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RESEARCH PAPER · Green Chemistry · 2007

A synchrotron radiation study of the hydrothermal synthesis of layered double hydroxides from MgO and Al2O3 slurries

Sharon Mitchell, Timothy Tiwonge Biswick, William Jones, Gareth R. Williams, Dermot M. O'Hare

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A synchrotron radiation study of the hydrothermal synthesis of layered double hydroxides from MgO and Al2O3 slurriesOriginalNano/Microporous Materials: Nanostructured Layered Double Hydroxides0The application of focused microwave irradiation coupled with freeze drying to investigate the reaction of MgO and Al2O3 slurries in the formation of layered double hydroxides9Facile synthesis of Zn-Al layered double hydroxide from aqueous suspension of zinc oxide and aluminum hydroxide11High‐Pressure, High‐Temperature Formation of Phase‐Pure Monoclinic Zirconia Nanocrystals Studied by Time‐Resolved in situ Synchrotron X‐Ray Diffraction57Comparative study of the synthesis of layered transition metal molybdates26Efficient synthesis of ordered organo-layered double hydroxides31Antireflection/antifogging coatings based on nanoporous films derived from layered double hydroxide35Polytype Selection by Intercalated Anions: Design and Synthesis of the 3R2 Polytype of the Layered Double Hydroxide of Zn and Al20Nano/Microporous Materials: Nanostructured Layered Double Hydroxides3A structured catalyst based on cobalt phthalocyanine/calcined Mg–Al hydrotalcite film for the oxidation of mercaptan50Rapid Hydrothermal Preparation of Rutile TiO2 Nanoparticles by Simultaneous Transformation of Primary Brookite and Anatase: An in Situ Synchrotron PXRD Study45A kinetic and mechanistic study into the formation of the Cu–Cr layered double hydroxide14In situ synchrotron powder X-ray diffraction study of formation and growth of yttrium and ytterbium aluminum garnet nanoparticles in sub- and supercritical water16Ultrasonic-assisted synthesis and characterization of layered double hydroxides intercalated with bioactive N,N′-(pyromellitoyl)-bis-l-α-amino acids55Alkali- and nitrate-free synthesis of highly active Mg–Al hydrotalcite-coated alumina for FAME production46A Structured Catalyst toward Mercaptan Sweetening with Largely Enhanced Synergistic Effect12In Situ Studies of Solvothermal Synthesis of Energy Materials159In Situ X‑ray Diffraction Study of the Formation, Growth, and Phase Transition of Colloidal Cu2– x S Nanocrystals61TiO 2 @Layered Double Hydroxide Core–Shell Nanospheres with Largely Enhanced Photocatalytic Activity Toward O 2 Generation263Development of a new in situ analysis technique applying luminescence of local coordination sensors: principle and application for monitoring metal-ligand exchange processes23The fabrication of oriented organic–inorganic ultrathin films with enhanced electrochromic properties20Ultrahigh-rate-capability of a layered double hydroxide supercapacitor based on a self-generated electrolyte reservoir67Hydrothermal Synthesis of CoSb2O4: In Situ Powder X-ray Diffraction, Crystal Structure, and Electrochemical Properties29Synthesis and Characterization of a [Li0+xMg2-2xAl1+x(OH)6][Cl·mH2O] Solid Solution with X = 0 - 1 at Different Temperatures1Facile preparation methods of hydrotalcite layered materials and their structural characterization by combined techniques99Green synthesis of hydrotalcite from untreated magnesium oxide and aluminum hydroxide43Hydrotalcite-Derived Mixed Oxides for the Synthesis of a Key Vitamin A Intermediate Reducing Waste11Hydrotalcite and hydrocalumite as resources from waste materials of concrete aggregate and Al-dross by microwave-hydrothermal process32Preparation of Layered Double Hydroxides toward Precisely Designed Hierarchical Organization92In situ scattering studies of material formation during wet-chemical syntheses1Efficient, scalable, closed-loop synthesis of highly crystalline pure phase MgAl-layered double hydroxides intercalated with hydroxyl anions11Calcium/iron-layered double hydroxides-sodium alginate for removal of tetracycline antibiotic from aqueous solution51Detailed insights into the formation pathway of CdS and ZnS in solution: a multi-modal in situ characterisation approach9High efficiency dye-sensitized solar cells with a novel two dimensional Cd-V-LDH photoanode15Hybridization of layered double hydroxides with functional particles7Optimization of Mg–Al Layered Double Hydroxide Film Preparation and Corrosion Resistance Study on AZ91D Mg Alloy by Multivariate Polynomial Regression Fitting4Novel green synthesis and transformation mechanism of layered double hydroxides from metal hydroxides and light magnesium carbonate0

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  1. Nano/Microporous Materials: Nanostructured Layered Double Hydroxides

    Encyclopedia of Inorganic Chemistry · 2005-09-07

    Fabrice Leroux, Vanessa Prévot

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  2. The application of focused microwave irradiation coupled with freeze drying to investigate the reaction of MgO and Al2O3 slurries in the formation of layered double hydroxides

    Green Chemistry · 2008-01-01

    Sharon Mitchell, Ian R. Baxendale, William Jones

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  3. Facile synthesis of Zn-Al layered double hydroxide from aqueous suspension of zinc oxide and aluminum hydroxide

    Journal of the Ceramic Society of Japan · 2009-01-01

    Makoto Ogawa, Yu SUGIYAMA

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  4. High‐Pressure, High‐Temperature Formation of Phase‐Pure Monoclinic Zirconia Nanocrystals Studied by Time‐Resolved in situ Synchrotron X‐Ray Diffraction

    Advanced Materials · 2009-05-12

    Martin Bremholm, Jacob Becker, Bo B. Iversen

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  5. Comparative study of the synthesis of layered transition metal molybdates

    Journal of Solid State Chemistry · 2009-10-29

    Sharon Mitchell, Almudena Gómez‐Avilés, Catherine E. Gardner, William Jones

    Read original paper ↗ ·

  6. Efficient synthesis of ordered organo-layered double hydroxides

    Green Chemistry · 2010-01-01

    H. Chris Greenwell, William Jones, S.L. Rugen-Hankey, Peter J. Holliman, Richard L. Thompson

    Read original paper ↗ ·

  7. Antireflection/antifogging coatings based on nanoporous films derived from layered double hydroxide

    Chemical Engineering Journal · 2011-03-08

    Jingbin Han, Yibo Dou, Min Wei, David G. Evans, Xue Duan

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  8. Polytype Selection by Intercalated Anions: Design and Synthesis of the 3R2 Polytype of the Layered Double Hydroxide of Zn and Al

    Crystal Growth & Design · 2011-04-21

    S. Radha, Srinivasa V. Prasanna, P. Vishnu Kamath

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  9. Nano/Microporous Materials: Nanostructured Layered Double Hydroxides

    Encyclopedia of Inorganic and Bioinorganic Chemistry · 2011-12-09

    Fabrice Leroux, Vanessa Prévot

    Read original paper ↗ ·

  10. A structured catalyst based on cobalt phthalocyanine/calcined Mg–Al hydrotalcite film for the oxidation of mercaptan

    Green Chemistry · 2012-01-01

    Zhiyong Sun, Lan Jin, Shan He, Yufei Zhao, Min Wei, David G. Evans, Xue Duan

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  11. Rapid Hydrothermal Preparation of Rutile TiO2 Nanoparticles by Simultaneous Transformation of Primary Brookite and Anatase: An in Situ Synchrotron PXRD Study

    Crystal Growth & Design · 2012-10-24

    Jianli Mi, Casper Clausen, Martin Bremholm, Nina Lock, Kirsten M. Ø. Jensen, Mogens Christensen, Bo B. Iversen

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  12. A kinetic and mechanistic study into the formation of the Cu–Cr layered double hydroxide

    Physical Chemistry Chemical Physics · 2013-01-01

    Gareth R. Williams, Alexander E. Clout, J. Burley

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  13. In situ synchrotron powder X-ray diffraction study of formation and growth of yttrium and ytterbium aluminum garnet nanoparticles in sub- and supercritical water

    RSC Advances · 2013-01-01

    Peter Nørby, Kirsten M. Ø. Jensen, Nina Lock, Mogens Christensen, Bo B. Iversen

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  14. Ultrasonic-assisted synthesis and characterization of layered double hydroxides intercalated with bioactive N,N′-(pyromellitoyl)-bis-l-α-amino acids

    RSC Advances · 2013-01-01

    Shadpour E Mallakpour, Mohammad Dinari, Vajiheh Behranvand

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  15. Alkali- and nitrate-free synthesis of highly active Mg–Al hydrotalcite-coated alumina for FAME production

    Catalysis Science & Technology · 2014-01-01

    Julia J. Creasey, Alessandro Chieregato, Jinesh Cherukkattu Manayil, Christopher M. A. Parlett, Karen Wilson, Adam Fraser Lee

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  16. A Structured Catalyst toward Mercaptan Sweetening with Largely Enhanced Synergistic Effect

    Industrial & Engineering Chemistry Research · 2014-03-04

    Zhiyong Sun, Lan Jin, Yufei Zhao, Shan He, Shuangde Li, Min Wei, Liren Wang

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  17. In Situ Studies of Solvothermal Synthesis of Energy Materials

    ChemSusChem · 2014-03-05

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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  18. In Situ X‑ray Diffraction Study of the Formation, Growth, and Phase Transition of Colloidal Cu2– x S Nanocrystals

    ACS Nano · 2014-04-09

    Peter Nørby, Simon Johnsen, Bo B. Iversen

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  19. TiO 2 @Layered Double Hydroxide Core–Shell Nanospheres with Largely Enhanced Photocatalytic Activity Toward O 2 Generation

    Advanced Functional Materials · 2015-02-25

    Yibo Dou, Shitong Zhang, Ting Pan, Simin Xu, Awu Zhou, Min Pu, Hong Juan Yan, Jingbin Han, Min Wei, David G. Evans, Xue Duan

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  20. Development of a new in situ analysis technique applying luminescence of local coordination sensors: principle and application for monitoring metal-ligand exchange processes

    The Analyst · 2016-01-01

    Huayna Terraschke, Laura Ruiz Arana, Patric Lindenberg, Wolfgang Bensch

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  21. The fabrication of oriented organic–inorganic ultrathin films with enhanced electrochromic properties

    Journal of Materials Chemistry C · 2016-01-01

    Awu Zhou, Xiaoxi Liu, Yibo Dou, Shanyue Guan, Jingbin Han, Min Wei

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  22. Ultrahigh-rate-capability of a layered double hydroxide supercapacitor based on a self-generated electrolyte reservoir

    Journal of Materials Chemistry A · 2016-01-01

    Xiaoxi Liu, Awu Zhou, Ting Pan, Yibo Dou, Mingfei Shao, Jingbin Han, Min Wei

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  23. Hydrothermal Synthesis of CoSb2O4: In Situ Powder X-ray Diffraction, Crystal Structure, and Electrochemical Properties

    Crystal Growth & Design · 2016-01-05

    Peter Nørby, Martin Roelsgaard, Martin Søndergaard, Bo B. Iversen

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  24. Synthesis and Characterization of a [Li0+xMg2-2xAl1+x(OH)6][Cl·mH2O] Solid Solution with X = 0 - 1 at Different Temperatures

    Natural Resources · 2017-01-01

    Anton Niksch, Holger Pollmann

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  25. Facile preparation methods of hydrotalcite layered materials and their structural characterization by combined techniques

    Inorganica Chimica Acta · 2017-08-09

    Eleonora Conterosito, Valentina Gianotti, Luca Palin, Enrico Boccaleri, Davide Viterbo, Marco Milanesio

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  26. Green synthesis of hydrotalcite from untreated magnesium oxide and aluminum hydroxide

    Green Chemistry Letters and Reviews · 2018-01-02

    Frederick J. W. J. Labuschagné, A. Wiid, H. P. Venter, Bianca R. Gevers, Andreas Leuteritz

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  27. Hydrotalcite-Derived Mixed Oxides for the Synthesis of a Key Vitamin A Intermediate Reducing Waste

    ACS Omega · 2018-11-12

    Ferdy J. A. G. Coumans, Sharon Mitchell, Jan Schütz, Jonathan Medlock, Javier Pérez‐Ramírez

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  28. Hydrotalcite and hydrocalumite as resources from waste materials of concrete aggregate and Al-dross by microwave-hydrothermal process

    Construction and Building Materials · 2019-02-22

    Fawzia Abd EL-Raoof, Ahmed Tawfik, Sridhar Komarneni, S. E. Ahmed

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  29. Preparation of Layered Double Hydroxides toward Precisely Designed Hierarchical Organization

    ChemEngineering · 2019-08-01

    Rattanawadee Ploy Wijitwongwan, Soontaree Intasa-ard, Makoto Ogawa

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  30. In situ scattering studies of material formation during wet-chemical syntheses

    Elsevier eBooks · 2021-08-04

    Susanne Linn Skjærvø, Mikkel Juelsholt, Kirsten M. Ø. Jensen

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  31. Efficient, scalable, closed-loop synthesis of highly crystalline pure phase MgAl-layered double hydroxides intercalated with hydroxyl anions

    Dalton Transactions · 2021-12-16

    Luofu Min, Jingying Duan, Lu Liu, Sheng Ge, Wen Zhang, Yuxin Wang

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  32. Calcium/iron-layered double hydroxides-sodium alginate for removal of tetracycline antibiotic from aqueous solution

    Alexandria Engineering Journal · 2022-08-04

    Marwa F. Abed, Ayad A.H. Faisal

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  33. Detailed insights into the formation pathway of CdS and ZnS in solution: a multi-modal in situ characterisation approach

    Physical Chemistry Chemical Physics · 2022-12-19

    Jonas Ströh, Thomas C. Hess, L. Ohrt, Harald Fritzsch A, Martin Etter, Ann‐Christin Dippel, Linda Dyorisse Nyamen, Huayna Terraschke

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  34. High efficiency dye-sensitized solar cells with a novel two dimensional Cd-V-LDH photoanode

    Frontiers in Materials · 2023-09-07

    Samar H. Bendary, Amira A. Hashem, Sawsan A. Mahmoud

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  35. Hybridization of layered double hydroxides with functional particles

    Dalton Transactions · 2024-01-01

    Rattanawadee Ploy Wijitwongwan, Soontaree Intasa-ard, Makoto Ogawa

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  36. Optimization of Mg–Al Layered Double Hydroxide Film Preparation and Corrosion Resistance Study on AZ91D Mg Alloy by Multivariate Polynomial Regression Fitting

    ACS Omega · 2024-04-19

    Chengfeng Wang, Bofan Liu, Pengxu Wei, Kepei Xie, Yu Chen, Meifeng Wang, Xiaoqing Du, Dongchu Chen

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  37. Novel green synthesis and transformation mechanism of layered double hydroxides from metal hydroxides and light magnesium carbonate

    Journal of Solid State Chemistry · 2026-01-20

    Yuman Guo, Qian Zhang, He Zhou, Christine Taviot‐Guého, Fabrice Leroux, Yongjun Feng

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