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RESEARCH PAPER · Review of Scientific Instruments · 2017

A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions

Niclas Heidenreich, U. Rütt, Milan Köppen, A. Ken Inge, S. Beier, Ann‐Christin Dippel, Ralf Suren, Norbert Stock

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42 direct citing works

A multi-purpose reaction cell for the investigation of reactions under solvothermal conditionsOriginalMonitoring the mechanism of formation of [Ce(1,10-phenanthroline) 2 (NO 3 ) 3 ] by in situ luminescence analysis of 5d–4f electronic transitions15Co-Ligand Dependent Formation and Phase Transformation of Four Porphyrin-Based Cerium Metal–Organic Frameworks38In situ monitoring metal-ligand exchange processes by optical spectroscopy and X-ray diffraction analysis: a review22Green synthesis of a new layered aluminium citraconate: crystal structures, intercalation behaviour towards H 2 O and in situ PXRD studies of its crystallisation12From ligand exchange to reaction intermediates: what does really happen during the synthesis of emissive complexes?20Probing the Evolution of Palladium Species in Pd@MOF Catalysts during the Heck Coupling Reaction: An Operando X-ray Absorption Spectroscopy Study97Synthesis, Transformation, Catalysis, and Gas Sorption Investigations on the Bismuth Metal–Organic Framework CAU‐17106Multiparameter High-Throughput and in Situ X-ray Diffraction Study of Six New Bismuth Sulfonatocarboxylates: Discovery, Phase Transformation, and Reaction Trends25Nuclear Magnetic Resonance Spectroscopy for In Situ Monitoring of Porous Materials Formation under Hydrothermal Conditions32Investigation of the Kinetic Stabilization of a Ce4+‐based MOF by in‐situ Powder X‐ray Diffraction26Metal–organic frameworks in Germany: From synthesis to function125In situ XAS study of the local structure and oxidation state evolution of palladium in a reduced graphene oxide supported Pd( ii ) carbene complex during an undirected C–H acetoxylation reaction23New insights into the crystallization of polymorphic materials: from real-time serial crystallography to luminescence analysis11Real‐time Probing the Formation of [M(2,2‐bipyridine)2(NO3)3] (M = Ce, La, Tb) Complexes and Influence of Synthesis Parameters7New Directions in Metal Phosphonate and Phosphinate Chemistry131Mapping the redox chemistry of common solvents in solvothermal synthesis through in situ X-ray diffraction22Metal Phosphonates and Phosphinates2In Situ Structural Determination of a Homogeneous Ruthenium Racemization Catalyst and Its Activated Intermediates Using X‐Ray Absorption Spectroscopy13A Scandium MOF with an Unprecedented Inorganic Building Unit, Delimiting the Micropore Windows12In situ X-ray Diffraction Investigation of the Crystallisation of Perfluorinated Ce(IV)-based Metal-Organic Frameworks with UiO-66 and MIL-140 architectures2Exploiting in situ NMR to monitor the formation of a metal–organic framework43In Situ X‐ray Diffraction Investigation of the Crystallisation of Perfluorinated Ce IV ‐Based Metal–Organic Frameworks with UiO‐66 and MIL‐140 Architectures**23Synthesis and characterisation of novel phosphonate-based linkers and metal-organic frameworks based on tetravalent metals0Crystallisation of phosphates revisited: a multi-step formation process for SrHPO44Detailed insights into the formation pathway of CdS and ZnS in solution: a multi-modal in situ characterisation approach9LiquidReactionCell – a versatile setup for in situ synchrotron studies of compounds in liquid suspension and solution2Discovery and In Situ Crystallization Studies of Cerium-Based Metal–Organic Frameworks with V-Shaped Linker Molecules11Exploring cluster formation in Zr-MOF synthesis in situ using X-ray absorption spectroscopy4Synthesis, Structure and (Photo)Catalytic Behavior of Ce‐MOFs Containing Perfluoroalkylcarboxylate Linkers: Experimental and Theoretical Insights9Probing Ce- and Zr-Fumarate Metal–Organic Framework Formation in Aqueous Solutions with In Situ Raman Spectroscopy and Synchrotron X-ray Diffraction8Synthesis and Characterization of a Cerium(IV) Coordination Polymer Containing Isonicotinic Acid Zwitterions0Cerium-Based Coordination Network Formation: An In Situ X-ray Absorption Spectroscopy and Powder X-ray Diffraction Study1Interface engineering of COF/Semiconductor S-scheme heterojunctions photocatalyst for coupled energy conversion and environmental detoxification5

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33 direct citing papers saved.

  1. Monitoring the mechanism of formation of [Ce(1,10-phenanthroline) 2 (NO 3 ) 3 ] by in situ luminescence analysis of 5d–4f electronic transitions

    RSC Advances · 2017-01-01

    Laura Ruiz Arana, Patric Lindenberg, H. Said, Marvin Radke, Niclas Heidenreich, C. S. Cunha, Sebastian Leubner, Huayna Terraschke

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  2. Co-Ligand Dependent Formation and Phase Transformation of Four Porphyrin-Based Cerium Metal–Organic Frameworks

    Crystal Growth & Design · 2017-05-08

    Timo Rhauderwiek, Niclas Heidenreich, Helge Reinsch, Sigurd Øien‐Ødegaard, Kirill A. Lomachenko, Uta Ruett, Alexander V. Soldatov, Karl Petter Lillerud, Norbert Stock

    Read original paper ↗ ·

  3. In situ monitoring metal-ligand exchange processes by optical spectroscopy and X-ray diffraction analysis: a review

    Reviews in Analytical Chemistry · 2017-08-19

    Huayna Terraschke, Merrit Rothe, Patric Lindenberg

    Read original paper ↗ ·

  4. Green synthesis of a new layered aluminium citraconate: crystal structures, intercalation behaviour towards H 2 O and in situ PXRD studies of its crystallisation

    Dalton Transactions · 2017-11-23

    Niclas Heidenreich, Alexandra Lieb, Norbert Stock, Helge Reinsch

    Read original paper ↗ ·

  5. From ligand exchange to reaction intermediates: what does really happen during the synthesis of emissive complexes?

    Physical Chemistry Chemical Physics · 2017-12-20

    Philipp Müscher‐Polzin, Irma Vania Eliani, Jonas Ströh, M. Braun, Niklas Ruser, Niclas Heidenreich, Pia Rönfeldt, Florian Bertram, Christian Näther, Stephan Wöhlbrandt, Markus Suta, Huayna Terraschke

    Read original paper ↗ ·

  6. Probing the Evolution of Palladium Species in Pd@MOF Catalysts during the Heck Coupling Reaction: An Operando X-ray Absorption Spectroscopy Study

    Journal of the American Chemical Society · 2018-06-11

    Ning Yuan, Vlad Paşcanu, Zhehao Huang, Alejandro Valiente, Niclas Heidenreich, Sebastian Leubner, A. Ken Inge, Jakob Gaar, Norbert Stock, Ingmar Persson, Belén Martín‐Matute, Xiaodong Zou

    Read original paper ↗ ·

  7. Synthesis, Transformation, Catalysis, and Gas Sorption Investigations on the Bismuth Metal–Organic Framework CAU‐17

    European Journal of Inorganic Chemistry · 2018-06-19

    Milan Köppen, Amarajothi Dhakshinamoorthy, A. Ken Inge, Ocean Y. H. Cheung, Jonas Ångström, Péter Mayer, Norbert Stock

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  8. Multiparameter High-Throughput and in Situ X-ray Diffraction Study of Six New Bismuth Sulfonatocarboxylates: Discovery, Phase Transformation, and Reaction Trends

    Inorganic Chemistry · 2018-08-02

    Martin Albat, Norbert Stock

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  9. Nuclear Magnetic Resonance Spectroscopy for In Situ Monitoring of Porous Materials Formation under Hydrothermal Conditions

    Materials · 2018-08-12

    Mohamed Haouas

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  10. Investigation of the Kinetic Stabilization of a Ce4+‐based MOF by in‐situ Powder X‐ray Diffraction

    Zeitschrift für anorganische und allgemeine Chemie · 2018-10-31

    Niclas Heidenreich, Steve Waitschat, Helge Reinsch

    Read original paper ↗ ·

  11. Metal–organic frameworks in Germany: From synthesis to function

    Coordination Chemistry Reviews · 2018-11-15

    Jack D. Evans, Bikash Garai, Helge Reinsch, Weijin Li, Stefano Dissegna, Volodymyr Bon, Irena Senkovska, Roland A. Fischer, Stefan Kaskel, Christoph Janiak, Norbert Stock, Dirk Volkmer

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  12. In situ XAS study of the local structure and oxidation state evolution of palladium in a reduced graphene oxide supported Pd( ii ) carbene complex during an undirected C–H acetoxylation reaction

    Catalysis Science & Technology · 2019-01-01

    Ning Yuan, Maitham H. Majeed, Éva G. Bajnóczi, Axel R. Persson, Reine Wallenberg, A. Ken Inge, Niclas Heidenreich, Norbert Stock, Xiaodong Zou, Ola F. Wendt, Ingmar Persson

    Read original paper ↗ ·

  13. New insights into the crystallization of polymorphic materials: from real-time serial crystallography to luminescence analysis

    Reaction Chemistry & Engineering · 2019-01-01

    Patric Lindenberg, Laura Ruiz Arana, Lisa K. Mahnke, Pia Rönfeldt, Niclas Heidenreich, Giscard Doungmo, Nicolas Guignot, Richard Bean, Henry N. Chapman, D. Dierksmeyer, J. Knoška, Manuela Kuhn, Jan Garrevoet, Valerio Mariani, D. Oberthüer, Kanupriya Pande, Stephan Stern, Aleksandra Tolstikova, Thomas A. White, Kenneth R. Beyerlein, Huayna Terraschke

    Read original paper ↗ ·

  14. Real‐time Probing the Formation of [M(2,2‐bipyridine)2(NO3)3] (M = Ce, La, Tb) Complexes and Influence of Synthesis Parameters

    Zeitschrift für anorganische und allgemeine Chemie · 2019-02-15

    Jonas Ströh, Laura Ruiz Arana, Philipp Müscher‐Polzin, Irma Vania Eliani, Patric Lindenberg, Niclas Heidenreich, Cesar Dos Santos Cunha, Sebastian Leubner, Huayna Terraschke

    Read original paper ↗ ·

  15. New Directions in Metal Phosphonate and Phosphinate Chemistry

    Crystals · 2019-05-24

    Stephen J. I. Shearan, Norbert Stock, Franziska Emmerling, Jan Demel, Paul A. Wright, Konstantinos D. Demadis, Maria Vassaki, Ferdinando Costantino, Riccardo Vivani, Sébastien Sallard, Inés R. Salcedo, Aurelio Cabeza, Marco Taddei

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  16. Mapping the redox chemistry of common solvents in solvothermal synthesis through in situ X-ray diffraction

    Nanoscale · 2020-01-01

    Nils Lau Nyborg Broge, Frederik Søndergaard‐Pedersen, Martin Roelsgaard, Xenia Hassing-Hansen, Bo B. Iversen

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  17. Metal Phosphonates and Phosphinates

    MDPI eBooks · 2020-01-15

    Taddei, Marco, Costantino, Ferdinando

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  18. In Situ Structural Determination of a Homogeneous Ruthenium Racemization Catalyst and Its Activated Intermediates Using X‐Ray Absorption Spectroscopy

    Chemistry - A European Journal · 2020-01-24

    Karl P. J. Gustafson, Arnar Guðmundsson, Éva G. Bajnóczi, Ning Yuan, Xiaodong Zou, Ingmar Persson, Jan‐E. Bäckvall

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  19. A Scandium MOF with an Unprecedented Inorganic Building Unit, Delimiting the Micropore Windows

    Inorganic Chemistry · 2020-06-17

    Pia Rönfeldt, Erik Svensson Grape, A. Ken Inge, Dmitri Novikov, Azat Khadiev, Martin Etter, Timo Rabe, Jannik Benecke, Huayna Terraschke, Norbert Stock

    Read original paper ↗ ·

  20. In situ X-ray Diffraction Investigation of the Crystallisation of Perfluorinated Ce(IV)-based Metal-Organic Frameworks with UiO-66 and MIL-140 architectures

    ChemRxiv · 2020-11-19

    Stephen J. I. Shearan, Jannick Jacobsen, Ferdinando Costantino, Roberto D’Amato, Dmitri Novikov, Norbert Stock, Enrico Andreoli, Marco Taddei

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  21. Exploiting in situ NMR to monitor the formation of a metal–organic framework

    Chemical Science · 2020-11-20

    Corey L. Jones, Colan E. Hughes, Hamish H.‐M. Yeung, Alison Paul, Kenneth D M Harris, Timothy L. Easun

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  22. In Situ X‐ray Diffraction Investigation of the Crystallisation of Perfluorinated Ce IV ‐Based Metal–Organic Frameworks with UiO‐66 and MIL‐140 Architectures**

    Chemistry - A European Journal · 2021-01-22

    Stephen J. I. Shearan, Jannick Jacobsen, Ferdinando Costantino, Roberto D’Amato, Dmitri Novikov, Norbert Stock, Enrico Andreoli, Marco Taddei

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  23. Synthesis and characterisation of novel phosphonate-based linkers and metal-organic frameworks based on tetravalent metals

    Unknown journal · 2022-01-01

    Shearan, Steve

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  24. Crystallisation of phosphates revisited: a multi-step formation process for SrHPO4

    Zeitschrift für Naturforschung B · 2022-03-03

    Laura Ruiz Arana, Jonas Ströh, Jasper Amtsfeld, Giscard Doungmo, Dmitri Novikov, Azat Khadiev, Martin Etter, Michael T. Wharmby, Markus Suta, Huayna Terraschke

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  25. Detailed insights into the formation pathway of CdS and ZnS in solution: a multi-modal in situ characterisation approach

    Physical Chemistry Chemical Physics · 2022-12-19

    Jonas Ströh, Thomas C. Hess, L. Ohrt, Harald Fritzsch A, Martin Etter, Ann‐Christin Dippel, Linda Dyorisse Nyamen, Huayna Terraschke

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  26. LiquidReactionCell – a versatile setup for in situ synchrotron studies of compounds in liquid suspension and solution

    CrystEngComm · 2022-12-20

    Henrik Særkjær Jeppesen, Ida Gjerlevsen Nielsen, Jens Christian Kondrup, Justus Just, Nina Lock

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  27. Discovery and In Situ Crystallization Studies of Cerium-Based Metal–Organic Frameworks with V-Shaped Linker Molecules

    Inorganic Chemistry · 2023-12-04

    Jonas Gosch, Virginia Guiotto, Felix Steinke, Erik Svensson Grape, Cesare Atzori, Kalle S. Mertin, Tobias Otto, Niklas Ruser, Christoph Meier, Diletta Morelli Venturi, A. Ken Inge, Kirill A. Lomachenko, Valentina Crocellà, Norbert Stock

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  28. Exploring cluster formation in Zr-MOF synthesis in situ using X-ray absorption spectroscopy

    Physical Chemistry Chemical Physics · 2024-01-01

    Olena Zavorotynska, Anna Cecilie Åsland, Pascal D. C. Dıetzel, Sachin Chavan

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  29. Synthesis, Structure and (Photo)Catalytic Behavior of Ce‐MOFs Containing Perfluoroalkylcarboxylate Linkers: Experimental and Theoretical Insights

    Chemistry - A European Journal · 2024-04-03

    Diletta Morelli Venturi, Maria Sole Notari, Letizia Trovarelli, Edoardo Mosconi, Asma A. Alothman, Anastasia Yu. Molokova, Niklas Ruser, Christoph Meier, Bastian Achenbach, Kirill A. Lomachenko, Tiziana Del Giacco, Ferdinando Costantino, Norbert Stock

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  30. Probing Ce- and Zr-Fumarate Metal–Organic Framework Formation in Aqueous Solutions with In Situ Raman Spectroscopy and Synchrotron X-ray Diffraction

    ACS Omega · 2024-10-21

    Sofiia Bercha, Simmy Rathod, Olena Zavorotynska, Sachin Chavan

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  31. Synthesis and Characterization of a Cerium(IV) Coordination Polymer Containing Isonicotinic Acid Zwitterions

    Zeitschrift für anorganische und allgemeine Chemie · 2025-12-26

    Niklas Ruser, Folke Weidemann, Jonas Gosch, Felix Steinke, Anastasia Yu. Molokova, Kirill A. Lomachenko, Diletta Morelli Venturi, Christoph Meier, Bastian Achenbach, Norbert Stock

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  32. Cerium-Based Coordination Network Formation: An In Situ X-ray Absorption Spectroscopy and Powder X-ray Diffraction Study

    Chemistry of Materials · 2026-02-02

    Niklas Ruser, Anastasia Yu. Molokova, Kirill A. Lomachenko, Zheting Chu, Xiaodong Zou, Felix Steinke, Diletta Morelli Venturi, Christoph Meier, Bastian Achenbach, Azat Khadiev, Jonas Gosch, Norbert Stock

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  33. Interface engineering of COF/Semiconductor S-scheme heterojunctions photocatalyst for coupled energy conversion and environmental detoxification

    International Journal of Hydrogen Energy · 2026-03-24

    Mahatab Ali, Afreen Inam, Saad M. Alshehri, Yoshio Bando, Tansir Ahamad

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