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RESEARCH PAPER · Inorganic Chemistry · 2003

A Novel Open Framework Uranyl Molybdate: Synthesis and Structure of (NH4)4[(UO2)5(MoO4)7](H2O)5

Sergey V. Krivovichev, Christopher L. Cahill, Peter Carman Burns

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A Novel Open Framework Uranyl Molybdate: Synthesis and Structure of (NH4)4[(UO2)5(MoO4)7](H2O)5OriginalA Novel Open Framework Uranyl Molybdate: Synthesis and Structure of (NH4)4 [(UO2)5(MoO4)7] (H2O)5.0Geometrical isomerism in uranyl chromates I. Crystal structures of (UO2)(CrO4)(H2O)2, [(UO2)(CrO4)(H2O)2](H2O) and [(UO2)(CrO4)(H2O)2]4(H2O)954The First Sodium Uranyl Chromate, Na4[(UO2)(CrO4)3]: Synthesis and Crystal Structure Determination39CRYSTAL CHEMISTRY OF URANYL MOLYBDATES. X. THE CRYSTAL STRUCTURE OF Ag10[(UO2)8O8(Mo5O20)]1522 New compounds and structures in the solid state2[N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride50Two new lithium uranyl tungstates Li2(UO2)(WO4)2 and Li2(UO2)4(WO4)4O with framework based on the uranophane sheet anion topology32Comparative study of the flexibility of structural complexes in uranyl sulfates, chromates, and molybdates28Synthesis and crystal structure of Cu2{(UO2)3[(S,Cr)O4]5}(H2O)179Cationic cobaltammines as anion receptors. Part V. Synthesis, characterization and X-ray structure of [CO(NH3)6]ClMoO4·3H2O39Chiral open-framework uranyl molybdates. 1. Topological diversity: synthesis and crystal structure of [(C2H5)2NH2]2[(UO2)4(MoO4)5(H2O)](H2O)53Chiral open-framework uranyl molybdates. 3. Synthesis, structure and the C2221→P212121 low-temperature phase transition of [C6H16N]2[(UO2)6(MoO4)7(H2O)2](H2O)24320 New compounds and structures in the solid state5Lone electron pair stereoactivity, cation arrangements and distortion of heteropolyhedral sheets in the structures of Tl2[(UO2)(AO4)2] (A = Cr, Mo)34Topology of Microporous Structures51Highly Porous Uranyl Selenate Nanotubules170Nanoscale Tubules in Uranyl Selenates122Nanoscale Tubules in Uranyl Selenates144CRYSTAL CHEMISTRY OF URANYL MOLYBDATES. XI. CRYSTAL STRUCTURES OF Cs2[(UO2)(MoO4)2] AND Cs2[(UO2)(MoO4)2](H2O)33Self‐Assembly of Protonated 1,12‐Dodecanediamine Molecules and Strongly Undulated Uranyl Selenate Sheets in the Structure of Amine‐Templated Uranyl Selenate: (H3O)2[C12H30N2]3[(UO2)4(SeO4)8](H2O)543Hydrothermal synthesis and crystal structures of new uranyl oxalate hydroxides: α- and β-[(UO2)2(C2O4)(OH)2(H2O)2] and [(UO2)2(C2O4)(OH)2(H2O)2]·H2O37Synthesis, Structure, and Properties of Inorganic Nanotubes Based on Uranyl Selenates9U6+ MINERALS AND INORGANIC COMPOUNDS: INSIGHTS INTO AN EXPANDED STRUCTURAL HIERARCHY OF CRYSTAL STRUCTURES627The A1−xUNbO6−x/2 compounds (x=0, A=Li, Na, K, Cs and x=0.5, A=Rb, Cs): from layered to tunneled structure15[NH4]4[UO2]5[MoO4]7[H2O]50Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)26An organic–inorganic hybrid uranyl nicotinate molybdate polymer and its fluorescent property16Structural Units in Three Uranyl Perrhenates33A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds90A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds11Synthesis, Structure, and Infrared Spectroscopy of the First Np5+ Neptunyl Silicates, Li6(NpO2)4(H2Si2O7)(HSiO4)2(H2O)4 and K3(NpO2)3(Si2O7)19Synthesis and structure of [C6H14N2][(UO2)4(HPO4)2(PO4)2(H2O)]·H2O: An expanded open-framework amine-bearing uranyl phosphate12An Open-Framework Thorium Sulfate Hydrate with 11.5 Å Voids42Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Amine-templated uranyl selenates with chiral [(UO2)2(SeO4)3(H2O)]2– layers: topology, isomerism, structural relationships31Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?18Hydrothermal Synthesis and Crystal Structures of Actinide Compounds2Unusual case of a polar copper(II) uranyl phosphonate that fluoresces14Use of Polyazaheterocycles in the Assembly of New Cadmium Sulfate Frameworks: Synthesis, Structure, and Properties38From ∞1[(UO2)2O(MoO4)4]6− to ∞1[(UO2)2(MoO4)3(MoO5)]6− infinite chains in A6U2Mo4O21 (A=Na, K, Rb, Cs) compounds: Synthesis and crystal structure of Cs6[(UO2)2(MoO4)3(MoO5)]9Uranyl carboxyphosphonates that incorporate Cd(II)20Unprecedented Bidentate Coordination of the Uranyl Cation by the Chromate Anion in the Structure of [(CH3)2CHNH3]2[UO2(CrO4)2]21Mixed-ligand coordination of the (UO2)2+ cation and apophyllite topology of uranyl chlorochromate layer in the structure of ((CH3)2CHNH3)[(UO2)(CrO4)Cl(H2O)]18In-Situ Raman Spectroscopy Studies of Room-Temperature and Hydrothermal Reactions1Structural topology and dimensional reduction in uranyl oxysalts: eight novel phases in the methylamine–(UO2)(NO3)2–H2SeO4–H2O system24Crystal Chemistry of Uranium Oxides and Minerals27High-Temperature Phase Transitions, Spectroscopic Properties, and Dimensionality Reduction in Rubidium Thorium Molybdate Family23Unexpected Structural Complexity in Cesium Thorium Molybdates18Structural and Morphological Influences on Neptunium Incorporation in Uranyl Molybdates1The structural effects of alkaline- and rare-earth element incorporation into thorium molybdates8A Revised and Expanded Structure Hierarchy of Natural and Synthetic Hexavalent Uranium Compounds172Investigation of reactivity and structure formation in a K–Te–U oxo-system under high-temperature/high-pressure conditions7Hydrolytically Stable Nanoporous Thorium Mixed Phosphite and Pyrophosphate Framework Generated from Redox-Active Ionothermal Reactions20Microporous uranyl chromates successively formed by evaporation from acidic solution9Expansion of the structural diversity of f-element bearing molybdate iodates: synthesis, structures, and optical properties19Crystal Chemistry and Structural Complexity of the Uranyl Molybdate Minerals and Synthetic Compounds9Uranyl-Tc( vii )/Tc( v ) hybrid clusters5Results of 25-Year Studies of Uranium Compounds at the Department of Crystallography of St. Petersburg State University3

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  1. A Novel Open Framework Uranyl Molybdate: Synthesis and Structure of (NH4)4 [(UO2)5(MoO4)7] (H2O)5.

    ChemInform · 2003-07-01

    Sergey V. Krivovichev, Christopher L. Cahill, Peter Carman Burns

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  2. Geometrical isomerism in uranyl chromates I. Crystal structures of (UO2)(CrO4)(H2O)2, [(UO2)(CrO4)(H2O)2](H2O) and [(UO2)(CrO4)(H2O)2]4(H2O)9

    Zeitschrift für Kristallographie - Crystalline Materials · 2003-08-01

    Sergey V. Krivovichev, Peter Carman Burns

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  3. The First Sodium Uranyl Chromate, Na4[(UO2)(CrO4)3]: Synthesis and Crystal Structure Determination

    Zeitschrift für anorganische und allgemeine Chemie · 2003-10-01

    Sergey V. Krivovichev, Peter Carman Burns

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  4. CRYSTAL CHEMISTRY OF URANYL MOLYBDATES. X. THE CRYSTAL STRUCTURE OF Ag10[(UO2)8O8(Mo5O20)]

    The Canadian Mineralogist · 2003-12-01

    Sergey V. Krivovichev, Peter Carman Burns

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  5. 22 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2004-01-01

    Gary B. Hix

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  6. [N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride

    Chemistry of Materials · 2004-01-30

    M.B. Doran, Clair L. Stuart, Alexander J. Norquist, Dermot M. O'Hare

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  7. Two new lithium uranyl tungstates Li2(UO2)(WO4)2 and Li2(UO2)4(WO4)4O with framework based on the uranophane sheet anion topology

    Journal of Solid State Chemistry · 2004-02-17

    S. Obbade, S. Yagoubi, C. Dion, Mohamed Saadi, F. Abraham

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  8. Comparative study of the flexibility of structural complexes in uranyl sulfates, chromates, and molybdates

    Radiochemistry · 2004-09-01

    Sergey V. Krivovichev

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  9. Synthesis and crystal structure of Cu2{(UO2)3[(S,Cr)O4]5}(H2O)17

    Radiochemistry · 2004-09-01

    Sergey V. Krivovichev, Peter Carman Burns

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  10. Cationic cobaltammines as anion receptors. Part V. Synthesis, characterization and X-ray structure of [CO(NH3)6]ClMoO4·3H2O

    Journal of Coordination Chemistry · 2004-11-20

    R.P. Sharma, R.P. Sharma, Ritu Bala, R.P. Sharma, R.P. Sharma, Paloth Venugopalan

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  11. Chiral open-framework uranyl molybdates. 1. Topological diversity: synthesis and crystal structure of [(C2H5)2NH2]2[(UO2)4(MoO4)5(H2O)](H2O)

    Microporous and Mesoporous Materials · 2004-12-16

    Sergey V. Krivovichev, Christopher L. Cahill, Еvgeny V. Nazarchuk, Peter Carman Burns, Thomas Armbruster, Wulf Depmeier

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  12. Chiral open-framework uranyl molybdates. 3. Synthesis, structure and the C2221→P212121 low-temperature phase transition of [C6H16N]2[(UO2)6(MoO4)7(H2O)2](H2O)2

    Microporous and Mesoporous Materials · 2004-12-16

    Sergey V. Krivovichev, Thomas Armbruster, Dmitry Chernyshov, Peter Carman Burns, Еvgeny V. Nazarchuk, Wulf Depmeier

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  13. 20 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2005-01-01

    Gary B. Hix

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  14. Lone electron pair stereoactivity, cation arrangements and distortion of heteropolyhedral sheets in the structures of Tl2[(UO2)(AO4)2] (A = Cr, Mo)

    Zeitschrift für Kristallographie - Crystalline Materials · 2005-01-01

    Sergey V. Krivovichev, Andrew J. Locock, Peter Carman Burns

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  15. Topology of Microporous Structures

    Reviews in Mineralogy and Geochemistry · 2005-01-01

    Sergey V. Krivovichev

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  16. Highly Porous Uranyl Selenate Nanotubules

    Journal of the American Chemical Society · 2005-01-06

    Sergey V. Krivovichev, Volker Kahlenberg, Ivan Gundarovich Tananaev, Reinhard Kaindl, Edgar Mersdorf, Boris F. Myasoedov

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  17. Nanoscale Tubules in Uranyl Selenates

    Angewandte Chemie · 2005-01-11

    Sergey V. Krivovichev, Volker Kahlenberg, Reinhard Kaindl, Edgar Mersdorf, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  18. Nanoscale Tubules in Uranyl Selenates

    Angewandte Chemie International Edition · 2005-01-11

    Sergey V. Krivovichev, Volker Kahlenberg, Reinhard Kaindl, Edgar Mersdorf, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  19. CRYSTAL CHEMISTRY OF URANYL MOLYBDATES. XI. CRYSTAL STRUCTURES OF Cs2[(UO2)(MoO4)2] AND Cs2[(UO2)(MoO4)2](H2O)

    The Canadian Mineralogist · 2005-04-01

    Sergey V. Krivovichev, Peter Carman Burns

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  20. Self‐Assembly of Protonated 1,12‐Dodecanediamine Molecules and Strongly Undulated Uranyl Selenate Sheets in the Structure of Amine‐Templated Uranyl Selenate: (H3O)2[C12H30N2]3[(UO2)4(SeO4)8](H2O)5

    European Journal of Inorganic Chemistry · 2005-04-28

    Sergey V. Krivovichev, Volker Kahlenberg, Evgeniya Y. Avdontseva, Edgar Mersdorf, Reinhard Kaindl

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  21. Hydrothermal synthesis and crystal structures of new uranyl oxalate hydroxides: α- and β-[(UO2)2(C2O4)(OH)2(H2O)2] and [(UO2)2(C2O4)(OH)2(H2O)2]·H2O

    Journal of Solid State Chemistry · 2005-10-03

    L. Duvieubourg, G. Nowogrocki, F. Abraham, S. Grandjean

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  22. Synthesis, Structure, and Properties of Inorganic Nanotubes Based on Uranyl Selenates

    Radiochemistry · 2005-11-01

    Sergey V. Krivovichev, Ivan Gundarovich Tananaev, Volker Kahlenberg, Reinhard Kaindl, Boris F. Myasoedov

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  23. U6+ MINERALS AND INORGANIC COMPOUNDS: INSIGHTS INTO AN EXPANDED STRUCTURAL HIERARCHY OF CRYSTAL STRUCTURES

    The Canadian Mineralogist · 2005-12-01

    Peter Carman Burns

    Read original paper ↗ ·

  24. The A1−xUNbO6−x/2 compounds (x=0, A=Li, Na, K, Cs and x=0.5, A=Rb, Cs): from layered to tunneled structure

    Journal of Solid State Chemistry · 2006-06-22

    Suzy Surblé, S. Obbade, S. Saad, S. Yagoubi, C. Dion, F. Abraham

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  25. [NH4]4[UO2]5[MoO4]7[H2O]5

    Numerical data and functional relationships in science and technology. Group III, Condensed matter · 2007-01-01

    Pierre Villars, Karin CENZUAL, J.L.C. Daams, Roman E. GLADYSHEVSKII, O. Shcherban, Vitaly Dubenskyy, N. Koblyuk, Oksana PAVLYUK, Igor SAVYSYUK, S. Stoyko, L. V. SYSA

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  26. Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)

    Elsevier eBooks · 2007-01-01

    Sergey V. Krivovichev, Peter Carman Burns

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  27. An organic–inorganic hybrid uranyl nicotinate molybdate polymer and its fluorescent property

    Inorganic Chemistry Communications · 2007-04-05

    Xiang‐Jian Kong, Yanping Ren, La‐Sheng Long, Rong‐Bin Huang, Lan‐Sun Zheng

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  28. Structural Units in Three Uranyl Perrhenates

    Inorganic Chemistry · 2007-10-31

    Oxana V. Karimova, Peter Carman Burns

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  29. A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds

    Angewandte Chemie International Edition · 2007-12-03

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

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  30. A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds

    Angewandte Chemie · 2007-12-03

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

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  31. Synthesis, Structure, and Infrared Spectroscopy of the First Np5+ Neptunyl Silicates, Li6(NpO2)4(H2Si2O7)(HSiO4)2(H2O)4 and K3(NpO2)3(Si2O7)

    Inorganic Chemistry · 2007-12-18

    Tori Z. Forbes, Peter Carman Burns

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  32. Synthesis and structure of [C6H14N2][(UO2)4(HPO4)2(PO4)2(H2O)]·H2O: An expanded open-framework amine-bearing uranyl phosphate

    Journal of Solid State Chemistry · 2008-05-17

    Travis H. Bray, John D. Gorden, Thomas E. Albrecht‐Schmitt

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  33. An Open-Framework Thorium Sulfate Hydrate with 11.5 Å Voids

    Inorganic Chemistry · 2008-09-24

    Richard E. Wilson, S. Skanthakumar, Karah E. Knope, Christopher L. Cahill, L. Soderholm

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  34. Alternative approaches to structure description

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  35. Anion-topology approach

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  36. Basic concepts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  37. Copyright Page

    Unknown journal · 2009-01-22

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  38. Dedication

    Unknown journal · 2009-01-22

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  39. Dimensional reduction in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  40. Graph theory applied to low-dimensional structural units in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  41. Preface

    Unknown journal · 2009-01-22

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  42. Structural Crystallography of Inorganic Oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  43. Topology of framework structures in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

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  44. Amine-templated uranyl selenates with chiral [(UO2)2(SeO4)3(H2O)]2– layers: topology, isomerism, structural relationships

    Zeitschrift für Kristallographie · 2009-05-01

    Sergey V. Krivovichev, Vladislav V. Gurzhiy, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  45. Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?

    Inorganic Chemistry · 2009-10-30

    Jie Ling, Shijun Wu, Fanrong Chen, Antonio Simonetti, J. T. Shafer, Thomas E. Albrecht‐Schmitt

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  46. Hydrothermal Synthesis and Crystal Structures of Actinide Compounds

    Springer eBooks · 2010-01-01

    Wolfgang Runde, Mary P. Neu

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  47. Unusual case of a polar copper(II) uranyl phosphonate that fluoresces

    Comptes Rendus Chimie · 2010-05-05

    Anna‐Gay D. Nelson, Thomas E. Albrecht‐Schmitt

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  48. Use of Polyazaheterocycles in the Assembly of New Cadmium Sulfate Frameworks: Synthesis, Structure, and Properties

    Crystal Growth & Design · 2010-08-04

    Avijit Kumar Paul, Udishnu Sanyal, Srinivasan Natarajan

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  49. From ∞1[(UO2)2O(MoO4)4]6− to ∞1[(UO2)2(MoO4)3(MoO5)]6− infinite chains in A6U2Mo4O21 (A=Na, K, Rb, Cs) compounds: Synthesis and crystal structure of Cs6[(UO2)2(MoO4)3(MoO5)]

    Journal of Solid State Chemistry · 2011-03-07

    S. Yagoubi, S. Obbade, S. Saad, F. Abraham

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  50. Uranyl carboxyphosphonates that incorporate Cd(II)

    Journal of Solid State Chemistry · 2011-04-14

    A.N. Alsobrook, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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