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RESEARCH PAPER · Journal of Solid State Chemistry · 2010

Hydrazine-hydrothermal method to synthesize three-dimensional chalcogenide framework for photocatalytic hydrogen generation

Yi Liu, Pushkar D. Kanhere, Chui Ling Wong, Yuefeng Tian, Yuhua Feng, Freddy Boey, Tom Wu, Hongyu Chen, Timothy John White, Zhong Chen, Qichun Zhang

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Hydrazine-hydrothermal method to synthesize three-dimensional chalcogenide framework for photocatalytic hydrogen generationOriginalVisible-light-driven photocatalytic water splitting on nanostructured semiconducting materials94ChemInform Abstract: Hydrazine‐Hydrothermal Method to Synthesize Three‐Dimensional Chalcogenide Framework for Photocatalytic Hydrogen Generation.0A new hydrazine-bridged thioantimonate Mn2Sb4S8(N2H4)2: Synthesis, structure, optical and magnetic properties43Optical properties of amorphous CuS thin films deposited chemically at different pH values115Assembly of novel organic-decorated quaternary TM–Hg–Sb–Q compounds (TM = Mn, Fe, Co; Q = S, Se) by the combination of three types of metal coordination geometries72Reaction pathways for the formation of Cu2ZnSn(Se,S)4 absorber materials from liquid-phase hydrazine-based precursor inks60Slow magnetic relaxation in one dimensional nitronyl nitroxide-Dy(III) chain suggesting single-chain magnet behavior14Two Zeolite‐Type Frameworks in One Metal–Organic Framework with Zn 24 @Zn 104 Cube‐in‐Sodalite Architecture69Two Zeolite‐Type Frameworks in One Metal–Organic Framework with Zn 24 @Zn 104 Cube‐in‐Sodalite Architecture9Synthesis, structure and characterization of two new copper(І)-thioarsenates (ІІІ) constructed by the [AsS3]3− and CuS units25[AEPH2][GeSb2S6]·CH3OH: a thiogermanate–thioantimonate featuring an infinite ribbon-like structure with an unusual {GeSb3S11} unit and exhibiting the ability of photocatalytic degradation of organic dye29Nanostructured Inorganic–Organic Hybrid Semiconductor Materials3Solvothermal syntheses, crystal structures, and properties of new mercury(II)–thioantimonates(III) and a mixed-valent thioantimonate(III,V)21Base-Induced Dehydrogenation of Ruthenium Hydrazine Complexes39Influence of Replacing Si by Ge in the Chalcogenide Quaternary Sulfides Ag2In2Si(Ge)S6 on the Chemical Bonding, Linear and Nonlinear Optical Susceptibilities, and Hyperpolarizability38Coassembly between the Largest and Smallest Metal Chalcogenide Supertetrahedral Clusters36Self-assembled cabbage-like NaInS2 microstructures with efficient visible light photocatalytic performance4Changes in the Structural Dimensionality of Selenidostannates in Ionic Liquids: Formation, Structures, Stability, and Photoconductivity50A Sulfide‐Bridged Diiron(II) Complex with a N2H4 Ligand21Solvothermal syntheses of three new one-dimensional ternary selenidostannates: [DBNH][M1/2Sn1/2Se2] (M=Mn, Zn, Hg)14Syntheses, crystal structures, and properties of two new one-dimensional heterometallic selenides: [DBNH]4[M3Sn4Se11(Se2)2] (M = Cd, Hg)14Synthesis, crystal structure and properties of [(dien)2Mn]Ge2S4 with mixed-valent Ge centers12Surfactant–Thermal Method to Synthesize a Novel Two‐Dimensional Oxochalcogenide79[TM(en)3][SnSb4S9] (TM = Ni, Co): 3D Chiral Framework of Mixed Main-Group Metals and [Mn(dien)2]2Sb4S9: 1D Chains with Mixed-Valent Sb Centers54[enH][Cu 2 AgSnS 4 ]: a quaternary layered sulfide based on Cu–Ag–Sn–S composition45Monodisperse CuS nanodisks: low-temperature solvothermal synthesis and enhanced photocatalytic activity19New strategies to prepare crystalline chalcogenides165Two manganese–amine complexes incorporating thioantimonates and exhibiting diversiform roles of amine ligands20Syntheses, Crystal Structures, and Photocatalytic Properties of a Series of Mercury Thioantimonates Directed by Transition Metal Complexes69Preparation by Solvothermal Synthesis, Growth Mechanism, and Photocatalytic Performance of CuS Nanopowders70Mild Solvothermal Syntheses and Characterization of Layered Copper Thioantimonates(III) and Thioarsenate(III)44Structures and properties of ion pair charge-transfer salts: [DMBPE]2Ge4S10 (DMBPE = N,N′-dimethyl-1,2-bis(4-pyridinium)-ethylene)6{[M(NH3)6][Ag4M4Sn3Se13]}∞ (M=Zn, Mn): Three-dimensional chalcogenide frameworks constructed from quaternary metal selenide clusters with two different transition metals23Surfactant-thermal method to prepare two novel two-dimensional Mn–Sb–S compounds for photocatalytic applications32Surfactant-Thermal Syntheses, Structures, and Magnetic Properties of Mn–Ge–Sulfides/Selenides45New Members of the Family of In–Sb–S Compounds: Different Roles of Organic Amines20Ubiquitous quantum dot-sensitized nanoporous film for hydrogen production under visible-light irradiation9Synthesis, crystal structure and optical property of a novel metal chalcohalide: ZnHg3Se2Cl47Hydrazine-Hydrothermal Synthesis and Characterization of the Two New Quaternary Thioantimonates(III) BaAgSbS3 and BaAgSbS3·H2O40Preparation of Porous Three‐Dimensional Quaternary Thioantimonates(III) ACuSb2S4 (A=Rb, Cs) through a Surfactant‐Thermal Method29Facile surfactant-thermal syntheses and characterization of quaternary copper thioantimonates(III) ACu 2 SbS 3 (A = K, Rb, Cs)23Synthese kristalliner Chalkogenide in ionischen Flüssigkeiten43Synthesis of Crystalline Chalcogenides in Ionic Liquids150Controllable synthesis of Bi 2 S 3 /CuS heterostructures by an in situ ion-exchange solvothermal process and their enhanced photocatalytic performance25Surfactants as additives make the structures of organic–inorganic hybrid bromoplumbates diverse38Nanostructured Conjugated Polymers for Energy‐Related Applications beyond Solar Cells166Hydrazine-hydrothermal syntheses, characterizations and photoelectrochemical properties of two quaternary chalcogenidoantimonates(III) BaCuSbQ3 (Q = S, Se)51Facile Hydrazine‐Hydrothermal Syntheses and Characterizations of Two Quaternary Thioarsenates(III): Two‐Dimensional SrAg4As2S6⋅2 H2O and One‐Dimensional BaAgAsS320Organically directed heterometallic chalcogenidometalates containing group 12(II)/13(III)/14(IV) metal ions and antimony(III)68Effect of alkali cations on two-dimensional networks of two new quaternary thioarsenates (III) prepared by a facile surfactant-thermal method13Effect of HNO3 Concentration on the Morphologies and Properties of Bi2WO6 Photocatalyst Synthesized by a Hydrothermal Method24Unprecedented 3D and 2D Frameworks of Manganese Thioarsenates Based on Heterometallic Cubic Cluster [Mn6(µ6‐S)(AsS3)4] and Covalent Linker N2H46Tetra-EDOT substituted 3D electrochromic polymers with lower band gaps9Multitopic ligand directed assembly of low-dimensional metal-chalcogenide organic frameworks5Recent progress in crystalline metal chalcogenides as efficient photocatalysts for organic pollutant degradation179Syntheses, crystal structures, and photocatalytic properties of two ammonium-directed Ag–Sb–S complexes30Hydrazine-Assisted Syntheses and Properties of Mercury Tellurides Containing Transition-Metal Complexes20Different roles of hydrazine as a complexant, alkali resource and reductant on reacting with metal ions for material synthesis7Integrating Zeolite-Type Chalcogenide with Titanium Dioxide Nanowires for Enhanced Photoelectrochemical Activity19Hydrazine-solvothermal methods to synthesize polymeric thioarsenates from one-dimensional chains to a three-dimensional framework8Ionothermal synthesis of discrete supertetrahedral T n ( n = 4, 5) clusters with tunable components, band gaps, and fluorescence properties57Surface Decorated Zn0.15Cd0.85S Nanoflowers with P25 for Enhanced Visible Light Driven Photocatalytic Degradation of Rh-B and Stability7Exploring the Surfactant–Thermal Synthesis of Crystalline Functional Thioarsenates48Supertetrahedral Cluster-Based In–Se Open Frameworks with Unique Polyselenide Ion as Linker9Enhanced photocatalytic activity in hybrid composite combined BiOBr nanosheets and Bi2S3 nanoparticles54Hybrid Assembly of Different-Sized Supertetrahedral Clusters into a Unique Non-Interpenetrated Mn–In–S Open Framework with Large Cavity17A 3D Haloplumbate Framework Constructed From Unprecedented Lindqvist‐like Highly Coordinated [Pb6Br25]13− Nanoclusters with Temperature‐Dependent Emission29An unprecedented molybdenum oxide based helical MOF with peroxidase-like activity synthesized by surfactant-thermal method8Growing crystalline selenidostannates in deep eutectic solvent7Complexations of Mn(II) with SbS4 and SbS3 ligands: Hydrazine-solvothermal syntheses, crystal structures and photocatalytic properties of manganese thioantimonates8Anti-Site Defects-Assisted Enhancement of Electrogenerated Chemiluminescence from in Situ Mn2+-Doped Supertetrahedral Chalcogenide Nanoclusters20Solar-charged pseudocapacitors: Simultaneous conversion and storage of solar energy in ZnO@NiO nanorod arrays28Surfactants as promising media in the field of metal-organic frameworks386New 2D Assemblage of Supertetrahedral Chalcogenide Clusters with Tetravalent-Metal-Induced Interrupted Sites17In situ fabrication of self-assembled BiOBr x I 1−x coated on carbon nanofibers for efficient solar light-driven photocatalytic nitrogen fixation15Surface defect engineering of mesoporous Cu/ZnS nanocrystal-linked networks for improved visible-light photocatalytic hydrogen production41Two new layered metal chalcogenide frameworks as photocatalysts for highly efficient and selective dye degradation6New quaternary selenogermanates of Rb2Ag2GeSe4 and Cs2Cu2GeSe48A Coordination Polymer based on Interconnection of Thioantimonate(III) and [Mn(terpy)]2+ Complexes: Synthesis, Crystal Structure, and Properties of {[(Mn(terpy))2Sb4S8]·0.5H2O}n4[Mn(terpy)Sb2S4]n, a 1D Network of MnSb4S5 Rings Exhibiting a Pronounced Magnetocaloric Effect and Luminescence9Using thiol-amine solvent mixture to prepare main group heterometallic chalcogenides8Recent Progress in Metal‐Free Covalent Organic Frameworks as Heterogeneous Catalysts372Two Copper-Rich Open-Framework Chalcogenides Built from Unusual [Cu5(SnxM1–x)Se10] Clusters and [(SnxM1–x)2Se6] Dimeric Linkers (M = In and Ga)4Effect of CeO2-ZnO Nanocomposite for Photocatalytic and Antibacterial Activities60A 3 Mn 2 Sb 3 S 8 (A = K and Rb): a new type of multifunctional infrared nonlinear optical material based on unique three-dimensional open frameworks53A pillar-layered chalcogenide framework assembled by [Mn 5 S 12 N 12 ] n layers and [Sb 2 S 5 ] inorganic pillars6Basic principles, fundamentals, and mechanisms of chalcogenide-based nanomaterials in photocatalytic reactions8Chalcogenides as well as chalcogenides-based nanomaterials and its importance in photocatalysis19Recent advances in the “on–off” approaches for on-demand liquid-phase hydrogen evolution78Three-dimensional ordered macroporous materials for photocatalysis: design and applications67Unveiling the impurity-modulated photoluminescence from Mn 2+ -containing metal chalcogenide semiconductors via Fe 2+ doping10Hierarchical fibrous bimetallic electrocatalyst based on ZnO-MoS2 composite nanostructures as high performance for hydrogen evolution reaction44Advances in metal–organic frameworks and their derivatives for diverse electrocatalytic applications179Pristine and Janus monolayers of vanadium dichalcogenides: potential materials for overall water splitting and solar energy conversion13Ionothermal Synthesis of Two New Thioantimonates with Transition Metal Regulation4Fabrication of Highly Textured 2D SnSe Layers with Tunable Electronic Properties for Hydrogen Evolution13Cube Cu 2 O modified CoAL‐LDH p‐n heterojunction for photocatalytic hydrogen evolution19An overview of photocatalytic water splitting on semiconductor oxides for hydrogen production4State‐of‐the‐Art Advancements in Photocatalytic Hydrogenation: Reaction Mechanism and Recent Progress in Metal‐Organic Framework (MOF)‐Based Catalysts94Highly Active Electrochemiluminescence of Ruthenium Complex Co-assembled Chalcogenide Nanoclusters and the Application for Label-Free Detection of Alkaline Phosphatase33State of the art developments and prospects of metal–organic frameworks for energy applications40Interface engineering: Synergism between S-scheme heterojunctions and Mo-O bonds for promote photocatalytic hydrogen evolution42Enhancing interfacial charge transfer in mesoporous MoS 2 /CdS nanojunction architectures for highly efficient visible-light photocatalytic water splitting17Mild solvothermal syntheses and characterizations of five Nb-containing quaternary sulfides6Ba 3 Zr 2 Cu 4 S 9 : the first quaternary phase of the Ba–Zr–Cu–S system5Crystalline chalcogenidometalate-based compounds from uncommon reaction media12Cu/Cu x O@C nanocomposites as efficient electrodes for high-performance supercapacitor devices18Molecular surface modification of silver chalcogenolate clusters1Role of processing parameters in solution routes for controlling size, shape, and morphology of chalcogenide nanoparticles1Structural regulation of Co-based coordination polymers by adjusting solvent polarity toward electrocatalytic hydrogen evolution performance4Integration of CdS with a Fiber-Based Cadmium Coordination Polymer for Turning On Photocatalytic Oxidative Coupling Reactions15Photothermal-chemical synthesis of P–S–H ternary hydride at high pressures1Polymer/non-fullerene acceptor bulk heterojunction nanoparticles for efficient photocatalytic hydrogen production from water33Electrocatalysts for Oxygen/Hydrogen-Involved Reactions0Temperature-Induced Structure Transformation from Co0.85Se to Orthorhombic Phase CoSe2 Realizing Enhanced Hydrogen Evolution Catalysis13Optimized Metal Deficiency-Induced Operando Phase Transformation Enhances Charge Polarization Promoting Hydrogen Evolution Reaction12Structural, surface, optical, and antimicrobial characterization of I2/Polymethyl methacrylate and CuS/I2/polymethyl methacrylate thin films1Fabrication of a Sm 2 O 3 /In 2 S 3 photocatalyst for boosting ciprofloxacin oxidation and the Cr( vi ) reduction: process parameters and degradation mechanism11Ni3S2/Co9S8 embedded poor crystallinity NiCo layered double hydroxides hierarchical nanostructures for efficient overall water splitting50Hydrogen evolution properties: Cr doping and V co-doping effect of ZnS nanoparticles12Two-dimensional layered organic hybrid selenidostannate coupled with polyaniline for high efficient photocatalytic Cr(VI) reduction72Advances in Chalcogenide Crystal Growth: Flux and Solution Syntheses, and Approaches for Postsynthetic Modifications13Ligand-functionalized and ligand-bridged or organyl-separated chalcogenido metalate-based clusters15CeO2-ZnO nano composites: Dual-functionality for enhanced photocatalysis and biomedical applications57Fabrication of high-surface-area mesoporous frameworks of β-Ni(OH) 2 –CdIn 2 S 4 p–n nano-heterojunctions for improved visible light photocatalytic hydrogen production7Hydrazine-Assisted Synthesis, Structures, Photoelectricity, and Photocatalysis of Ternary Mercury–Tellurostannate Hybrids with Transition-Metal Complexes4Efficient Visible Light Photocatalytic Hydrogen Evolution by Boosting the Interfacial Electron Transfer in Mesoporous Mott–Schottky Heterojunctions of Co 2 P-Modified CdIn 2 S 4 Nanocrystals25Preparation of aqueous zinc ion rGH/BiVO4 photorechargeable integrated supercapacitor12Green Hydrogen from Wastewater─A Dual Crisis Resolution26Development of an aqueous zinc ion rGH//Bi 2 MoO 6 photo-assisted charging supercapacitor1Ionothermal Synthesis of Selenido Metalates in Tunable Aryl Alkyl Ionic Liquids (TAAILs)0Magnetic‐Field Modulation of Charge Transport in Non‐Fullerene Semiconductors for Enhanced Hydrogen Evolution0

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  11. [AEPH2][GeSb2S6]·CH3OH: a thiogermanate–thioantimonate featuring an infinite ribbon-like structure with an unusual {GeSb3S11} unit and exhibiting the ability of photocatalytic degradation of organic dye

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  33. {[M(NH3)6][Ag4M4Sn3Se13]}∞ (M=Zn, Mn): Three-dimensional chalcogenide frameworks constructed from quaternary metal selenide clusters with two different transition metals

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  34. Surfactant-thermal method to prepare two novel two-dimensional Mn–Sb–S compounds for photocatalytic applications

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  36. New Members of the Family of In–Sb–S Compounds: Different Roles of Organic Amines

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  37. Ubiquitous quantum dot-sensitized nanoporous film for hydrogen production under visible-light irradiation

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  38. Synthesis, crystal structure and optical property of a novel metal chalcohalide: ZnHg3Se2Cl4

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  39. Hydrazine-Hydrothermal Synthesis and Characterization of the Two New Quaternary Thioantimonates(III) BaAgSbS3 and BaAgSbS3·H2O

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  40. Preparation of Porous Three‐Dimensional Quaternary Thioantimonates(III) ACuSb2S4 (A=Rb, Cs) through a Surfactant‐Thermal Method

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  41. Facile surfactant-thermal syntheses and characterization of quaternary copper thioantimonates(III) ACu 2 SbS 3 (A = K, Rb, Cs)

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