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RESEARCH PAPER · Chemistry of Materials · 2021

K5Mg2La3(BO3)6: An Efficient, Deep-Ultraviolet Nonlinear Optical Material

Runqing Liu, Hongping Wu, Hongwei Yu, Zhanggui Hu, Jiyang Wang, Yicheng Wu

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K5Mg2La3(BO3)6: An Efficient, Deep-Ultraviolet Nonlinear Optical MaterialOriginalPhotoinduced versus spontaneous host–guest electron transfer within a MOF and chromic/luminescent response37Nd2CaB10O19: A potential self-activated and self-frequency-doubling multifunctional crystal8La 3 Ga 3 Ge 2 S 3 O 10 : An Ultraviolet Nonlinear Optical Oxysulfide Designed by Anion‐Directed Band Gap Engineering63La3Ga3Ge2S3O10: An Ultraviolet Nonlinear Optical Oxysulfide Designed by Anion‐Directed Band Gap Engineering18Ba 10 LuB 18 O 32 F 13 : the first example of borate in the Lu–B–O–F system with the unprecedented FBB [B 9 O 22 ]12Crystal Structures and Magnetocaloric Properties of Li5asrmb12o24 (a = Mg, Zn; M = Cr, Ni)6KRE(CO 3 ) 2 (RE = Eu, Gd, Tb): new mixed metal carbonates with strong photoluminescence and large birefringence15Li 6.58 Na 7.43 Sr 4 (B 9 O 18 )(B 12 O 24 )Cl: unprecedented combination of the largest two highly polymerized isolated B–O clusters with novel isolated B 9 O 18 FBB18Two non-centrosymmetric scandium borate nonlinear optical crystals containing the B5O10 anion group26Chiral Ligand‐Driven Systematic Synthesis of Coordination Polymers with Non‐centrosymmetric Structures12Enhanced Electron–Phonon Coupling Effect in Rare-Earth Borate Crystals Containing a “Quasi-Free-Oxygen” Motif11Additive‐Triggered Polar Polymorph Formation: β‐Sc(IO 3 ) 3 , a Promising Next‐Generation Mid‐Infrared Nonlinear Optical Material42Additive‐Triggered Polar Polymorph Formation: β‐Sc(IO3)3, a Promising Next‐Generation Mid‐Infrared Nonlinear Optical Material3Shedding Light on the Structure and Characterization of K2ZnGe2O6: A Phase-Matchable Nonlinear Optical Crystal19Deep Ultraviolet-Transparent Materials with Strong Second-Harmonic Response50RE(OH) 2 NO 3 (RE = Tb, Dy, Ho, and Er): Synthesis and Nonlinear Optical Properties of Water-Resistant Lanthanide Hydroxide Nitrates15Rb 3 B 11 P 2 O 23 : Materials Design of a New Chemically Benign Deep-Ultraviolet Nonlinear Optical Material58A lithium–scandium sulfate with second-harmonic generation response and deep-ultraviolet transparency7Achieving broadband ultraviolet to mid-infrared transparency in germanate-based nonlinear optical crystals Cs 3 REGe 3 O 9 (RE = Y, Gd)16Growth and characterization of Na 3 R(BO 3 ) 2 (R = La–Gd) borates: crystal structure, high-temperature behavior, and optical properties7KNa 2 La 2 (BO 3 ) 3 : a shortite-type lanthanide borate exhibiting strong nonlinear optical activity induced by isolated [BO 3 ] triangles and distorted [LaO 9 ] polyhedra26Two non-centrosymmetric mixed alkali metal and alkaline earth metal scandium borate nonlinear optical materials with short ultraviolet cutoff edges14Rational Design of the First Ammonium Magnesium Borate with Deep-Ultraviolet Cutoff Edge and Moderate Birefringence and Further Investigation into the Nature of Ammonium in the Borate System15Recent advances of inorganic phosphates with UV/DUV cutoff edge and large second harmonic response7Ba2B9O13F4·BF4: first fluorooxoborate with unprecedented infinite [B18O26F8] tubes and deep-ultraviolet cutoff edge14Mixed Alkali Metal and Alkaline Earth Metal Scandium Borate Birefringence Material with Layered Structure and Short Ultraviolet Cutoff Edge17Design Principles for Noncentrosymmetric Materials23Luminescence of Sr 6 YAl(BO 3 ) 6 activated with Tb 3+ and Gd 3+2LiGa(IO3)4: An Excellent NLO Material with Unprecedented 2D [Ga(IO3)4]∞− Layer Synthesized by Aliovalent Substitution20Computationally-driven discovery of second harmonic generation in EuBa 3 (B 3 O 6 ) 3 through inversion symmetry breaking4A-site cation manipulation of exemplary second harmonic generation response and optical anisotropy in rare-earth borates18Enhanced near-infrared optical transmission in zinc germanium phosphide crystals via precise magnesium doping3Exploring a new short-wavelength nonlinear optical fluoride material featuring unprecedented polar cis -[Zr 6 F 34 ] 10− clusters48Li 3 Na 7 B 4 P 6 O 26 : a new ultraviolet transparent congruently melting non-linear optical crystal3Recent advances in rational structure design for nonlinear optical crystals: leveraging advantageous templates153From ZnF2 to ZnF2(H2O)4: Partial Substitution Achieves Structural Transformation and Nonlinear Optical Activity while Keeping Short Ultraviolet Cutoff Edge19KNa 2 Lu(BO 3 ) 2 : A Rare-Earth Borate Crystal Characterized by an Enhanced Birefringence and Wide Ultraviolet Transparency Range19Recent advances and future perspectives on rare-earth-based nonlinear optical materials with π-conjugated [XO3] (X = B, C, N) units66A3Sc(SO4)3 (A = K, Rb, Cs): Three Deep‐Ultraviolet Transparent Alkali‐Scandium Sulfates with Strong Second‐Harmonic Generation Response and High Thermal Stability14NaK5La2(SO4)6: Enhanced Birefringence of Multiple-Alkali Metal Sulfate Systems via Rare Earth Metal-Centered Polyhedra5A Rare-Earth-Based Borate Optical Crystal with Enlarged Dihedral Angles of Distinct [BO3] Groups Exhibiting a Wide UV Transparent Range8K3Y3(BO3)4: A Potential UV Nonlinear-Optical Crystal Designed by a Chemical Substitution Strategy14Chemical substitution towards a rare-earth borate ultraviolet NLO crystal exhibiting a strong SHG response17K 15 La 7 (BO 3 ) 12 : A KBBF-Like Nonlinear-Optical Material with a Short Cutoff Edge and a Strong Second-Harmonic-Generation Response10Rational design of a series of non-centrosymmetric antiperovskite and double antiperovskite borate fluorides13A potential UV nonlinear-optical crystal with a strong second-harmonic response: RbNa 2 Eu 2 (BO 3 ) 35An excellent ultraviolet nonlinear optical crystal derived from the polar methylphosphonate unit8Na 2 PbB 6 O 10 SO 4 and Ca 2.58 Pb 0.42 B 6 O 11 SO 4 : first borate–sulfates featuring 3D porous borate anionic frameworks0Synthesising a series of promising ultraviolet nonlinear optical materials with the aid of the flexibility of isolated [B 5 O 10 ] groups3Hetero‐Anionic Oxychalcogenides with Structures and Properties Tuned by the O:S Ratio14An alkali and rare earth metal mixed cyanurate KLa2(C3N3O3)2Cl with large birefringence: Synthesis and characterization2Crystal Structures, Phase Transition, and Optical Properties of Two Rare Earth Borate Fluorides: α- and β-BaGdBO3F26The self-activated K7CaY2(B5O10)3 phosphor and the effect of trivalent dopants on the emission properties4Review of KBe2BO3F2-like second-order nonlinear optical materials and their structure-performance relationships13CsLa(SO 4 ) 2 : A Lanthanum Sulfate Crystal for Nonlinear Optical Applications10La3Ga5HfO14: Rare-Earth Polyhedron Coupled with Structural Protected Octahedron for Designing Nonlinear Optical Material with Wide Bandgap and Well-Balanced Properties5Cd3Sc(BO3)3: a novel orthoborate with pseudo-1D ∞[ScB6O18] chains0A Promising Short-Wave UV NLO Crystal with an Optimized KBBF-like Structure and Well-Balanced Properties Achieved via a Chemical Substitution Strategy6LnEuGa3OS6 (Ln = La, Pr, Nd): three dual rare earth metal-based oxychalcogenides with good IR nonlinear optical performances1A Band‐Orientation Co‐Anchoring Strategy for the Design of a High‐Performance Mid‐Infrared Nonlinear Optical Crystal2A Band‐Orientation Co‐Anchoring Strategy for the Design of a High‐Performance Mid‐Infrared Nonlinear Optical Crystal12Shape‐Topology‐Driven Design of Deep Ultraviolet Nonlinear Optical Crystals: Engineering [CH 3 PO 3 ]–Metal‐Oxo Layered Frameworks for Enhanced SHG, DUV Transparency3Ba 3 BiPbREO(BO 3 ) 4 (RE = Pr, Nd, Gd, and Dy): two-dimensional rare-earth antiferromagnets with a geometrically-perfect triangular lattice directed by a triangular BO 3 unit0Beating the concentration quenching: A review0Strong Optical Nonlinearity in Polar Hypophosphites via Chiral Cation Assembly1Exploring the luminescence behaviour of RE³ + (Gd, Tb, Eu) activated borate host K₅Mg₂La₃(BO₃)₆0Review on recent trends in NIR-emitting trivalent chromium (Cr 3+ ) ion-doped phosphors for applications in pc-LEDs0Cation-driven symmetry breaking in rare-earth borates toward ultraviolet nonlinear optical materials1When Octahedra Learn to Be Prisms: Unlocking a Record Deep‑UV NLO Crystal0When Octahedra Learn to Be Prisms: Unlocking a Record Deep‑UV NLO Crystal0

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  1. Photoinduced versus spontaneous host–guest electron transfer within a MOF and chromic/luminescent response

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  2. Nd2CaB10O19: A potential self-activated and self-frequency-doubling multifunctional crystal

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  3. La 3 Ga 3 Ge 2 S 3 O 10 : An Ultraviolet Nonlinear Optical Oxysulfide Designed by Anion‐Directed Band Gap Engineering

    Angewandte Chemie International Edition · 2021-10-09

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  4. La3Ga3Ge2S3O10: An Ultraviolet Nonlinear Optical Oxysulfide Designed by Anion‐Directed Band Gap Engineering

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  5. Ba 10 LuB 18 O 32 F 13 : the first example of borate in the Lu–B–O–F system with the unprecedented FBB [B 9 O 22 ]

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  6. Crystal Structures and Magnetocaloric Properties of Li5asrmb12o24 (a = Mg, Zn; M = Cr, Ni)

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    Yuwei Chen, Jingcheng Feng, Feidi Fan, Jun Shen, Guochun Zhang, Heng Tu

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  7. KRE(CO 3 ) 2 (RE = Eu, Gd, Tb): new mixed metal carbonates with strong photoluminescence and large birefringence

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    Yuan Hua Lin, Chun‐Li Hu, Zhi Gang Fang, Jin Chen, Weijie Xie, Yan Chen, Jianpu Wang, Jiang‐Gao Mao

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  8. Li 6.58 Na 7.43 Sr 4 (B 9 O 18 )(B 12 O 24 )Cl: unprecedented combination of the largest two highly polymerized isolated B–O clusters with novel isolated B 9 O 18 FBB

    Inorganic Chemistry Frontiers · 2022-01-01

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  9. Two non-centrosymmetric scandium borate nonlinear optical crystals containing the B5O10 anion group

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  10. Chiral Ligand‐Driven Systematic Synthesis of Coordination Polymers with Non‐centrosymmetric Structures

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  11. Enhanced Electron–Phonon Coupling Effect in Rare-Earth Borate Crystals Containing a “Quasi-Free-Oxygen” Motif

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  12. Additive‐Triggered Polar Polymorph Formation: β‐Sc(IO 3 ) 3 , a Promising Next‐Generation Mid‐Infrared Nonlinear Optical Material

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  13. Additive‐Triggered Polar Polymorph Formation: β‐Sc(IO3)3, a Promising Next‐Generation Mid‐Infrared Nonlinear Optical Material

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  14. Shedding Light on the Structure and Characterization of K2ZnGe2O6: A Phase-Matchable Nonlinear Optical Crystal

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  15. Deep Ultraviolet-Transparent Materials with Strong Second-Harmonic Response

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  16. RE(OH) 2 NO 3 (RE = Tb, Dy, Ho, and Er): Synthesis and Nonlinear Optical Properties of Water-Resistant Lanthanide Hydroxide Nitrates

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  17. Rb 3 B 11 P 2 O 23 : Materials Design of a New Chemically Benign Deep-Ultraviolet Nonlinear Optical Material

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  18. A lithium–scandium sulfate with second-harmonic generation response and deep-ultraviolet transparency

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  19. Achieving broadband ultraviolet to mid-infrared transparency in germanate-based nonlinear optical crystals Cs 3 REGe 3 O 9 (RE = Y, Gd)

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  20. Growth and characterization of Na 3 R(BO 3 ) 2 (R = La–Gd) borates: crystal structure, high-temperature behavior, and optical properties

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  21. KNa 2 La 2 (BO 3 ) 3 : a shortite-type lanthanide borate exhibiting strong nonlinear optical activity induced by isolated [BO 3 ] triangles and distorted [LaO 9 ] polyhedra

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  22. Two non-centrosymmetric mixed alkali metal and alkaline earth metal scandium borate nonlinear optical materials with short ultraviolet cutoff edges

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  23. Rational Design of the First Ammonium Magnesium Borate with Deep-Ultraviolet Cutoff Edge and Moderate Birefringence and Further Investigation into the Nature of Ammonium in the Borate System

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  24. Recent advances of inorganic phosphates with UV/DUV cutoff edge and large second harmonic response

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  25. Ba2B9O13F4·BF4: first fluorooxoborate with unprecedented infinite [B18O26F8] tubes and deep-ultraviolet cutoff edge

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  28. Luminescence of Sr 6 YAl(BO 3 ) 6 activated with Tb 3+ and Gd 3+

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  29. LiGa(IO3)4: An Excellent NLO Material with Unprecedented 2D [Ga(IO3)4]∞− Layer Synthesized by Aliovalent Substitution

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  30. Computationally-driven discovery of second harmonic generation in EuBa 3 (B 3 O 6 ) 3 through inversion symmetry breaking

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  31. A-site cation manipulation of exemplary second harmonic generation response and optical anisotropy in rare-earth borates

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  32. Enhanced near-infrared optical transmission in zinc germanium phosphide crystals via precise magnesium doping

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  33. Exploring a new short-wavelength nonlinear optical fluoride material featuring unprecedented polar cis -[Zr 6 F 34 ] 10− clusters

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  34. Li 3 Na 7 B 4 P 6 O 26 : a new ultraviolet transparent congruently melting non-linear optical crystal

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  35. Recent advances in rational structure design for nonlinear optical crystals: leveraging advantageous templates

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  36. From ZnF2 to ZnF2(H2O)4: Partial Substitution Achieves Structural Transformation and Nonlinear Optical Activity while Keeping Short Ultraviolet Cutoff Edge

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  37. KNa 2 Lu(BO 3 ) 2 : A Rare-Earth Borate Crystal Characterized by an Enhanced Birefringence and Wide Ultraviolet Transparency Range

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  40. NaK5La2(SO4)6: Enhanced Birefringence of Multiple-Alkali Metal Sulfate Systems via Rare Earth Metal-Centered Polyhedra

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  42. K3Y3(BO3)4: A Potential UV Nonlinear-Optical Crystal Designed by a Chemical Substitution Strategy

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  43. Chemical substitution towards a rare-earth borate ultraviolet NLO crystal exhibiting a strong SHG response

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  44. K 15 La 7 (BO 3 ) 12 : A KBBF-Like Nonlinear-Optical Material with a Short Cutoff Edge and a Strong Second-Harmonic-Generation Response

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  45. Rational design of a series of non-centrosymmetric antiperovskite and double antiperovskite borate fluorides

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  46. A potential UV nonlinear-optical crystal with a strong second-harmonic response: RbNa 2 Eu 2 (BO 3 ) 3

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  47. An excellent ultraviolet nonlinear optical crystal derived from the polar methylphosphonate unit

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  48. Na 2 PbB 6 O 10 SO 4 and Ca 2.58 Pb 0.42 B 6 O 11 SO 4 : first borate–sulfates featuring 3D porous borate anionic frameworks

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  49. Synthesising a series of promising ultraviolet nonlinear optical materials with the aid of the flexibility of isolated [B 5 O 10 ] groups

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  50. Hetero‐Anionic Oxychalcogenides with Structures and Properties Tuned by the O:S Ratio

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