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RESEARCH PAPER · Materials · 2018

Nuclear Magnetic Resonance Spectroscopy for In Situ Monitoring of Porous Materials Formation under Hydrothermal Conditions

Mohamed Haouas

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Nuclear Magnetic Resonance Spectroscopy for In Situ Monitoring of Porous Materials Formation under Hydrothermal ConditionsOriginalCyclodextrin-Driven Formation of Double Six-Ring (D6R) Silicate Cage: NMR Spectroscopic Characterization from Solution to Crystals7Real-time inline monitoring of zeolite synthesis by Photon Density Wave spectroscopy18On the Role of Enthalpic and Entropic Contributions on the Conformational Free Energy Landscape of MIL-101(Cr) Structural Building Units0Seed- and solvent-free synthesis of ZSM-5 with tuneable Si/Al ratios for biomass hydrogenation32Solid-state NMR spectroscopy: an advancing tool to analyse the structure and properties of metal–organic frameworks118Spectroscopy, microscopy, diffraction and scattering of archetypal MOFs: formation, metal sites in catalysis and thin films116Unraveling Structure and Dynamics in Porous Frameworks via Advanced In Situ Characterization Techniques134A brief introduction to the basics of NMR spectroscopy and selected examples of its applications to materials characterization42On the Role of Enthalpic and Entropic Contributions to the Conformational Free Energy Landscape of MIL‐101(Cr) Secondary Building Units16Development and validation of an analytical methodology for quantification of Al in alumina-based materials by 27Al Solid-state nmr1Predicting inorganic dimensionality in templated metal oxides8Application of Multinuclear MAS NMR for the in situ Monitoring of Hydrothermal Synthesis of Zeolites33Understanding MOF nucleation from solution with Evolving Graphs0Understanding Metal–Organic Framework Nucleation from a Solution with Evolving Graphs45Unraveling the molecular mechanism of MIL-53(Al) crystallization87Solvothermal and hydrothermal methods for preparative solid-state chemistry5Tracking Sub-Nano-Scale Structural Evolution in Zeolite Synthesis by In Situ High-Energy X-ray Total Scattering Measurement with Pair Distribution Function Analysis45In Situ Multinuclear Magic-Angle Spinning NMR: Monitoring Crystallization of Molecular Sieve AlPO4-11 in Real Time11Microwave-assisted rapid synthesize of cadmium–thallium mixed fluoride hydrate complex and its physiochemical properties1Perspective on the Use of Ultrasonic Monitoring for In Situ Diagnostics of Zeolite and MOF Crystallization6Illuminating the Black Box: A Perspective on Zeolite Crystallization in Inorganic Media36Deciphering the Mechanism of Crystallization of UiO‐66 Metal‐Organic Framework74Green and low-cost synthesis of zeolites from kaolin: a promising technology or a delusion?19Dual templated-based synthesis of smart zeolites and its self-healing anticorrosion coatings7The Dynamic View: Multiscale Characterisation Techniques for Flexible Frameworks1NMR crystallization: in situ NMR strategies for monitoring the evolution of crystallization processes9Exploiting in situ NMR spectroscopy to understand non-traditional methods for zeolite synthesis7Advancements in Understanding the Physicochemical Properties of Reticular Materials: An In Situ and Operando Spectroscopic Perspective25NMR Crystallization: The Application of NMR Strategies to Monitor the Evolution of Crystallization Processes0Role of a Modulator in the Synthesis of an MIL-53 Metal–Organic Framework Revealed by In Situ Time-Resolved MAS NMR Spectroscopy4Probing the heterogeneous amorphous network of silicoaluminophosphate binders by advanced multidimensional multinuclear SSNMR and DFT modeling1In Situ Ultrasound Monitoring of Fast ZIF-8 Nanoparticle Synthesis0

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32 direct citing papers saved.

  1. Cyclodextrin-Driven Formation of Double Six-Ring (D6R) Silicate Cage: NMR Spectroscopic Characterization from Solution to Crystals

    Crystals · 2018-12-07

    Mohamed Haouas, Clément Falaise, Charlotte Martineau, Emmanuel Cadot

    Read original paper ↗ ·

  2. Real-time inline monitoring of zeolite synthesis by Photon Density Wave spectroscopy

    Microporous and Mesoporous Materials · 2019-06-28

    Janick Häne, Dominik Brühwiler, Achim Ecker, Roland Hass

    Read original paper ↗ ·

  3. On the Role of Enthalpic and Entropic Contributions on the Conformational Free Energy Landscape of MIL-101(Cr) Structural Building Units

    ChemRxiv · 2019-10-11

    Loukas Kollias, David C. Cantu, Vassiliki‐Alexandra Glezakou, Roger J. Rousseau, Matteo Salvalaglio

    Read original paper ↗ ·

  4. Seed- and solvent-free synthesis of ZSM-5 with tuneable Si/Al ratios for biomass hydrogenation

    Green Chemistry · 2020-01-01

    Bin Zhang, Mark Douthwaite, Qiang Liu, Chao Zhang, Qifan Wu, Ruhui Shi, Peixuan Wu, Ke Liu, Zhuangqing Wang, Weiwei Lin, Haiyang Cheng, Ding Ma, Fengyu Zhao, Graham John Hutchings

    Read original paper ↗ ·

  5. Solid-state NMR spectroscopy: an advancing tool to analyse the structure and properties of metal–organic frameworks

    Chemical Science · 2020-01-01

    Eike Brunner, Marcus Rauche

    Read original paper ↗ ·

  6. Spectroscopy, microscopy, diffraction and scattering of archetypal MOFs: formation, metal sites in catalysis and thin films

    Chemical Society Reviews · 2020-01-01

    Miguel Rivera‐Torrente, Laurens D. B. Mandemaker, Matthias Filez, Guusje Delen, Beatriz Seoane, Florian Meirer, Bert Marc Weckhuysen

    Read original paper ↗ ·

  7. Unraveling Structure and Dynamics in Porous Frameworks via Advanced In Situ Characterization Techniques

    Advanced Functional Materials · 2020-01-28

    Volodymyr Bon, Eike Brunner, Andreas Pöppl, Stefan Kaskel

    Read original paper ↗ ·

  8. A brief introduction to the basics of NMR spectroscopy and selected examples of its applications to materials characterization

    Physical Sciences Reviews · 2020-06-03

    Alberto Tampieri, Márk Szabó, F. Medina, Henrik Gulyás

    Read original paper ↗ ·

  9. On the Role of Enthalpic and Entropic Contributions to the Conformational Free Energy Landscape of MIL‐101(Cr) Secondary Building Units

    Advanced Theory and Simulations · 2020-09-15

    Loukas Kollias, David C. Cantu, Vassiliki‐Alexandra Glezakou, Roger J. Rousseau, Matteo Salvalaglio

    Read original paper ↗ ·

  10. Development and validation of an analytical methodology for quantification of Al in alumina-based materials by 27Al Solid-state nmr

    International Journal of Development Research · 2021-03-17

    Read original paper ↗ ·

  11. Predicting inorganic dimensionality in templated metal oxides

    The Journal of Chemical Physics · 2021-05-12

    Qianxiang Ai, Davion Marquise Williams, Matthew Danielson, Liam G. Spooner, Joshua A. Engler, Zihui Ding, Mat­thias Zeller, Alexander J. Norquist, Joshua Schrier

    Read original paper ↗ ·

  12. Application of Multinuclear MAS NMR for the in situ Monitoring of Hydrothermal Synthesis of Zeolites

    Chemistry - A European Journal · 2021-08-17

    Irina I. Ivanova, Yu. G. Kolyagin

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  13. Understanding MOF nucleation from solution with Evolving Graphs

    ChemRxiv · 2021-12-23

    Loukas Kollias, Roger J. Rousseau, Vassiliki‐Alexandra Glezakou, Matteo Salvalaglio

    Read original paper ↗ ·

  14. Understanding Metal–Organic Framework Nucleation from a Solution with Evolving Graphs

    Journal of the American Chemical Society · 2022-06-16

    Loukas Kollias, Roger J. Rousseau, Vassiliki‐Alexandra Glezakou, Matteo Salvalaglio

    Read original paper ↗ ·

  15. Unraveling the molecular mechanism of MIL-53(Al) crystallization

    Nature Communications · 2022-06-29

    Daniil Salionov, Olesya O. Semivrazhskaya, Nicola Pietro Maria Casati, Marco Ranocchiari, Saša Bjelić, René Verel, Jeroen A. van Bokhoven, Vitaly L. Sushkevich

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  16. Solvothermal and hydrothermal methods for preparative solid-state chemistry

    Elsevier eBooks · 2022-11-25

    Richard I. Walton

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  17. Tracking Sub-Nano-Scale Structural Evolution in Zeolite Synthesis by In Situ High-Energy X-ray Total Scattering Measurement with Pair Distribution Function Analysis

    Journal of the American Chemical Society · 2022-12-16

    Ayano Minami, Peidong Hu, Yuki Sada, Hiroki Yamada, Koji Ohara, Yasuo Yonezawa, Yukichi Sasaki, Yutaka Yanaba, Masanori Takemoto, Yuki Yoshida, Tatsuya Okubo, Toru Wakihara

    Read original paper ↗ ·

  18. In Situ Multinuclear Magic-Angle Spinning NMR: Monitoring Crystallization of Molecular Sieve AlPO4-11 in Real Time

    JACS Au · 2023-05-09

    Sandamini H. Alahakoon, Mathew J. Willans, Yining Huang

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  19. Microwave-assisted rapid synthesize of cadmium–thallium mixed fluoride hydrate complex and its physiochemical properties

    Optical Materials · 2023-06-03

    D. Joseph Daniel, Subbaiah Muthu Prabhu, H. J. Kim

    Read original paper ↗ ·

  20. Perspective on the Use of Ultrasonic Monitoring for In Situ Diagnostics of Zeolite and MOF Crystallization

    Crystal Growth & Design · 2023-06-27

    Matthias Ermer, Rebecca Reber, Hasan Baser, Marcus Fischer, Wilhelm Schwieger, Martin Hartmann

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  21. Illuminating the Black Box: A Perspective on Zeolite Crystallization in Inorganic Media

    Accounts of Chemical Research · 2023-08-11

    Karel Asselman, Christine E. A. Kirschhock, Eric Breynaert

    Read original paper ↗ ·

  22. Deciphering the Mechanism of Crystallization of UiO‐66 Metal‐Organic Framework

    Small · 2023-08-27

    Olesya O. Semivrazhskaya, Daniil Salionov, Adam H. Clark, Nicola Pietro Maria Casati, Maarten Nachtegaal, Marco Ranocchiari, Saša Bjelić, René Verel, Jeroen A. van Bokhoven, Vitaly L. Sushkevich

    Read original paper ↗ ·

  23. Green and low-cost synthesis of zeolites from kaolin: a promising technology or a delusion?

    Reaction Chemistry & Engineering · 2024-01-01

    Ivan M. Zdretsov, Andrey M. Gerasimov

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  24. Dual templated-based synthesis of smart zeolites and its self-healing anticorrosion coatings

    European Polymer Journal · 2024-03-20

    Tamilvanan Siva, Balasubramaniam Saravanakumar, Ananthakumar Ramadoss

    Read original paper ↗ ·

  25. The Dynamic View: Multiscale Characterisation Techniques for Flexible Frameworks

    Royal Society of Chemistry eBooks · 2024-03-25

    Volodymyr Bon, Kornel Roztocki, Paul Iacomi, Claire L. Hobday, Irena Senkovska, Andreas Pöppl, Eike Brunner, Stefan Kaskel

    Read original paper ↗ ·

  26. NMR crystallization: in situ NMR strategies for monitoring the evolution of crystallization processes

    Faraday Discussions · 2024-06-28

    Colan E. Hughes, Naomi V. Ratnasingam, P. Andrew Williams, Erwan Benhenou, Rhian Patterson, Kenneth D M Harris

    Read original paper ↗ ·

  27. Exploiting in situ NMR spectroscopy to understand non-traditional methods for zeolite synthesis

    Chemical Science · 2025-01-01

    Nicole L. Kelly, Emma A. L. Borthwick, Gaynor B. Lawrence, Paul S. Wheatley, Colan E. Hughes, Kenneth D M Harris, Russell E. Morris, Sharon Elizabeth Ashbrook

    Read original paper ↗ ·

  28. Advancements in Understanding the Physicochemical Properties of Reticular Materials: An In Situ and Operando Spectroscopic Perspective

    Advanced Materials · 2025-02-24

    Bettina Baumgartner, Anna Wach, Xinwei Ye, Evelyn Ploetz, Bert Marc Weckhuysen

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  29. NMR Crystallization: The Application of NMR Strategies to Monitor the Evolution of Crystallization Processes

    Royal Society of Chemistry eBooks · 2025-03-31

    Kenneth D M Harris, Colan E. Hughes

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  30. Role of a Modulator in the Synthesis of an MIL-53 Metal–Organic Framework Revealed by In Situ Time-Resolved MAS NMR Spectroscopy

    Journal of the American Chemical Society · 2025-11-20

    Bastian Achenbach, René Verel, Jeroen A. van Bokhoven, Norbert Stock, Vitaly L. Sushkevich

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  31. Probing the heterogeneous amorphous network of silicoaluminophosphate binders by advanced multidimensional multinuclear SSNMR and DFT modeling

    Journal of Non-Crystalline Solids · 2026-03-13

    Davide Bernasconi, Simone Bordignon, Pierre Florian, Franck Fayon, Annalisa Pallini, Geo Paul, Janez Volavšek, Nadia Curetti, Alfonso Pedone, Roberto Gobetto, Alessandrο Pavese, Alberto Viani

    Read original paper ↗ ·

  32. In Situ Ultrasound Monitoring of Fast ZIF-8 Nanoparticle Synthesis

    Crystal Growth & Design · 2026-07-01

    Rebecca Reber, Louis Rupprecht, Marcus Fischer, Martin Hartmann

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