilicate gel before and after its hydrothermal treatment

    Microporous and Mesoporous Materials · 2007-07-20

    Cleo Kosanović, Sanja Bosnar, Boris Subotić, Vesna Svetličić, Tea Mišić Radić, Goran Dražić, K. Havancsák

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  19. Examining the Self-Assembly of Microporous Material AlPO4-11 by Dry-Gel Conversion

    The Journal of Physical Chemistry C · 2007-10-01

    Banghao Chen, Yining Huang

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  20. The influences of the way of preparation of Me-aluminosilicates (Me=Li, Na, K, Rb and Cs) on the products

    Microporous and Mesoporous Materials · 2007-12-04

    Cleo Kosanović, Sanja Bosnar, Boris Subotić, Nataša Novak Tušar, Alenka Ristić, Roman Gabrovšek, Venčeslav Kaučič

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  21. Neutron Scattering

    Handbook of Heterogeneous Catalysis · 2008-02-21

    H. Jobic

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  22. Crystallization of magnesium substituted aluminophosphate of type-36 as studied by solid-state NMR spectroscopy

    Microporous and Mesoporous Materials · 2008-03-05

    Jun Xu, Dan Zhou, Xiaowei Song, Lei Chen, Jihong Yu, Chaohui Ye, Feng Deng

    Read original paper ↗ ·

  23. Investigation of Crystallization of Molecular Sieve AlPO4-5 by the Dry Gel Conversion Method

    The Journal of Physical Chemistry C · 2009-08-18

    Banghao Chen, Christopher W. Kirby, Yining Huang

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  24. Tracking the formation of cobalt substituted ALPO-5 using simultaneous in situ X-ray diffraction and X-ray absorption spectroscopy techniques

    Physical Chemistry Chemical Physics · 2009-11-13

    Kerry Simmance, Gopinathan Sankar, Robert G. Bell, Carmelo Prestipino, Wouter van Beek

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  25. Kinetic Analysis of Isothermal Crystallization of Potassium Aluminosilicate Ceramics (Leucite and Kalsilite) from Amorphous Potassium Aluminosilicate Precursors

    Crystal Growth & Design · 2010-01-12

    Iva Buljan, Cleo Kosanović, Boris Subotić, Nataša Novak Tušar, Alenka Ristić, Roman Gabrovšek, Venčeslav Kaučič, Tea Mišić Radić

    Read original paper ↗ ·

  26. Influence of reaction conditions on the properties of sodium alumino silicate synthesized by simultaneous addition of precursors

    Journal of Non-Crystalline Solids · 2010-05-31

    Askwar Hamanjida Hilonga, Jong-Kil Kim, Pradip Bhikaji Sarawade, Hee Taik Kim

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  27. A time-resolved diffraction study of a window of stability in the synthesis of a copper carboxylate metal–organic framework

    CrystEngComm · 2010-10-01

    Franck Millange, Racha El Osta, Manuela E. Medina, Richard I. Walton

    Read original paper ↗ ·

  28. Nascent zeolite frameworks grown from amorphous gels – identification and prospects for crystal engineering

    Zeitschrift für Kristallographie · 2010-11-19

    Douglas L. Dorset

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  29. Alkali Hydrothermal Synthesis of Zeolite A Using Oxide By-products

    ISIJ International · 2011-01-01

    Taichi Murakami, Yoshiyuki Sugano, Tsunetoshi Kinami, Takayuki Narushima, Yasutaka Iguchi, Chiaki Ouchi

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  30. Synthesis, Structure, and Crystallization Study of a Layered Lithium Thiophene-Dicarboxylate

    Crystal Growth & Design · 2012-01-19

    Racha El Osta, Michel Frigoli, Jérôme Marrot, Manuela E. Medina, Richard I. Walton, Franck Millange

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  31. Neutron Scattering

    Unknown journal · 2012-04-04

    H. Jobic

    Read original paper ↗ ·

  32. Copper Phosphonatoethanesulfonates: Temperature Dependent in Situ Energy Dispersive X-ray Diffraction Study and Influence of the pH on the Crystal Structures

    Inorganic Chemistry · 2012-11-09

    Mark Feyand, Annika Hübner, André Rothkirch, David Stephen Wragg, Norbert Stock

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  33. Neutron Scattering forIn‐situCharacterization of Heterogeneous Catalysis

    Unknown journal · 2013-06-10

    Ashfia Huq, Wei‐Ren Chen

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  34. In Situ Studies of Solvothermal Synthesis of Energy Materials

    ChemSusChem · 2014-03-05

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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  35. Präparationsprinzipien mikroporöser Materialien: Vom building block zum hierarchisch aufgebauten porösen System

    Chemie Ingenieur Technik · 2016-02-10

    Wilhelm Schwieger, Michael Klumpp, Shaeel Ahmed Al-Thabaiti, Martin Hartmann

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  36. In SituStudies of the Crystallization of Metal-Organic Frameworks

    Wiley-VCH eBooks · 2016-06-16

    Richard I. Walton, Franck Millange

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  37. Solid-State NMR Studies of Zeolites and Zeotype Materials Synthesis

    Lecture notes in chemistry · 2019-01-01

    Jun Xu, Qiang Wang, Shenhui Li, Feng Deng

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  38. In situ scattering studies of material formation during wet-chemical syntheses

    Elsevier eBooks · 2021-08-04

    Susanne Linn Skjærvø, Mikkel Juelsholt, Kirsten M. Ø. Jensen

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  39. Panoramic (in beam) studies of materials synthesis

    Elsevier eBooks · 2021-10-12

    Mercouri G. Kanatzidis, Rebecca McClain

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  40. In Situ and In Operando Neutron Diffraction of Transition Metal Oxides for Electrochemical Storage

    Unknown journal · 2022-04-08

    Christophe Didier, Zhanhu Guo, Bohang Song, Ashfia Huq, Vanessa Kate Peterson

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  41. Solvothermal and hydrothermal methods for preparative solid-state chemistry

    Elsevier eBooks · 2022-11-25

    Richard I. Walton

    Read original paper ↗ ·

  42. Direct Correlation of the Crystalline Phases of La 0.9 Sr 0.1 Co 1– y Fe y O 3−δ with the Partial Oxidation of Methane via In Situ Neutron and Synchrotron Diffraction

    ACS Materials Au · 2025-04-17

    Dennis D. Nguyen, Mara J. Milhander, Elizabeth M. Hitch, Dmitri Leo Mesoza Cordova, J. Jimenez, Juana Mora, Daniel Sandoval, Maxx Q. Arguilla, Allyson M. Fry‐Petit

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