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RESEARCH PAPER · Faraday Discussions · 2002

Recent results from the in situ study of hydrothermal crystallisations using time-resolved X-ray and neutron diffraction methods

Richard I. Walton, Alexander J. Norquist, Ronald I. Smith, Dermot O’Hare

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Recent results from the in situ study of hydrothermal crystallisations using time-resolved X-ray and neutron diffraction methodsOriginalSample containment for neutron and high-energy x-ray scattering studies of hydrogen fluoride and related molecular species11Kinetic and Mechanistic Investigations of Hydrothermal Transformations in Zinc Phosphates64The use of neutron scattering in the study of ceramics11Hydrothermal reversible interconversion of two zincophosphates with three-dimensional open frameworks containing diprotonated 1,4-diazacycloheptane molecules6High pressurein situx-ray absorption spectroscopy cell for studying simultaneously the liquid phase and the solid/liquid interface68The use of softer X-rays in the structure elucidation of microporous materials8Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques105Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken24Neutron Scattering and Diffraction Studies of Fluids and Fluid-Solid Interactions62In-situ XRD as a tool to understanding zeolite crystallization105A Combined SAXS/WAXS/XAFS Setup Capable of Observing Concurrent Changes Across the Nano-to-Micrometer Size Range in Inorganic Solid Crystallization Processes113A synchrotron radiation study of the hydrothermal synthesis of layered double hydroxides from MgO and Al2O3 slurries37In-situ ultrasonic methods for monitoring the hydrothermal synthesis of LTA-type zeolite from colloidal solutions9Watching the crystallisation of complex oxides by in situ X-ray techniques28Synthesis and Structural Determination of Four Novel Metal−Organic Frameworks in a Zn−3-Amino-1,2,4-Triazole System51Viscosity sensing in heated alkaline zeolite synthesis media24Preparation of SrTiO3-supported TiO2 photocatalyst34Recent progress in the use of in situ X-ray methods for the study of heterogeneous catalysts in packed-bed capillary reactors29Synthesis, Structure, and Transformation Studies in a Family of Inorganic−Organic Hybrid Framework Structures Based on Indium36Formation and Annealing of BaTiO3 and SrTiO3 Nanoparticles in KOH Solution30Hybridized Nanowires and Cubes: A Novel Architecture of a Heterojunctioned TiO 2 /SrTiO 3 Thin Film for Efficient Water Splitting311Catalyst Characterization—Heterogeneous2Structure, Size, and Morphology Control of Nanocrystalline Lithium Cobalt Oxide25In‐Situ Monitoring of the Formation of Crystalline Solids251In‐situ‐Verfolgung der Bildung kristalliner Feststoffe69Hierarchical assembly of immobilized TiO2-based nanostructured epitaxial films on Ti Substrates for photocatalytic water decontamination and hydrogen generation0Steric-Induced Layer Flection in Templated Vanadium Tellurites11Tailored SrTiO 3 /TiO 2 heterostructures for dye-sensitized solar cells with enhanced photoelectric conversion performance84Pursuing the Crystallization of Mono- and Polymetallic Nanosized Crystalline Inorganic Compounds by Low-Temperature Wet-Chemistry and Colloidal Routes80Facile Low Temperature Hydrothermal Synthesis of BaTiO3 Nanoparticles Studied by In Situ X-ray Diffraction21Nuclear Magnetic Resonance Spectroscopy for In Situ Monitoring of Porous Materials Formation under Hydrothermal Conditions32In situ scattering studies of material formation during wet-chemical syntheses1Solvothermal synthesis of zirconia nanomaterials: Latest developments and future45

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  1. Sample containment for neutron and high-energy x-ray scattering studies of hydrogen fluoride and related molecular species

    Review of Scientific Instruments · 2003-09-25

    John F. Turner, Sylvia E. McLain, Timothy H. Free, Chris J. Benmore, Kenneth W. Herwig, Joan E. Siewenie

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  2. Kinetic and Mechanistic Investigations of Hydrothermal Transformations in Zinc Phosphates

    Journal of the American Chemical Society · 2004-05-08

    Alexander J. Norquist, Dermot O’Hare

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  3. The use of neutron scattering in the study of ceramics

    Journal of Materials Science · 2004-10-23

    S. M. Bennington

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  4. Hydrothermal reversible interconversion of two zincophosphates with three-dimensional open frameworks containing diprotonated 1,4-diazacycloheptane molecules

    Journal of Solid State Chemistry · 2005-02-15

    Michael Wiebcke, Clemens Kühn, Gerhard Wildermuth

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  5. High pressurein situx-ray absorption spectroscopy cell for studying simultaneously the liquid phase and the solid/liquid interface

    Review of Scientific Instruments · 2005-04-29

    Jan‐Dierk Grunwaldt, Michael Ramin, Markus Rohr, Alexej Michailovski, Greta Ricarda Patzke, Alfons Baiker

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  6. The use of softer X-rays in the structure elucidation of microporous materials

    Journal of Synchrotron Radiation · 2005-06-15

    Madeleine Helliwell, Richard H. Jones, Venčeslav Kaučič, Nataša Zabukovec Logar

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  7. Studying the Solvothermal Formation of MoO3 Fibers by Complementary In Situ EXAFS/EDXRD Techniques

    Angewandte Chemie International Edition · 2005-08-02

    Alexej Michailovski, Jan‐Dierk Grunwaldt, Alfons Baiker, Ragnar Kiebach, Wolfgang Bensch, Greta Ricarda Patzke

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  8. Untersuchung der solvothermalen Bildung von MoO3‐Fasern mithilfe komplementärer In‐situ‐EXAFS/EDXRD‐Techniken

    Angewandte Chemie · 2005-08-02

    Alexej Michailovski, Jan‐Dierk Grunwaldt, Alfons Baiker, Ragnar Kiebach, Wolfgang Bensch, Greta Ricarda Patzke

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  9. Neutron Scattering and Diffraction Studies of Fluids and Fluid-Solid Interactions

    Reviews in Mineralogy and Geochemistry · 2006-01-01

    D. R. Cole, Kenneth W. Herwig, Eugene Mamontov, John Z. Larese

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  10. In-situ XRD as a tool to understanding zeolite crystallization

    Current Opinion in Colloid & Interface Science · 2006-01-28

    Poul Norby

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  11. A Combined SAXS/WAXS/XAFS Setup Capable of Observing Concurrent Changes Across the Nano-to-Micrometer Size Range in Inorganic Solid Crystallization Processes

    Journal of the American Chemical Society · 2006-08-31

    Andrew Michael Beale, Ad M. J. van der Eerden, Simon D. M. Jacques, Olivier Leynaud, Matthew G. O’Brien, Florian Meneau, S. G. Nikitenko, Wim Bras, Bert Marc Weckhuysen

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  12. A synchrotron radiation study of the hydrothermal synthesis of layered double hydroxides from MgO and Al2O3 slurries

    Green Chemistry · 2007-01-01

    Sharon Mitchell, Timothy Tiwonge Biswick, William Jones, Gareth R. Williams, Dermot O’Hare

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  13. In-situ ultrasonic methods for monitoring the hydrothermal synthesis of LTA-type zeolite from colloidal solutions

    Studies in surface science and catalysis · 2007-01-01

    Hasan Baser, T. Selvam, Jimmy Ofili, Ralph Herrmann, Wilhelm Schwieger

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  14. Watching the crystallisation of complex oxides by in situ X-ray techniques

    Applied Catalysis A General · 2007-03-04

    Andrew Michael Beale, Lee M. Reilly, Gopinathan Sankar

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  15. Synthesis and Structural Determination of Four Novel Metal−Organic Frameworks in a Zn−3-Amino-1,2,4-Triazole System

    Crystal Growth & Design · 2007-06-08

    Hyunsoo Park, Gabriel Krigsfeld, Simon J. Teat, John B. Parise

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  16. Viscosity sensing in heated alkaline zeolite synthesis media

    Physical Chemistry Chemical Physics · 2008-12-24

    Lana R. A. Follens, Erwin Konrad Reichel, Christian Riesch, Jan Vermant, Johan A. Martens, Christine E. A. Kirschhock, Bernhard Jakoby

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  17. Preparation of SrTiO3-supported TiO2 photocatalyst

    Materials Science and Engineering B · 2008-12-28

    Tomoki Tsumura, Kazuo Sogabe, Masahiro Toyoda

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  18. Recent progress in the use of in situ X-ray methods for the study of heterogeneous catalysts in packed-bed capillary reactors

    Catalysis Today · 2009-03-23

    Simon D. M. Jacques, Olivier Leynaud, D. Strusevich, Paul Stukas, Paul Barnes, Gopinathan Sankar, Mike Sheehy, Matthew G. O’Brien, Ana Iglesias‐Juez, Andrew Michael Beale

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  19. Synthesis, Structure, and Transformation Studies in a Family of Inorganic−Organic Hybrid Framework Structures Based on Indium

    Inorganic Chemistry · 2009-11-13

    Padmini Ramaswamy, N.N. Hegde, Ramanath Prabhu, V.M. Vidya, Ayan Datta, Srinivasan Natarajan

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  20. Formation and Annealing of BaTiO3 and SrTiO3 Nanoparticles in KOH Solution

    Journal of Material Science and Technology · 2010-01-01

    Tomoki Tsumura, Keiichi Matsuoka, Masahiro Toyoda

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  21. Hybridized Nanowires and Cubes: A Novel Architecture of a Heterojunctioned TiO 2 /SrTiO 3 Thin Film for Efficient Water Splitting

    Advanced Functional Materials · 2010-10-20

    Jiawei Ng, Shiping Xu, Xiwang Zhang, Hui Ying Yang, Darren Delai Sun

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  22. Catalyst Characterization—Heterogeneous

    Encyclopedia of Catalysis · 2010-11-15

    Eli Stavitski, Andrew Michael Beale, Bert Marc Weckhuysen

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  23. Structure, Size, and Morphology Control of Nanocrystalline Lithium Cobalt Oxide

    Crystal Growth & Design · 2011-01-20

    Kirsten M. Ø. Jensen, Mogens Christensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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  24. In‐Situ Monitoring of the Formation of Crystalline Solids

    Angewandte Chemie International Edition · 2011-02-15

    Nicole Pienack, Wolfgang Bensch

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  25. In‐situ‐Verfolgung der Bildung kristalliner Feststoffe

    Angewandte Chemie · 2011-02-15

    Nicole Pienack, Wolfgang Bensch

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  26. Hierarchical assembly of immobilized TiO2-based nanostructured epitaxial films on Ti Substrates for photocatalytic water decontamination and hydrogen generation

    Unknown journal · 2012-01-01

    Jiawei Ng

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  27. Steric-Induced Layer Flection in Templated Vanadium Tellurites

    Crystal Growth & Design · 2013-04-02

    Kelvin B. Chang, Matthew D. Smith, Samuel M. Blau, Ethan C. Glor, Mat­thias Zeller, Joshua Schrier, Alexander J. Norquist

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  28. Tailored SrTiO 3 /TiO 2 heterostructures for dye-sensitized solar cells with enhanced photoelectric conversion performance

    Journal of Materials Chemistry A · 2015-01-01

    Enyan Guo, Longwei Yin

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  29. Pursuing the Crystallization of Mono- and Polymetallic Nanosized Crystalline Inorganic Compounds by Low-Temperature Wet-Chemistry and Colloidal Routes

    Chemical Reviews · 2015-09-25

    Stefano Diodati, Paolo Dolcet, Maurizio Casarin, Silvia Gross

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  30. Facile Low Temperature Hydrothermal Synthesis of BaTiO3 Nanoparticles Studied by In Situ X-ray Diffraction

    Crystals · 2018-06-17

    Ola G. Grendal, Anders B. Blichfeld, Susanne Linn Skjærvø, Wouter van Beek, Sverre M. Selbach, Tor Grande, Mari‐Ann Einarsrud

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  31. Nuclear Magnetic Resonance Spectroscopy for In Situ Monitoring of Porous Materials Formation under Hydrothermal Conditions

    Materials · 2018-08-12

    Mohamed Haouas

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  32. In situ scattering studies of material formation during wet-chemical syntheses

    Elsevier eBooks · 2021-08-04

    Susanne Linn Skjærvø, Mikkel Juelsholt, Kirsten M. Ø. Jensen

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  33. Solvothermal synthesis of zirconia nanomaterials: Latest developments and future

    Ceramics International · 2022-08-06

    Lu Liu, Shuzhong Wang, Guanyu Jiang, Baoquan Zhang, Jianqiao Yang, Jinglong Wang, Wei Liu, Yanhui Li, Hui Liu

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