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RESEARCH PAPER · Inorganic Chemistry · 2011

Occurence of an Octanuclear Motif of Uranyl Isophthalate with Cation–Cation Interactions through Edge-Sharing Connection Mode

Ionut Mihalcea, Natacha Henry, Nicolas Clavier, Nicolas Dacheux, Thierry Loiseau

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Occurence of an Octanuclear Motif of Uranyl Isophthalate with Cation–Cation Interactions through Edge-Sharing Connection ModeOriginalIn situ oxalate formation during hydrothermal synthesis of uranyl hybrid materials50Three-Dimensional Hybrid Framework Containing U2O13 Dimers Connected via Cation–Cation Interactions48Crystal Engineering with the Uranyl Cation III. Mixed Aliphatic Dicarboxylate/Aromatic Dipyridyl Coordination Polymers: Synthesis, Structures, and Speciation74Uranyl–Pyromellitate Coordination Polymers: Toward Three-Dimensional Open Frameworks with Large Channel Systems83Uranyl and/or Rare-Earth Mellitates in Extended Organic–Inorganic Networks: A Unique Case of Heterometallic Cation–Cation Interaction with UVI═O–LnIII Bonding (Ln = Ce, Nd)117Magnetic communication and reactivity of a stable homometallic cation–cation trimer of pentavalent uranyl73Four Low-Dimensional Cobalt(II) Coordination Polymers Based on a New Isophthalic Acid Derivative: Syntheses, Crystal Structures, and Properties55(UO2)2[UO4(trz)2](OH)2: A U(VI) Coordination Intermediate between a Tetraoxido Core and a Uranyl Ion with Cation–Cation Interactions43A Series of Cd(II) and Zn(II) Coordination Polymers with Helical Subunits Assembled from a Versatile 3-(4-hydroxypyridinium-1-yl) Phthalic Acid and N-Donor Ancillary Coligands56Tailor-Made Zinc Uranyl Diphosphonates from Layered to Framework Structures46Ring-Opening Polymerization of Epoxides Catalyzed by Uranyl Complexes: An Experimental and Theoretical Study of the Reaction Mechanism27Uranyl Bearing Hybrid Materials: Synthesis, Speciation, and Solid-State Structures418Six-Fold Coordinated Uranyl Cations in Extended Coordination Polymers82Copper uranyl phosphate and arsenate incorporating an organic ligand with a pillared layer structure: [Cu(4,4′-bpy)(UO2)0.5(HPO4)(H2PO4)]·H2O and [Cu(4,4′-bpy)(UO2)0.5(HAsO4)(H2AsO4)]·1.5H2O15Series of Mixed Uranyl–Lanthanide (Ce, Nd) Organic Coordination Polymers with Aromatic Polycarboxylates Linkers92One-Dimensional Uranyl-2,2′-bipyridine Coordination Polymer with Cation–Cation Interactions: (UO2)2(2,2′-bpy)(CH3CO2)(O)(OH)44From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange82Solution and Solid-State Structural Chemistry of Actinide Hydrates and Their Hydrolysis and Condensation Products372New Reactivity of the Uranyl(VI) Ion116Four New Cd(II) Coordination Polymers with Mixed Multidentate N-Donors and Biphenyl-Based Polycarboxylate Ligands: Syntheses, Structures, and Photoluminescent Properties208Sulfonate Complexes of Actinide Ions: Structural Diversity in Uranyl Complexes with 2-Sulfobenzoate71Structural Observations of Heterometallic Uranyl Copper(II) Carboxylates and Their Solid‐State Topotactic Transformation upon Dehydration63One- to three-dimensional uranyl–organic assemblies with 3-sulfophthalic and 5-sulfoisophthalic acids29Transuranium Inorganic Chemistry4Uranyl–3d block metal ion heterometallic carboxylate complexes including additional chelating nitrogen donors37Synthesis, Structures, and Luminescent Properties of Uranyl Terpyridine Aromatic Carboxylate Coordination Polymers85Synthesis, Structural Characterization, and Dehydration Analysis of Uranyl Zinc Mellitate, (UO2)Zn(H2O)4(H2mel)·2H2O31Comparisons of Plutonium, Thorium, and Cerium Tellurite Sulfates41Crystal structure of [M(H2O)6][UO2(CH3COO)3]2 (M=Mg2+, Co2+ and Zn2+)17Self‐Assembly of Four Helical Metal–Organic Frameworks Based on 3‐[4‐(Carboxymethoxy)phenyl]propanoic Acid Ligands: Syntheses, Crystal Structures, and Properties15Series of Uranyl-4,4′-biphenyldicarboxylates and an Occurrence of a Cation–Cation Interaction: Hydrothermal Synthesis and in Situ Raman Studies36Synthesis and Structural Characterization of Hydrolysis Products within the Uranyl Iminodiacetate and Malate Systems25The crystal chemistry of uranium carboxylates394Uranyl Coordination Polymers Incorporating η5-Cyclopentadienyliron-Functionalized η6-Phthalate Metalloligands: Syntheses, Structures and Photophysical Properties29Thermochromism, the Alexandrite Effect, and Dynamic Jahn–Teller Distortions in Ho2Cu(TeO3)2(SO4)221Synthesis and Crystal Structure of Two Coordination Polymers Assembled from a Versatile 4-(4-Hydroxypyridinium-1-yl)phthalic Acid7Crystal growth, structural characterization, cation–cation interaction classification, and optical properties of uranium( vi ) containing oxychlorides, A 4 U 5 O 16 Cl 2 (A = K, Rb), Cs 5 U 7 O 22 Cl 3 , and AUO 3 Cl (A = Rb, Cs)27Synthesis, structures, characterization and antimicrobial activity of two novel coordination complexes derived from 2-naphthoxyacetic acid4Tuning Different Kinds of Entangled Networks by Varying N-Donor Ligands: From Self-Penetrating to Multi-interpenetrating70A Series of Transition-metal Coordination Complexes Assembled from 3-Nitrophthalic Acid and Thiabendazole: Synthesis, Structure and Properties5Uranyl–Organic Frameworks with Polycarboxylates: Unusual Effects of a Coordinating Solvent77Crystal Chemistry of Uranyl Carboxylate Coordination Networks Obtained in the Presence of Organic Amine Molecules60Cation–cation interactions and cation exchange in a series of isostructural framework uranyl tungstates17Postsynthetic Rearrangement/Metalation as a Route to Bimetallic Uranyl Coordination Polymers: Syntheses, Structures, and Luminescence70Cation-cation interactions between uranyl(VI) ions31Construction of Three Novel Coordination Complexes by 3-Nitrophthalic Acid Plus N-Donor Ligands: Synthesis, Structure, and Properties1A 3D cadmium coordination polymer with 2-fold interpenetration structure and helical chains based on biphenyl-4-hydroxyl-3,3′-bicarboxylic acid: Synthesis and crystal structure and properties3A Novel Co(II) Coordination Polymer Assembled from V-shaped 2,3,2’,3’-Thiodiphthalic Acid and N-donor Ancillary Ligand: Syntheses, Structure and Properties2Uranyl Ion Complexes with all-cis-1,3,5-Cyclohexanetricarboxylate: Unexpected Framework and Nanotubular Assemblies55The structure hierarchy hypothesis44The First Family of Actinide Carboxyphosphinates: Two‐ and Three‐Dimensional Uranyl Coordination Polymers27Synthesis, structural investigation and kinetic studies of uranyl(VI) unsymmetrical Schiff base complexes14A family of 3D UO 2 2+ –5-X-1,3-dicarboxylate (X = –H, –NO 2 , –NH 2 , –OH) hybrid materials: structural relevance with variation of substituent groups and photochemical properties29Flux crystal growth and structural analysis of two cesium uranium oxides, Cs 2.2 U 5 O 16 and Cs 2 U 4 O 13 , containing multiple cation–cation interactions9Hybrid Materials of the f-Elements Part I5Hybrid Materials of the f-Elements Part II5Solvent effects in solvo-hydrothermal synthesis of uranyl ion complexes with 1,3-adamantanediacetate33Two novel uranyl complexes of a semi-rigid aromatic tetracarboxylic acid supported by an organic base as an auxiliary ligand or a templating agent: an experimental and theoretical exploration16Uranium( vi ) complexes with isonicotinic acid: from monomer to 2D polymer with unique U–N bonding43A Copper Coordination Polymer Based on 3-(4-Hydroxypyridinium-1-yl) Phthalic Acid: Synthesis and Crystal Structure3Uranyl and Uranyl–3d Block Cation Complexes with 1,3-Adamantanedicarboxylate: Crystal Structures, Luminescence, and Magnetic Properties68Uranyl Ion Complexes with 1,1′-Biphenyl-2,2′,6,6′-tetracarboxylic Acid: Structural and Spectroscopic Studies of One- to Three-Dimensional Assemblies36Synthesis and structure of dimeric complexes of U(VI) and Np(VI) with isophthalic acid anions, {AnO2[C6H4(COO)(COOH)]2(H2O)}25Evaluating Best Practices in Raman Spectral Analysis for Uranium Speciation and Relative Abundance in Aqueous Solutions55Solvothermal synthesis of uranium(VI) phases with aromatic carboxylate ligands: A dinuclear complex with 4-hydroxybenzoic acid and a 3D framework with terephthalic acid28Synthesis and structural features of Np(VI) and Pu(VI) isophthalates2Novel Uranyl Coordination Polymers Based on Quinoline-Containing Dicarboxylate by Altering Auxiliary Ligands: From 1D Chain to 3D Framework31Tellurites of Hexavalent Uranium: First Observation of Polymerized (UO4)2– Tetraoxido Cores5Recent advances in structural studies of heterometallic uranyl-containing coordination polymers and polynuclear closed species93Complexes of Uranyl Ions with Aromatic Di‐ and Tetracarboxylates Involving [Ni(bipy)n]2+ (n = 2, 3) Counterions12Novel Viologen Derivative Based Uranyl Coordination Polymers Featuring Photochromic Behaviors61An Anionic Uranium-Based Metal–Organic Framework with Ultralarge Nanocages for Selective Dye Adsorption67Speciation of Actinide Complexes, Clusters, and Nanostructures in Solution2Template-Driven Assembly of Rare Hexameric Uranyl-Organic Rotaxane Networks Threaded on Dimeric Uranyl Chains11Photocatalytic degradation of tetracycline antibiotics under visible light using uranyl isophthalate coordination polymers10Detection and identification of solids, surfaces, and solutions of uranium using vibrational spectroscopy179Emerging investigator series: significantly enhanced uptake of Eu 3+ on a nanoporous zeolitic mineral in the presence of UO 2 2+ : insights into the impact of cation–cation interaction on the geochemical behavior of lanthanides and actinides27In situ nitroso formation induced structural diversity of uranyl coordination polymers21Uranyl Compounds Involving a Weakly Bonded Pseudorotaxane Linker: Combined Effect of pH and Competing Ligands on Uranyl Coordination and Speciation33A Uranyl Metal Organic Framework Arising from the Coordination of a Partially Hydrolyzed Tetrauranyl Node with the Tautomerically Diverse 1,4-(Diamidoximyl)benzene Ligand11Two uranium coordination polymers constructed by a polycarboxylic acid: Structural variation, photoluminescent and photocatalysis properties18Occurrence of polyoxouranium motifs in uranyl organic networks constructed by using silicon-centered carboxylate linkers: structures, spectroscopy and computation11Controlling Cation‐Cation Interactions in Uranyl Coordination Dimers by Varying the Length of the Dicarboxylate Linker4A Robust Titanium Isophthalate Metal-Organic Framework for Visible-Light Photocatalytic CO2 Methanation87A stable mixed-valent uranium( v , vi ) organic framework as a fluorescence thermometer28Sandwiched Kagomé Lattices in a Coordination Polymer Based on Mixed-Valent Uranium5Contrasting Structure-Directing Effects in the Uranyl–Phthalate/Isophthalate Isomer Systems19A self-assembled supramolecular organic material for selective extraction of uranium from aqueous solution10Evidence of a Uranium‐Paddlewheel Node in a Catecholate‐Based Metal–Organic Framework0Evidence of a Uranium‐Paddlewheel Node in a Catecholate‐Based Metal–Organic Framework6The crystal structure of poly[(μ 2-2-aminoisophthalato-κ4O,O′:O″:O″′)-(N-methylpyrrolidone κ1O)-dioxido-uranium(VI)], C13H14N2O7U1Uranyl‐Nickel(II) Cation‐Cation Interaction in a Triperiodic Framework with cis‐1,2‐Cyclohexanedicarboxylate and Isonicotinate Ligands1Tuning N-donor coordination and assembly structures in uranyl compounds of carboxylate ligands with divergent vinyl pyridine groups1Results of 25-Year Studies of Uranium Compounds at the Department of Crystallography of St. Petersburg State University3

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  2. Three-Dimensional Hybrid Framework Containing U2O13 Dimers Connected via Cation–Cation Interactions

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  4. Uranyl–Pyromellitate Coordination Polymers: Toward Three-Dimensional Open Frameworks with Large Channel Systems

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  5. Uranyl and/or Rare-Earth Mellitates in Extended Organic–Inorganic Networks: A Unique Case of Heterometallic Cation–Cation Interaction with UVI═O–LnIII Bonding (Ln = Ce, Nd)

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  6. Magnetic communication and reactivity of a stable homometallic cation–cation trimer of pentavalent uranyl

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  7. Four Low-Dimensional Cobalt(II) Coordination Polymers Based on a New Isophthalic Acid Derivative: Syntheses, Crystal Structures, and Properties

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  8. (UO2)2[UO4(trz)2](OH)2: A U(VI) Coordination Intermediate between a Tetraoxido Core and a Uranyl Ion with Cation–Cation Interactions

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  9. A Series of Cd(II) and Zn(II) Coordination Polymers with Helical Subunits Assembled from a Versatile 3-(4-hydroxypyridinium-1-yl) Phthalic Acid and N-Donor Ancillary Coligands

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  10. Tailor-Made Zinc Uranyl Diphosphonates from Layered to Framework Structures

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  11. Ring-Opening Polymerization of Epoxides Catalyzed by Uranyl Complexes: An Experimental and Theoretical Study of the Reaction Mechanism

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  13. Six-Fold Coordinated Uranyl Cations in Extended Coordination Polymers

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  14. Copper uranyl phosphate and arsenate incorporating an organic ligand with a pillared layer structure: [Cu(4,4′-bpy)(UO2)0.5(HPO4)(H2PO4)]·H2O and [Cu(4,4′-bpy)(UO2)0.5(HAsO4)(H2AsO4)]·1.5H2O

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  15. Series of Mixed Uranyl–Lanthanide (Ce, Nd) Organic Coordination Polymers with Aromatic Polycarboxylates Linkers

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  16. One-Dimensional Uranyl-2,2′-bipyridine Coordination Polymer with Cation–Cation Interactions: (UO2)2(2,2′-bpy)(CH3CO2)(O)(OH)

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  17. From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange

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  19. New Reactivity of the Uranyl(VI) Ion

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  21. Sulfonate Complexes of Actinide Ions: Structural Diversity in Uranyl Complexes with 2-Sulfobenzoate

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  22. Structural Observations of Heterometallic Uranyl Copper(II) Carboxylates and Their Solid‐State Topotactic Transformation upon Dehydration

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  36. Synthesis and Crystal Structure of Two Coordination Polymers Assembled from a Versatile 4-(4-Hydroxypyridinium-1-yl)phthalic Acid

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  37. Crystal growth, structural characterization, cation–cation interaction classification, and optical properties of uranium( vi ) containing oxychlorides, A 4 U 5 O 16 Cl 2 (A = K, Rb), Cs 5 U 7 O 22 Cl 3 , and AUO 3 Cl (A = Rb, Cs)

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  38. Synthesis, structures, characterization and antimicrobial activity of two novel coordination complexes derived from 2-naphthoxyacetic acid

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  39. Tuning Different Kinds of Entangled Networks by Varying N-Donor Ligands: From Self-Penetrating to Multi-interpenetrating

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  40. A Series of Transition-metal Coordination Complexes Assembled from 3-Nitrophthalic Acid and Thiabendazole: Synthesis, Structure and Properties

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  41. Uranyl–Organic Frameworks with Polycarboxylates: Unusual Effects of a Coordinating Solvent

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  42. Crystal Chemistry of Uranyl Carboxylate Coordination Networks Obtained in the Presence of Organic Amine Molecules

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  43. Cation–cation interactions and cation exchange in a series of isostructural framework uranyl tungstates

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  44. Postsynthetic Rearrangement/Metalation as a Route to Bimetallic Uranyl Coordination Polymers: Syntheses, Structures, and Luminescence

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  45. Cation-cation interactions between uranyl(VI) ions

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  46. Construction of Three Novel Coordination Complexes by 3-Nitrophthalic Acid Plus N-Donor Ligands: Synthesis, Structure, and Properties

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  47. A 3D cadmium coordination polymer with 2-fold interpenetration structure and helical chains based on biphenyl-4-hydroxyl-3,3′-bicarboxylic acid: Synthesis and crystal structure and properties

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  48. A Novel Co(II) Coordination Polymer Assembled from V-shaped 2,3,2’,3’-Thiodiphthalic Acid and N-donor Ancillary Ligand: Syntheses, Structure and Properties

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  49. Uranyl Ion Complexes with all-cis-1,3,5-Cyclohexanetricarboxylate: Unexpected Framework and Nanotubular Assemblies

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  50. The structure hierarchy hypothesis

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