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RESEARCH PAPER · Journal of the American Chemical Society · 2006

A Combined SAXS/WAXS/XAFS Setup Capable of Observing Concurrent Changes Across the Nano-to-Micrometer Size Range in Inorganic Solid Crystallization Processes

Andrew Michael Beale, Ad M. J. van der Eerden, Simon D. M. Jacques, Olivier Leynaud, Matthew G. O’Brien, Florian Meneau, S. G. Nikitenko, Wim Bras, Bert Marc Weckhuysen

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A Combined SAXS/WAXS/XAFS Setup Capable of Observing Concurrent Changes Across the Nano-to-Micrometer Size Range in Inorganic Solid Crystallization ProcessesOriginalPorous solids get organized27Designed open-structure heterogeneous catalysts for the synthesis of fine chemicals and pharmaceuticals11In situ studies of the crystallisation of microporous materials using synchrotron radiation based X-ray techniques0Insight into the structure of supported palladium catalysts during the total oxidation of methane125New insights into the formation of microporous materials by in situ scattering techniques35The Zeolite Scene – An Overview61Understanding the crystallisation processes leading to the formation of microporous aluminophosphates2Zeolites: physical aspects and environmental applications49Watching the crystallisation of complex oxides by in situ X-ray techniques28Probing in situ the Nucleation and Growth of Gold Nanoparticles by Small-Angle X-ray Scattering258In situsimultaneous Raman/high-resolution X-ray powder diffraction study of transformations occurring in materials at non-ambient conditions52Reactor design for in situ X-ray scattering studies of nanoparticle formation in supercritical water syntheses55Structural Characterization of Frozen n-Heptane Solutions of Metal-Containing Reverse Micelles17Synthesis0Effect of Organic Templates on the Kinetics and Crystallization of Microporous Metal-Substituted Aluminophosphates24IR and Raman Investigation of One-Dimensional and Three-Dimensional Aluminophosphite11Characterization of cement minerals, cements and their reaction products at the atomic and nano scale137Nucleation, Growth, and Aggregation of Mineral Phases: Mechanisms and Kinetic Controls64Synchrotron radiation studies of non-crystalline systems11The competition of organic amines and the phosphorus source on directing the formation of aluminophosphate-based molecular sieves with chabazite structure20Zeolite Mediated Reactions: Mechanistic Aspects and Environmental Applications18Implementation of a combined SAXS/WAXS/QEXAFS set-up for time-resolved in situ experiments261Dynamic “operando” observation of 1 wt% Pd-based TWCs: Simultaneous XAS/DRIFTS/mass spectrometry analysis of the effects of Ce0.5Zr0.5O2 loading on structure, reactivity and performance19Chapter 6 Characterization of Catalysts in Reactive Atmospheres by X‐ray Absorption Spectroscopy98EXAFS spectroscopy as a tool to probe metal–support interaction and surface molecular structures in oxide-supported catalysts: application to Al2O3-supported Ni(ii) complexes and ZrO2-supported tungstates29The Use of Scattering and Spectroscopic Synchrotron Radiation Methods in Materials Science0Local and long range order in promoted iron-based Fischer–Tropsch catalysts: A combined in situ X-ray absorption spectroscopy/wide angle X-ray scattering study179Multi-Technique In Situ Approach Towards the Study of Catalytic Solids at Work Using Synchrotron Radiation4Recent progress in the use of in situ X-ray methods for the study of heterogeneous catalysts in packed-bed capillary reactors29Molecular engineering of microporous crystals: (I) New insight into the formation process of open-framework aluminophosphates26Linking Simultaneous In Situ WAXS/SAXS/Raman with Raman/ATR/UV–vis Spectroscopy: Comprehensive Insight into the Synthesis of Molybdate Catalyst Precursors35Chemische Bildgebung von räumlichen Heterogenitäten in katalytischen Festkörpern auf unterschiedlichen Längen‐ und Zeitskalen81A Combined Multi-Technique In Situ Approach Used to Probe the Stability of Iron Molybdate Catalysts During Redox Cycling21Chemical Imaging of Spatial Heterogeneities in Catalytic Solids at Different Length and Time Scales372Insights into the formation of microporous materials by in situ X-ray scattering techniques21Shining X-rays on catalysts at work16In Situ XAS and XRPD Parametric Rietveld Refinement To Understand Dealumination of Y Zeolite Catalyst205Combined use of XAFS, XRD and TEM to unravel the microstructural evolution of nanostructured ZrO2–SiO2 binary oxides: from nanometres down to the molecular domain21Combining in situ characterization methods in one set-up: looking with more eyes into the intricate chemistry of the synthesis and working of heterogeneous catalysts135Methods for in situ spectroscopic probing of the synthesis of a zeolite112The role of synchrotron radiation in examining the self-assembly of crystalline nanoporous framework materials: from zeolites and aluminophosphates to metal organic hybrids47Spectroscopic set-up for simultaneous UV-Vis/(Q)EXAFSin situandin operandostudies of homogeneous reactions under laboratory conditions35Multitechnique analysis of supported Pd particles upon dynamic, cycling CO/NO conditions: Size-dependence of the structure–activity relationship28Combining Time-Resolved Hard X-ray Diffraction and Diffuse Reflectance Infrared Spectroscopy To Illuminate CO Dissociation and Transient Carbon Storage by Supported Pd Nanoparticles during CO/NO Cycling92Experimental setup forin situX-ray SAXS/WAXS/PDF studies of the formation and growth of nanoparticles in near- and supercritical fluids154Closing the operando gap: The application of high energy photons for studying catalytic solids at work34Properties and applications of Zeolites225Influence of Monomer Feeding on a Fast Gold Nanoparticles Synthesis: Time-Resolved XANES and SAXS Experiments90In Situ X-ray Diffraction and Absorption Studies of the Growth and Phase Transformation of Yttrium Hydroxide Nanotubes to Their Oxide Counterparts16Combined time-resolved SAXS and X-ray Spectroscopy methods9Catalyst Characterization—Heterogeneous2Oxide Nanomaterials: Synthetic Developments, Mechanistic Studies, and Technological Innovations366Oxidische Nanomaterialien: Von der Synthese über den Mechanismus zur technologischen Innovation25Live encapsulation of a Keggin polyanion in NH2-MIL-101(Al) observed by in situ time resolved X-ray scattering62In‐Situ Monitoring of the Formation of Crystalline Solids251In‐situ‐Verfolgung der Bildung kristalliner Feststoffe69On the nucleation and crystallization of silicalite-1 from a dilute clear sol38Probing ZnAPO-34 Self-Assembly Using Simultaneous Multiple in Situ Techniques39Kinetic Control of Metal–Organic Framework Crystallization Investigated by Time‐Resolved In Situ X‐Ray Scattering214Kinetic Control of Metal–Organic Framework Crystallization Investigated by Time‐Resolved In Situ X‐Ray Scattering41Experimental investigation of calcium carbonate mineralogy in past and future oceans2Preparation and helical folding of aromatic polyamides28Small angle X-ray scattering (SAXS) techniques for polymer electrolyte membrane fuel cell characterization9Techniques Coupling for Catalyst Characterisation8Microstructural degeneracy associated with a two-point correlation function and its information content88Review of Pt-Based Bimetallic Catalysis: From Model Surfaces to Supported Catalysts1253Application of Operando XAS, XRD, and Raman Spectroscopy for Phase Speciation in Water Gas Shift Reaction Catalysts68Synchrotron Techniques for In Situ Catalytic Studies: Capabilities, Challenges, and Opportunities136Comparative advantages and limitations of the basic metrology methods applied to the characterization of nanomaterials64Small-Angle X-Ray Scattering for the Study of Nanostructures and Nanostructured Materials4Tracking the structural changes in pure and heteroatom substituted aluminophosphate, AIPO-18, using synchrotron based X-ray diffraction techniques8Keimbildung organischer Kristalle aus molekularer Sichtweise37Nucleation of Organic Crystals—A Molecular Perspective567Characterization of Metal-Oxide Catalysts in Operando Conditions by Combining X-ray Absorption and Raman Spectroscopies in the Same Experiment17Critical review: Effects of complex interactions on structure and dynamics of supported metal catalysts32Low-dimensional systems investigated by x-ray absorption spectroscopy: a selection of 2D, 1D and 0D cases122In Situ Studies of Solvothermal Synthesis of Energy Materials159Determination of the electronic and structural configuration of coordination compounds by synchrotron-radiation techniques109Powder Diffraction and Synchrotron Radiation2Unravelling the Formation of Pt–Ga Alloyed Nanoparticles on Calcined Ga-Modified Hydrotalcites by in Situ XAS36Advanced Elemental Characterization during Pt–In Catalyst Formation by Wavelet Transformed X-ray Absorption Spectroscopy48A flexible gas flow reaction cell for in situ x-ray absorption spectroscopy studies3Small Angle X-ray Scattering for Nanoparticle Research975HEIMDAL: A thermal neutron powder diffractometer with high and flexible resolution combined with SANS and neutron imaging – Designed for materials science studies at the European Spallation Source12Easily Accessible Rare-Earth-Containing Phosphonium Room-Temperature Ionic Liquids: EXAFS, Luminescence, and Magnetic Properties32Characterization of Catalysts5Spatial and temporal exploration of heterogeneous catalysts with synchrotron radiation243Nucleation and crystallization of the MWW-type lamellar zeolitic precursor11Nucleation4Physical design of multipurpose physics neutron diffractometer for the CSNS25Moving Frontiers in Transition Metal Catalysis: Synthesis, Characterization and Modeling50Extended range X-ray pair distribution functions22Spectroscopy, microscopy, diffraction and scattering of archetypal MOFs: formation, metal sites in catalysis and thin films116Monitoring and quantifying morphological and structural changes in electrode materials under operando conditions9In situ scattering studies of material formation during wet-chemical syntheses1Past, present and future—sample environments for materials research studies in scattering and spectroscopy; a UK perspective3XANES spectroscopy for the clinician9A capillary sample cell used for in-situ SAXS, XRD, and XAFS measurements during hydrothermal synthesis4Silicon PIN photodiode applied to acquire high-frequency sampling XAFS spectra9A novel SAXS/XRD/XAFS combined technique for in-situ time-resolved simultaneous measurements42Solvothermal and hydrothermal methods for preparative solid-state chemistry5Visualizing Catalytic Dynamics Processes via Synchrotron Radiation Multitechniques43Crystallization of monodisperse gold ultrasmall icosahedral nanoparticles : nucleation/growth mechanism study using microfluidic chips0Mass spectrometry of polymers: A tutorial review67Electrochemical Restoration of Battery Materials Guided by Synchrotron Radiation Technology for Sustainable Lithium‐Ion Batteries24Simultaneous fast XAS/SAXS measurements in an energy-dispersive mode3Recent advances in small-angle scattering techniques for MOF colloidal materials27In-situ tracking CO2-assisted isothermal-isobaric synthesis of self-assembled Bi-based photocatalyst using novel SAXS/XRD/XAFS combined technique11Combined In Situ / Operando Techniques0The frontier progress in synchrotron X-ray scattering in situ characterization of molecular sieve synthesis3From Atoms to Earth: A Review of Synchrotron Techniques and Case Studies in Earth and Environmental Sciences1A new experimental station for the beamline 1W2B of the Beijing Synchrotron Radiation Facility3Data acquisition software for the updated 1W2B beamline station0

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  1. Porous solids get organized

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  2. Designed open-structure heterogeneous catalysts for the synthesis of fine chemicals and pharmaceuticals

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  3. In situ studies of the crystallisation of microporous materials using synchrotron radiation based X-ray techniques

    Studies in surface science and catalysis · 2007-01-01

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  4. Insight into the structure of supported palladium catalysts during the total oxidation of methane

    Chemical Communications · 2007-01-01

    Jan‐Dierk Grunwaldt, Niels van Vegten, Alfons Baiker

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  5. New insights into the formation of microporous materials by in situ scattering techniques

    Faraday Discussions · 2007-01-01

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  6. The Zeolite Scene – An Overview

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    Theo L. M. Maesen

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  7. Understanding the crystallisation processes leading to the formation of microporous aluminophosphates

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  8. Zeolites: physical aspects and environmental applications

    Annual Reports Section C (Physical Chemistry) · 2007-01-01

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  9. Watching the crystallisation of complex oxides by in situ X-ray techniques

    Applied Catalysis A General · 2007-03-04

    Andrew Michael Beale, Lee M. Reilly, Gopinathan Sankar

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  10. Probing in situ the Nucleation and Growth of Gold Nanoparticles by Small-Angle X-ray Scattering

    Nano Letters · 2007-05-26

    Benjamin Abécassis, Fabienne Testard, Olivier Spalla, P. Barboux

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  11. In situsimultaneous Raman/high-resolution X-ray powder diffraction study of transformations occurring in materials at non-ambient conditions

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  12. Reactor design for in situ X-ray scattering studies of nanoparticle formation in supercritical water syntheses

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  13. Structural Characterization of Frozen n-Heptane Solutions of Metal-Containing Reverse Micelles

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  14. Synthesis

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  15. Effect of Organic Templates on the Kinetics and Crystallization of Microporous Metal-Substituted Aluminophosphates

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  16. IR and Raman Investigation of One-Dimensional and Three-Dimensional Aluminophosphite

    The Journal of Physical Chemistry C · 2007-11-13

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  17. Characterization of cement minerals, cements and their reaction products at the atomic and nano scale

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  18. Nucleation, Growth, and Aggregation of Mineral Phases: Mechanisms and Kinetic Controls

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  19. Synchrotron radiation studies of non-crystalline systems

    Annual Reports Section C (Physical Chemistry) · 2008-01-01

    Michel H. J. Koch, Wim Bras

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  20. The competition of organic amines and the phosphorus source on directing the formation of aluminophosphate-based molecular sieves with chabazite structure

    Microporous and Mesoporous Materials · 2008-02-20

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  21. Zeolite Mediated Reactions: Mechanistic Aspects and Environmental Applications

    Progress in Reaction Kinetics and Mechanism · 2008-03-01

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  22. Implementation of a combined SAXS/WAXS/QEXAFS set-up for time-resolved in situ experiments

    Journal of Synchrotron Radiation · 2008-10-02

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  23. Dynamic “operando” observation of 1 wt% Pd-based TWCs: Simultaneous XAS/DRIFTS/mass spectrometry analysis of the effects of Ce0.5Zr0.5O2 loading on structure, reactivity and performance

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  24. Chapter 6 Characterization of Catalysts in Reactive Atmospheres by X‐ray Absorption Spectroscopy

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  25. EXAFS spectroscopy as a tool to probe metal–support interaction and surface molecular structures in oxide-supported catalysts: application to Al2O3-supported Ni(ii) complexes and ZrO2-supported tungstates

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  26. The Use of Scattering and Spectroscopic Synchrotron Radiation Methods in Materials Science

    Lecture notes in physics · 2009-01-01

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  27. Local and long range order in promoted iron-based Fischer–Tropsch catalysts: A combined in situ X-ray absorption spectroscopy/wide angle X-ray scattering study

    Journal of Catalysis · 2009-01-23

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  28. Multi-Technique In Situ Approach Towards the Study of Catalytic Solids at Work Using Synchrotron Radiation

    Synchrotron Radiation News · 2009-01-29

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  29. Recent progress in the use of in situ X-ray methods for the study of heterogeneous catalysts in packed-bed capillary reactors

    Catalysis Today · 2009-03-23

    Simon D. M. Jacques, Olivier Leynaud, D. Strusevich, Paul Stukas, Paul Barnes, Gopinathan Sankar, Mike Sheehy, Matthew G. O’Brien, Ana Iglesias‐Juez, Andrew Michael Beale

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  30. Molecular engineering of microporous crystals: (I) New insight into the formation process of open-framework aluminophosphates

    Microporous and Mesoporous Materials · 2009-03-25

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  31. Linking Simultaneous In Situ WAXS/SAXS/Raman with Raman/ATR/UV–vis Spectroscopy: Comprehensive Insight into the Synthesis of Molybdate Catalyst Precursors

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  32. Chemische Bildgebung von räumlichen Heterogenitäten in katalytischen Festkörpern auf unterschiedlichen Längen‐ und Zeitskalen

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  33. A Combined Multi-Technique In Situ Approach Used to Probe the Stability of Iron Molybdate Catalysts During Redox Cycling

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  34. Chemical Imaging of Spatial Heterogeneities in Catalytic Solids at Different Length and Time Scales

    Angewandte Chemie International Edition · 2009-06-17

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  35. Insights into the formation of microporous materials by in situ X-ray scattering techniques

    Catalysis Today · 2009-07-01

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  36. Shining X-rays on catalysts at work

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  37. In Situ XAS and XRPD Parametric Rietveld Refinement To Understand Dealumination of Y Zeolite Catalyst

    Journal of the American Chemical Society · 2009-12-15

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  38. Combined use of XAFS, XRD and TEM to unravel the microstructural evolution of nanostructured ZrO2–SiO2 binary oxides: from nanometres down to the molecular domain

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  39. Combining in situ characterization methods in one set-up: looking with more eyes into the intricate chemistry of the synthesis and working of heterogeneous catalysts

    Chemical Society Reviews · 2010-01-01

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  40. Methods for in situ spectroscopic probing of the synthesis of a zeolite

    Chemical Society Reviews · 2010-01-01

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  41. The role of synchrotron radiation in examining the self-assembly of crystalline nanoporous framework materials: from zeolites and aluminophosphates to metal organic hybrids

    Chemical Society Reviews · 2010-01-01

    Matthew G. O’Brien, Andrew Michael Beale, Bert Marc Weckhuysen

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  42. Spectroscopic set-up for simultaneous UV-Vis/(Q)EXAFSin situandin operandostudies of homogeneous reactions under laboratory conditions

    Journal of Synchrotron Radiation · 2010-01-22

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  43. Multitechnique analysis of supported Pd particles upon dynamic, cycling CO/NO conditions: Size-dependence of the structure–activity relationship

    Journal of Catalysis · 2010-02-06

    Anna Kubacka, Arturo Martínez-Arias, Marcos Fernández–García, Marco Di Michiel, Mark A. Newton

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  44. Combining Time-Resolved Hard X-ray Diffraction and Diffuse Reflectance Infrared Spectroscopy To Illuminate CO Dissociation and Transient Carbon Storage by Supported Pd Nanoparticles during CO/NO Cycling

    Journal of the American Chemical Society · 2010-03-12

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  45. Experimental setup forin situX-ray SAXS/WAXS/PDF studies of the formation and growth of nanoparticles in near- and supercritical fluids

    Journal of Applied Crystallography · 2010-05-21

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  46. Closing the operando gap: The application of high energy photons for studying catalytic solids at work

    Applied Catalysis A General · 2010-06-24

    Matthew G. O’Brien, Andrew Michael Beale, Simon D. M. Jacques, Marco Di Michiel, Bert Marc Weckhuysen

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  47. Properties and applications of Zeolites

    Science Progress · 2010-08-01

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  48. Influence of Monomer Feeding on a Fast Gold Nanoparticles Synthesis: Time-Resolved XANES and SAXS Experiments

    Langmuir · 2010-08-12

    Benjamin Abécassis, Fabienne Testard, Quingyu Kong, F. Baudelet, Oliver Spalla

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  49. In Situ X-ray Diffraction and Absorption Studies of the Growth and Phase Transformation of Yttrium Hydroxide Nanotubes to Their Oxide Counterparts

    The Journal of Physical Chemistry C · 2010-09-20

    James A. Dorman, Yuanbing Mao, John Bargar, Jane P. Chang

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  50. Combined time-resolved SAXS and X-ray Spectroscopy methods

    Journal of Physics Conference Series · 2010-10-01

    Wim Bras, Sergey Nikitenko, Giuseppe Portale, Andrew Michael Beale, Ad M. J. van der Eerden, Dirk Detollenaere

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