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RESEARCH PAPER · Journal of Solid State Chemistry · 2002

Crystal Structures of Three Framework Alkali Metal Uranyl Phosphate Hydrates

Andrew J. Locock, Peter Carman Burns

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Crystal Structures of Three Framework Alkali Metal Uranyl Phosphate HydratesOriginal22 New compounds and structures in the solid state221 New compounds and structures in the solid state1Advances in Understanding of the Crystal Chemistry of Hexavalent Uranium2The Actinides34THE CRYSTAL STRUCTURE OF BERGENITE, A NEW GEOMETRICAL ISOMER OF THE PHOSPHURANYLITE GROUP41CRYSTAL STRUCTURES AND SYNTHESIS OF THE COPPER-DOMINANT MEMBERS OF THE AUTUNITE AND META-AUTUNITE GROUPS: TORBERNITE, ZEUNERITE, METATORBERNITE AND METAZEUNERITE119Direct Investigations of the Immobilization of Radionuclides in the Alteration Phases of Spent Nuclear Fuel4Do Secondary and Tertiary Ammonium Cations Act as Structure-Directing Agents in the Formation of Layered Uranyl Selenites?48Structures and synthesis of framework Rb and Cs uranyl arsenates and their relationships with their phosphate analogues31The structure of hügelite, an arsenate of the phosphuranylite group, and its relationship to dumontite22Topological Evolution in Uranyl Dicarboxylates: Synthesis and Structures of One-Dimensional UO2(C6H8O4)(H2O)2 and Three-Dimensional UO2(C6H8O4)130Structures and syntheses of framework triuranyl diarsenate hydrates45An Unprecedented Uranyl Phosphate Framework in the Structure of [(UO2)3(PO4)O(OH)(H2O)2](H2O)53Revised Tl(I)–O bond valence parameters and the structures of thallous dichromate and thallous uranyl phosphate hydrate59Structures and syntheses of layered and framework amine-bearing uranyl phosphate and uranyl arsenates40MONOVALENT CATIONS IN STRUCTURES OF THE META-AUTUNITE GROUP65Theoretical studies on the nature of uranyl–silicate, uranyl–phosphate and uranyl–arsenate interactions in the model H2UO2SiO4· 3H2O, HUO2PO4· 3H2O, and HUO2AsO4· 3H2O molecules16Chiral open-framework uranyl molybdates. 1. Topological diversity: synthesis and crystal structure of [(C2H5)2NH2]2[(UO2)4(MoO4)5(H2O)](H2O)53Direct Investigations of the Immobilization of Radionuclides in the Alteration Products of Spent Nuclear Fuel2Topology of Microporous Structures51U6+ MINERALS AND INORGANIC COMPOUNDS: INSIGHTS INTO AN EXPANDED STRUCTURAL HIERARCHY OF CRYSTAL STRUCTURES627General Route to Three-Dimensional Framework Uranyl Transition Metal Phosphates with Atypical Structural Motifs: The Case Examples of Cs2{(UO2)4[Co(H2O)2]2(HPO4)(PO4)4} and Cs3+x[(UO2)3CuH4-x(PO4)5]·H2O40A Raman spectroscopic study of the uranyl phosphate mineral parsonsite68The A1−xUNbO6−x/2 compounds (x=0, A=Li, Na, K, Cs and x=0.5, A=Rb, Cs): from layered to tunneled structure15Expanding the Crystal Chemistry of Actinyl Peroxides: Open Sheets of Uranyl Polyhedra in Na5[(UO2)3(O2)4(OH)3](H2O)1333New Layered Uranium Phosphate Fluorides: Syntheses, Structures, Characterizations, and Ion-Exchange Properties of A(UO2)F(HPO4)·xH2O (A = Cs+, Rb+, K+; x = 0−1)88Structural chemistry of uranium vanadates: from 2-D to 3-D networks1Phosphate Bariers for Immobilization of Uranium Plumes0Raman spectroscopic study of the uranyl phosphate minerals phosphuranylite and yingjiangite63THE STEREOCHEMISTRY AND CHEMICAL COMPOSITION OF INTERSTITIAL COMPLEXES IN URANYL-OXYSALT MINERALS75Synthesis and structure of [C6H14N2][(UO2)4(HPO4)2(PO4)2(H2O)]·H2O: An expanded open-framework amine-bearing uranyl phosphate12[H2bipy]2[(UO2)6Zn2(PO3OH)4(PO4)4]·H2O: An Open-Framework Uranyl Zinc Phosphate Templated by Diprotonated 4,4′-Bipyridyl17Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Channels occupancy and distortion in new lithium uranyl phosphates with three-dimensional open-frameworks14A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems28U(VI) oxygen polyhedra as pillars for building frameworks from uranophane-type layers6New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates28Uranyl phosphate sheet reconstruction during dehydration of metatorbernite [Cu(UO2)2(PO4)2{middle dot}8H2O]15Linear Alkyl Diamine-Uranium-Phosphate Systems: U(VI) to U(IV) Reduction with Ethylenediamine10Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates38Synthesis, structure, and spectroscopic characterization of three uranyl phosphates with unique structural units10Ionothermal synthesis of uranyl compounds that incorporate imidazole derivatives14Crystal Chemistry of Uranium Oxides and Minerals27Novel Fundamental Building Blocks and Site Dependent Isomorphism in the First Actinide Borophosphates11Density Functional Theory Study of the Complexation of the Uranyl Dication with Anionic Phosphate Ligands with and without Water Molecules33A Revised and Expanded Structure Hierarchy of Natural and Synthetic Hexavalent Uranium Compounds172Rb2[Ca(NpO2)2(PO4)2], the First Mixed Alkali–Alkaline Earth Metals Neptunyl(V) Phosphate: Crystal Chemistry and Sheet Stereoisomerism7An experimental calorimetric and a DFT + U study of the thermodynamic properties of Cs 4 UO 2 4 WO 5 W 2 O 8 O 2 and Cs 4 [ UO 2 7 WO 5 3 O 3 ]4Practices of Dispersed Uranium Minerals Study by AТEM Methods0Mild hydrothermal synthesis of potassium uranyl phosphates with layered and framework structures2Exploring the Role of Organic Functional Groups in the Ionothermal Synthesis of Uranyl Phosphate Materials3The crystal chemistry of plutonium( iv ) borophosphate1Speciation of plutonium and analogs in phosphate media0Modularity, polytypism, topology, and complexity of crystal structures of inorganic compounds (Review)32Hydrothermal synthesis and structure of organically templated layered neptunyl( vi ) phosphate (NpO 2 ) 3 (PO 4 ) 2 (Terpy)0Uptake and coordination behaviour of uranyl on functionalised silica3

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  1. 22 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2002-01-01

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  2. 21 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2003-01-01

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  3. Advances in Understanding of the Crystal Chemistry of Hexavalent Uranium

    MRS Proceedings · 2003-01-01

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  4. The Actinides

    Elsevier eBooks · 2003-01-01

    Carol J. Burns, Mary P. Neu, Hakim Boukhalfa, Keith E. Gutowski, Nicholas J. Bridges, Robin Don Rogers

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  5. THE CRYSTAL STRUCTURE OF BERGENITE, A NEW GEOMETRICAL ISOMER OF THE PHOSPHURANYLITE GROUP

    The Canadian Mineralogist · 2003-02-01

    Andrew J. Locock, Peter Carman Burns

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  6. CRYSTAL STRUCTURES AND SYNTHESIS OF THE COPPER-DOMINANT MEMBERS OF THE AUTUNITE AND META-AUTUNITE GROUPS: TORBERNITE, ZEUNERITE, METATORBERNITE AND METAZEUNERITE

    The Canadian Mineralogist · 2003-04-01

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  7. Direct Investigations of the Immobilization of Radionuclides in the Alteration Phases of Spent Nuclear Fuel

    Unknown journal · 2003-06-01

    Peter Carman Burns, USDOE Office of Science (SC) (US), Argonne National Chemical Technology Division, Robert J. Finch, David J. Wronkiewicz

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  8. Do Secondary and Tertiary Ammonium Cations Act as Structure-Directing Agents in the Formation of Layered Uranyl Selenites?

    Inorganic Chemistry · 2003-08-12

    Philip M. Almond, Thomas E. Albrecht‐Schmitt

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  9. Structures and synthesis of framework Rb and Cs uranyl arsenates and their relationships with their phosphate analogues

    Journal of Solid State Chemistry · 2003-09-16

    Andrew J. Locock, Peter Carman Burns

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  10. The structure of hügelite, an arsenate of the phosphuranylite group, and its relationship to dumontite

    Mineralogical Magazine · 2003-10-01

    Andrew J. Locock, Peter Carman Burns

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  11. Topological Evolution in Uranyl Dicarboxylates: Synthesis and Structures of One-Dimensional UO2(C6H8O4)(H2O)2 and Three-Dimensional UO2(C6H8O4)

    Inorganic Chemistry · 2003-10-04

    Lauren A. Borkowski, Christopher L. Cahill

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  12. Structures and syntheses of framework triuranyl diarsenate hydrates

    Journal of Solid State Chemistry · 2003-10-15

    Andrew J. Locock, Peter Carman Burns

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  13. An Unprecedented Uranyl Phosphate Framework in the Structure of [(UO2)3(PO4)O(OH)(H2O)2](H2O)

    Inorganic Chemistry · 2004-02-24

    Peter Carman Burns, Cara M. Alexopoulos, Peter J. Hotchkiss, Andrew J. Locock

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  14. Revised Tl(I)–O bond valence parameters and the structures of thallous dichromate and thallous uranyl phosphate hydrate

    Zeitschrift für Kristallographie - Crystalline Materials · 2004-05-01

    Andrew J. Locock, Peter Carman Burns

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  15. Structures and syntheses of layered and framework amine-bearing uranyl phosphate and uranyl arsenates

    Journal of Solid State Chemistry · 2004-06-21

    Andrew J. Locock, Peter Carman Burns

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  16. MONOVALENT CATIONS IN STRUCTURES OF THE META-AUTUNITE GROUP

    The Canadian Mineralogist · 2004-08-01

    Andrew J. Locock, Peter Carman Burns, M. John M. Duke, Theodore M. Flynn

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  17. Theoretical studies on the nature of uranyl–silicate, uranyl–phosphate and uranyl–arsenate interactions in the model H2UO2SiO4· 3H2O, HUO2PO4· 3H2O, and HUO2AsO4· 3H2O molecules

    Chemical Physics Letters · 2004-09-14

    Devashis Majumdar, K. Balasubramanian

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  18. Chiral open-framework uranyl molybdates. 1. Topological diversity: synthesis and crystal structure of [(C2H5)2NH2]2[(UO2)4(MoO4)5(H2O)](H2O)

    Microporous and Mesoporous Materials · 2004-12-16

    Sergey V. Krivovichev, Christopher L. Cahill, Еvgeny V. Nazarchuk, Peter Carman Burns, Thomas Armbruster, Wulf Depmeier

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  19. Direct Investigations of the Immobilization of Radionuclides in the Alteration Products of Spent Nuclear Fuel

    Unknown journal · 2004-12-27

    Peter Carman Burns, Robert J. Finch, David J. Wronkiewicz

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  20. Topology of Microporous Structures

    Reviews in Mineralogy and Geochemistry · 2005-01-01

    Sergey V. Krivovichev

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  21. U6+ MINERALS AND INORGANIC COMPOUNDS: INSIGHTS INTO AN EXPANDED STRUCTURAL HIERARCHY OF CRYSTAL STRUCTURES

    The Canadian Mineralogist · 2005-12-01

    Peter Carman Burns

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  22. General Route to Three-Dimensional Framework Uranyl Transition Metal Phosphates with Atypical Structural Motifs: The Case Examples of Cs2{(UO2)4[Co(H2O)2]2(HPO4)(PO4)4} and Cs3+x[(UO2)3CuH4-x(PO4)5]·H2O

    Inorganic Chemistry · 2006-02-03

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  23. A Raman spectroscopic study of the uranyl phosphate mineral parsonsite

    Journal of Raman Spectroscopy · 2006-03-16

    Ray L. Frost, Jiřı́ Čejka, Matt L. Weier, Wayde N. Martens

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  24. The A1−xUNbO6−x/2 compounds (x=0, A=Li, Na, K, Cs and x=0.5, A=Rb, Cs): from layered to tunneled structure

    Journal of Solid State Chemistry · 2006-06-22

    Suzy Surblé, S. Obbade, S. Saad, S. Yagoubi, C. Dion, F. Abraham

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  25. Expanding the Crystal Chemistry of Actinyl Peroxides: Open Sheets of Uranyl Polyhedra in Na5[(UO2)3(O2)4(OH)3](H2O)13

    Inorganic Chemistry · 2006-07-06

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  26. New Layered Uranium Phosphate Fluorides: Syntheses, Structures, Characterizations, and Ion-Exchange Properties of A(UO2)F(HPO4)·xH2O (A = Cs+, Rb+, K+; x = 0−1)

    Inorganic Chemistry · 2006-11-15

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  27. Structural chemistry of uranium vanadates: from 2-D to 3-D networks

    Elsevier eBooks · 2007-01-01

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  28. Phosphate Bariers for Immobilization of Uranium Plumes

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  29. Raman spectroscopic study of the uranyl phosphate minerals phosphuranylite and yingjiangite

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  30. THE STEREOCHEMISTRY AND CHEMICAL COMPOSITION OF INTERSTITIAL COMPLEXES IN URANYL-OXYSALT MINERALS

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  31. Synthesis and structure of [C6H14N2][(UO2)4(HPO4)2(PO4)2(H2O)]·H2O: An expanded open-framework amine-bearing uranyl phosphate

    Journal of Solid State Chemistry · 2008-05-17

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  32. [H2bipy]2[(UO2)6Zn2(PO3OH)4(PO4)4]·H2O: An Open-Framework Uranyl Zinc Phosphate Templated by Diprotonated 4,4′-Bipyridyl

    Inorganic Chemistry · 2008-08-23

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  33. Alternative approaches to structure description

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  34. Anion-topology approach

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  35. Basic concepts

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  36. Copyright Page

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  37. Dedication

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  38. Dimensional reduction in inorganic oxysalts

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  39. Graph theory applied to low-dimensional structural units in inorganic oxysalts

    Unknown journal · 2009-01-22

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  40. Preface

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  41. Structural Crystallography of Inorganic Oxysalts

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  42. Topology of framework structures in inorganic oxysalts

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  43. Channels occupancy and distortion in new lithium uranyl phosphates with three-dimensional open-frameworks

    Journal of Solid State Chemistry · 2009-02-27

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  44. A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems

    Journal of Solid State Chemistry · 2009-11-01

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  45. U(VI) oxygen polyhedra as pillars for building frameworks from uranophane-type layers

    IOP Conference Series Materials Science and Engineering · 2010-03-01

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  46. New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates

    Journal of Solid State Chemistry · 2010-07-25

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  47. Uranyl phosphate sheet reconstruction during dehydration of metatorbernite [Cu(UO2)2(PO4)2{middle dot}8H2O]

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  48. Linear Alkyl Diamine-Uranium-Phosphate Systems: U(VI) to U(IV) Reduction with Ethylenediamine

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  49. Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates

    Crystal Growth & Design · 2011-04-18

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  50. Synthesis, structure, and spectroscopic characterization of three uranyl phosphates with unique structural units

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