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RESEARCH PAPER · Dalton Transactions · 2007

Hydrothermal chemistry of oligomeric vanadium oxyfluorides

David W. Aldous, Nicholas F. Stephens, Philip Lightfoot

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Hydrothermal chemistry of oligomeric vanadium oxyfluoridesOriginalThe role of temperature in the solvothermal synthesis of hybrid vanadium oxyfluorides41Vanadium through Dubnium2A new hybrid framework based on a ‘superoctahedral’ [V7O6F30]14− polyanion14Complexes of Vanadium(V) Oxide Trifluoride with Nitrogen and Oxygen Donor Ligands: Coordination Chemistry and Some Fluorination Reactions26An unusual hybrid fluoride featuring a [V7F27]6− chain motif based on a pyrochlore-like building unit14Hydrothermal Synthesis of Vanadium Oxyfluoride Chains Incorporating Covalently Bound Copper Coordination Complexes35Crystallisation of some mixed Na/V and K/V fluorides by solvothermal methods36A F-bridged Mn(ii) molecular square18Organic–inorganic hybrid chains and layers constructed from copper-amine cations and early transition metal (Nb, Mo) oxyfluoride anions21Novel building units with bimetallic rings in inorganic/organic hybrid chains and layers2Solvatothermal chemistry of organically-templated vanadium fluorides and oxyfluorides21Hydrothermal synthesis and structural characterization of bimetallic organic–inorganic hybrid materials: Copper vanadate–1,4-Carboxy-phenylphosphonate phases15Building Fe(iii) clusters with derivatised salicylaldoximes27Increasing the dimensionality of hybrid vanadium oxyfluorides using ionothermal synthesis31Structural chemistry of organically-templated metal fluorides61Syntheses and Physicochemical Properties of Low‐Melting Salts Based on VOF4– and MoOF5–, and the Molecular Geometries of the Dimeric (VOF4–)2 and Mo2O4F62– Anions24Hydrothermal synthesis and structure of a two-dimensional bimetallic copper–molybdophosphonate, [{Cu4(H2O)2(phenbisterpy)2(HO3P(CH2)4PO3H)}(Mo4FO12)2{O3P(CH2)4PO3}]·4H2O, constructed from {Mo4FO12}1− clusters and copper-ligand chains (phenbisterpy = 1,4-bis(2,2′:6′,2′′-terpyridin-4′-yl)benzene)15A new chain structure:catena-poly[4,4′-(ethane-1,2-diyl)dipyridinium bis[[aquadifluoridooxidovanadate]-μ-fluorido]]0A three-dimensional heterometallic CuI/VIV1,2-bis(1,2,4-triazol-4-yl)ethane framework: a new insight into the structure of vanadium oxyfluoride coordination hybrids2Ionic liquids and deep eutectic mixtures as new solvents for the synthesis of vanadium fluorides and oxyfluorides31Vanadium fluoroarsenates—folding sheets into highly corrugated layers and crystalline arrays of large inorganic tubes5Hydrothermal syntheses and structures of vanadium oxyfluorides templated by organic and metal organic cations9Synthesis, crystal and electronic structure, and theoretical investigations of charge-transfer, optical, and bonding properties of a [VF6]3− anion compound2The Role of Polar, Lamdba (Λ)-Shaped Building Units in Noncentrosymmetric Inorganic Structures139Lead Fluoridooxidovanadates(V), Pb(V 2 O 2 F 8 ), Pb(VOF 5 ), and Mixed Valent Fluoridooxidovanadate(IV, V), Pb 3 F(V 4 O 3 F 18 )4The Dimeric [V2O4F6]4– Vanadium Oxide‐Fluoride Anion in Na2(M(H2O)2)(V2O4F6) (M = Co2+, Ni2+, and Cu2+)8AgI/VV Heterobimetallic Frameworks Generated from Novel-Type {Ag2(VO2F2)2(triazole)4} Secondary Building Blocks: A New Aspect in the Design of SVOF Hybrids59New structural units in molybdenum oxyfluoride chemistry14Influence of Hydrofluoric Acid Formation on Lithium Ion Insertion in Nanostructured V2O516Solid state coordination chemistry: Structural consequences of varying diphosphonate tether length and fluoride incorporation in the copper–bisterpy/oxomolybdenum/organodiphosphonate system (bisterpy = 2,2′:4′,4″:2″,2″′-quarterpyridyl-6′,6″-di-2-pyridine)16The dimeric [V2O2F8]4− anion: Structural characterization of a magnetic basic-building-unit18Structure-Directing Self-Assembly, Structures and Characterization of Four d0-Transition Metal Oxide/Fluoride Compounds Constructed with Imidazole/1-Methylimidazole/1-Vinylimidazole and Copper(II)/Zinc(II)16Crystal Structures and Raman Spectra of Imidazolium Poly[perfluorotitanate(IV)] Salts Containing the [TiF6]2–, ([Ti2F9]−)∞, and [Ti2F11]3– and the New [Ti4F20]4– and [Ti5F23]3– Anions28Structural diversity in hybrid vanadium( iv ) oxyfluorides based on a common building block27Structural consequences of fluoride incorporation into oxovanadium-xylyldiphosphonates with charge compensating copper(II)-imine components13Spin Frustration from cis-Edge or -Corner Sharing Metal-Centered Octahedra29A hybrid vanadium fluoride with structurally isolated S = 1 kagome layers11Fluoroferrates with (dabcoH2)2+ or (dabcoH)+ Cations7F−/OH− substitution in [H4tren]4+ and [H3tren]3+ hydroxyfluorotitanates(IV) and classification of tren cation configurations11Synthesis, Crystal Structure, Vibrational and Optical Properties of (Hdea)4(V7O19F)∙0.42H2O, an Original (V7O19F)4− Cluster Oxyfluoride9Crystal Chemistry and Selected Physical Properties of Inorganic Fluorides and Oxide-Fluorides173Syntheses of Two Vanadium Oxide–Fluoride Materials That Differ in Phase Matchability46A New Vanadium (V) Coordination Based on [(H2C4O4)VO2F] n 2n− Polymeric Chains and Diethylammonium Cations, Synthesis, Crystal Structure, Vibrational and Optical Properties2Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 617Fluoride-coordination chemistry in molecular and low-dimensional magnetism67V2O2F4(H2O)2·H2O: a new V4+layer structure related to VOF33Bimetallic MOFs (H 3 O) x [Cu(MF 6 )(pyrazine) 2 ]·(4 − x)H 2 O (M = V 4+ , x = 0; M = Ga 3+ , x = 1): co-existence of ordered and disordered quantum spins in the V 4+ system6Revealing the electronic structure and optical properties of K6[Mo4O8F10] novel molybdenum oxyfluoride materials2Complexes of vanadium(IV) oxide difluoride with neutral N- and O-donor ligands11Design and Assembly of Covalently Functionalised Polyoxofluorovanadate Molecular Hybrids10Reactivity of VOF3 with N-Heterocyclic Carbene and Imidazolium Fluoride: Analysis of Ligand–VOF3 Bonding with Evidence of a Minute π Back-Donation of Fluoride16Controlled one pot synthesis of polyoxofluorovanadate molecular hybrids exhibiting peroxidase like activity4Theoretical studies of structural, electronic, and magnetic properties for small V2Fn0,− (2 ≤ n ≤ 7) clusters using first-principles calculations2Crystal structure of tetrakis[μ-3-carboxy-1-(1,2,4-triazol-4-yl)adamantane-κ2 N 1:N 2]tetrafluoridodi-μ2-oxido-dioxidodisilver(I)divanadium(V) tetrahydrate3Uncovering Multiple Metal–Metal Bonding in a Tetranuclear Fluoride Rhenium Cluster or the Curious Case of {[Ni(H2O)6](NH4)4}[Re4F18]·4H2O3Influence of structure-directing polyhedra and heterocyclic ligands on the chain structures and O/F ordering in a series of zinc vanadium oxyfluorides1Synthesis and characterisation of Vanadium(III) fluorides α-BaVF5 and BaV(F,OH)5 with an S = 1 spin chain structure1

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  1. The role of temperature in the solvothermal synthesis of hybrid vanadium oxyfluorides

    Dalton Transactions · 2007-01-01

    David W. Aldous, Nicholas F. Stephens, Philip Lightfoot

    Read original paper ↗ ·

  2. Vanadium through Dubnium

    Springer eBooks · 2007-01-01

    Read original paper ↗ ·

  3. A new hybrid framework based on a ‘superoctahedral’ [V7O6F30]14− polyanion

    Chemical Communications · 2008-01-01

    Thushitha Mahenthirarajah, Philip Lightfoot

    Read original paper ↗ ·

  4. Complexes of Vanadium(V) Oxide Trifluoride with Nitrogen and Oxygen Donor Ligands: Coordination Chemistry and Some Fluorination Reactions

    European Journal of Inorganic Chemistry · 2008-01-02

    Martin F. Davis, William Levason, James Paterson, Gillian Reid, Michael Webster

    Read original paper ↗ ·

  5. An unusual hybrid fluoride featuring a [V7F27]6− chain motif based on a pyrochlore-like building unit

    Journal of Solid State Chemistry · 2008-08-15

    David W. Aldous, Alexandra M. Z. Slawin, Philip Lightfoot

    Read original paper ↗ ·

  6. Hydrothermal Synthesis of Vanadium Oxyfluoride Chains Incorporating Covalently Bound Copper Coordination Complexes

    Inorganic Chemistry · 2008-08-19

    Thushitha Mahenthirarajah, Yang Li, Philip Lightfoot

    Read original paper ↗ ·

  7. Crystallisation of some mixed Na/V and K/V fluorides by solvothermal methods

    Solid State Sciences · 2008-10-01

    David W. Aldous, Philip Lightfoot

    Read original paper ↗ ·

  8. A F-bridged Mn(ii) molecular square

    Chemical Communications · 2009-01-01

    S.T. Meally, Kevin Mason, Patrick McArdle, Euan K. Brechin, Alan George Ryder, Leigh F. Jones

    Read original paper ↗ ·

  9. Organic–inorganic hybrid chains and layers constructed from copper-amine cations and early transition metal (Nb, Mo) oxyfluoride anions

    Dalton Transactions · 2009-01-01

    Thushitha Mahenthirarajah, Yang Li, Philip Lightfoot

    Read original paper ↗ ·

  10. Novel building units with bimetallic rings in inorganic/organic hybrid chains and layers

    Journal of Solid State Chemistry · 2009-09-10

    Thushitha Mahenthirarajah, Yang Li, Philip Lightfoot

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  11. Solvatothermal chemistry of organically-templated vanadium fluorides and oxyfluorides

    Inorganica Chimica Acta · 2009-10-15

    P. DeBurgomaster, W. Ouellette, Hongxue Liu, Charles J. O’Connor, G.T. Yee, Jon A. Zubieta

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  12. Hydrothermal synthesis and structural characterization of bimetallic organic–inorganic hybrid materials: Copper vanadate–1,4-Carboxy-phenylphosphonate phases

    Inorganica Chimica Acta · 2009-10-30

    P. DeBurgomaster, Hongxue Liu, Charles J. O’Connor, Jon A. Zubieta

    Read original paper ↗ ·

  13. Building Fe(iii) clusters with derivatised salicylaldoximes

    Dalton Transactions · 2010-01-01

    Kevin Mason, Ian A. Gass, Simon Parsons, Anna Collins, Fraser White, Alexandra M. Z. Slawin, Euan K. Brechin, Peter A. Tasker

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  14. Increasing the dimensionality of hybrid vanadium oxyfluorides using ionothermal synthesis

    Dalton Transactions · 2010-01-01

    Farida Himeur, Phoebe K. Allan, Simon J. Teat, Richard J. Goff, Russell E. Morris, Philip Lightfoot

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  15. Structural chemistry of organically-templated metal fluorides

    Dalton Transactions · 2010-01-01

    Karim Adil, M. Leblanc, V. Maisonneuve, Philip Lightfoot

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  16. Syntheses and Physicochemical Properties of Low‐Melting Salts Based on VOF4– and MoOF5–, and the Molecular Geometries of the Dimeric (VOF4–)2 and Mo2O4F62– Anions

    European Journal of Inorganic Chemistry · 2010-01-19

    Takatsugu Kanatani, Kazuhiko Matsumoto, Rika Hagiwara

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  17. Hydrothermal synthesis and structure of a two-dimensional bimetallic copper–molybdophosphonate, [{Cu4(H2O)2(phenbisterpy)2(HO3P(CH2)4PO3H)}(Mo4FO12)2{O3P(CH2)4PO3}]·4H2O, constructed from {Mo4FO12}1− clusters and copper-ligand chains (phenbisterpy = 1,4-bis(2,2′:6′,2′′-terpyridin-4′-yl)benzene)

    Inorganic Chemistry Communications · 2010-02-05

    Stephanie Jones, Hongxue Liu, W. Ouellette, Katherine Schmidtke, Charles J. O’Connor, Jon A. Zubieta

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  18. A new chain structure:catena-poly[4,4′-(ethane-1,2-diyl)dipyridinium bis[[aquadifluoridooxidovanadate]-μ-fluorido]]

    Acta Crystallographica Section C Crystal Structure Communications · 2010-04-13

    David W. Aldous, Alexandra M. Z. Slawin, Philip Lightfoot

    Read original paper ↗ ·

  19. A three-dimensional heterometallic CuI/VIV1,2-bis(1,2,4-triazol-4-yl)ethane framework: a new insight into the structure of vanadium oxyfluoride coordination hybrids

    Acta Crystallographica Section C Crystal Structure Communications · 2010-08-27

    Olena V. Sharga, A.B. Lysenko, Harald Krautscheid, K.V. Domasevitch

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  20. Ionic liquids and deep eutectic mixtures as new solvents for the synthesis of vanadium fluorides and oxyfluorides

    Dalton Transactions · 2011-01-01

    Farida H. Aidoudi, P.J. Byrne, Pheobe K. Allan, Simon J. Teat, Philip Lightfoot, Russell E. Morris

    Read original paper ↗ ·

  21. Vanadium fluoroarsenates—folding sheets into highly corrugated layers and crystalline arrays of large inorganic tubes

    Chemical Communications · 2011-01-01

    Eleni Kotsapa, Mark T. Weller

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  22. Hydrothermal syntheses and structures of vanadium oxyfluorides templated by organic and metal organic cations

    Inorganica Chimica Acta · 2011-09-10

    Tiffany M. Smith, Michael Tichenor, Jose Marcelo Vargas, Charles J. O’Connor, Jon A. Zubieta

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  23. Synthesis, crystal and electronic structure, and theoretical investigations of charge-transfer, optical, and bonding properties of a [VF6]3− anion compound

    Monatshefte für Chemie - Chemical Monthly · 2011-12-22

    Yi-Ping Tong, Hong Shu Liu, Zhen Jin, Yan‐Wen Lin

    Read original paper ↗ ·

  24. The Role of Polar, Lamdba (Λ)-Shaped Building Units in Noncentrosymmetric Inorganic Structures

    Journal of the American Chemical Society · 2012-02-15

    Martin D. Donakowski, Romain Gautier, Jeongho Yeon, Donald T. Moore, Juan C. Nino, P. Shiv Halasyamani, Kenneth Reinhard Poeppelmeier

    Read original paper ↗ ·

  25. Lead Fluoridooxidovanadates(V), Pb(V 2 O 2 F 8 ), Pb(VOF 5 ), and Mixed Valent Fluoridooxidovanadate(IV, V), Pb 3 F(V 4 O 3 F 18 )

    Zeitschrift für anorganische und allgemeine Chemie · 2012-06-20

    Matic Lozinšek, Evgeny Goreshnik, Boris Žemva

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  26. The Dimeric [V2O4F6]4– Vanadium Oxide‐Fluoride Anion in Na2(M(H2O)2)(V2O4F6) (M = Co2+, Ni2+, and Cu2+)

    Zeitschrift für anorganische und allgemeine Chemie · 2012-06-27

    Martin D. Donakowski, Anastasiya I. Vinokur, Kenneth Reinhard Poeppelmeier

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  27. AgI/VV Heterobimetallic Frameworks Generated from Novel-Type {Ag2(VO2F2)2(triazole)4} Secondary Building Blocks: A New Aspect in the Design of SVOF Hybrids

    Inorganic Chemistry · 2012-07-25

    Ganna A. Senchyk, Valerii Bukhanko, A.B. Lysenko, Harald Krautscheid, Eduard B. Rusanov, A.N. Chernega, Mirosław Karbowiak, K.V. Domasevitch

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  28. New structural units in molybdenum oxyfluoride chemistry

    Journal of Fluorine Chemistry · 2012-08-09

    David W. Aldous, Philip Lightfoot

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  29. Influence of Hydrofluoric Acid Formation on Lithium Ion Insertion in Nanostructured V2O5

    The Journal of Physical Chemistry C · 2012-09-12

    Jing Wu, Nellymar Membreño, Wen‐Yueh Yu, Jaclyn D. Wiggins-Camacho, David W. Flaherty, Charles Buddie Mullins, Keith J. Stevenson

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  30. Solid state coordination chemistry: Structural consequences of varying diphosphonate tether length and fluoride incorporation in the copper–bisterpy/oxomolybdenum/organodiphosphonate system (bisterpy = 2,2′:4′,4″:2″,2″′-quarterpyridyl-6′,6″-di-2-pyridine)

    Inorganica Chimica Acta · 2012-11-02

    Stephanie Jones, Jose Marcelo Vargas, Steven Pellizzeri, Charles J. O’Connor, Jon A. Zubieta

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  31. The dimeric [V2O2F8]4− anion: Structural characterization of a magnetic basic-building-unit

    Journal of Solid State Chemistry · 2013-01-26

    Hongcheng Lu, Romain Gautier, Zuo-Xi Li, Wanqi Jie, Zheng‐Tang Liu, Kenneth Reinhard Poeppelmeier

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  32. Structure-Directing Self-Assembly, Structures and Characterization of Four d0-Transition Metal Oxide/Fluoride Compounds Constructed with Imidazole/1-Methylimidazole/1-Vinylimidazole and Copper(II)/Zinc(II)

    Crystal Growth & Design · 2013-01-28

    Yi-Ping Tong, Guo‐Tian Luo, Zhen Jin, You Shen, Huiru Liu

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  33. Crystal Structures and Raman Spectra of Imidazolium Poly[perfluorotitanate(IV)] Salts Containing the [TiF6]2–, ([Ti2F9]−)∞, and [Ti2F11]3– and the New [Ti4F20]4– and [Ti5F23]3– Anions

    Inorganic Chemistry · 2013-07-09

    Igor M. Shlyapnikov, Hélène P. A. Mercier, Evgeny Goreshnik, Gary J. Schrobilgen, Zoran Mazej

    Read original paper ↗ ·

  34. Structural diversity in hybrid vanadium( iv ) oxyfluorides based on a common building block

    Dalton Transactions · 2013-10-07

    Farida H. Aidoudi, Cameron Black, Kasun S. Athukorala Arachchige, Alexandra M. Z. Slawin, Russell E. Morris, Philip Lightfoot

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  35. Structural consequences of fluoride incorporation into oxovanadium-xylyldiphosphonates with charge compensating copper(II)-imine components

    Inorganica Chimica Acta · 2013-11-28

    Tiffany M. Smith, Luke Strauskulage, Kathryn Perrin, Diona Symester, Steve R. Freund, Jose Marcelo Vargas, Leonard Spînu, Jon A. Zubieta

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  36. Spin Frustration from cis-Edge or -Corner Sharing Metal-Centered Octahedra

    Journal of the American Chemical Society · 2013-12-02

    Romain Gautier, Kengo Oka, Takumi Kihara, Nitesh Kumar, Athinarayanan Sundaresan, Masashi Tokunaga, Masaki Azuma, Kenneth Reinhard Poeppelmeier

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  37. A hybrid vanadium fluoride with structurally isolated S = 1 kagome layers

    Dalton Transactions · 2014-01-01

    Farida H. Aidoudi, Lewis J. Downie, Russell E. Morris, Mark A. de Vries, Philip Lightfoot

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  38. Fluoroferrates with (dabcoH2)2+ or (dabcoH)+ Cations

    Zeitschrift für anorganische und allgemeine Chemie · 2014-02-13

    Ganna Darmograi, Laurent J. Jouffret, Annie Hémon‐Ribaud, M. Leblanc, Gilles Dujardin, V. Maisonneuve, Jérôme Lhoste

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  39. F−/OH− substitution in [H4tren]4+ and [H3tren]3+ hydroxyfluorotitanates(IV) and classification of tren cation configurations

    Journal of Solid State Chemistry · 2014-05-16

    Jérôme Lhoste, Monique Body, Christophe Legein, Annie Hémon‐Ribaud, M. Leblanc, V. Maisonneuve

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  40. Synthesis, Crystal Structure, Vibrational and Optical Properties of (Hdea)4(V7O19F)∙0.42H2O, an Original (V7O19F)4− Cluster Oxyfluoride

    Journal of Cluster Science · 2014-08-14

    Issam Omri, Mohsen Graia, Tahar Mhiri

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  41. Crystal Chemistry and Selected Physical Properties of Inorganic Fluorides and Oxide-Fluorides

    Chemical Reviews · 2014-08-19

    M. Leblanc, V. Maisonneuve, A. Tressaud

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  42. Syntheses of Two Vanadium Oxide–Fluoride Materials That Differ in Phase Matchability

    Inorganic Chemistry · 2014-08-19

    Martin D. Donakowski, Romain Gautier, Hongcheng Lu, T. Thao Tran, Jacqueline Cantwell, P. Shiv Halasyamani, Kenneth Reinhard Poeppelmeier

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  43. A New Vanadium (V) Coordination Based on [(H2C4O4)VO2F] n 2n− Polymeric Chains and Diethylammonium Cations, Synthesis, Crystal Structure, Vibrational and Optical Properties

    Journal of Cluster Science · 2014-11-08

    Issam Omri, Tahar Mhiri, Mohsen Graia

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  44. Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 6

    CrystEngComm · 2015-01-01

    Jeongho Yeon, Justin B. Felder, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

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  45. Fluoride-coordination chemistry in molecular and low-dimensional magnetism

    Coordination Chemistry Reviews · 2015-04-10

    Kasper S. Pedersen, Mikkel A. Sørensen, Jesper Bendix

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  46. V2O2F4(H2O)2·H2O: a new V4+layer structure related to VOF3

    Acta Crystallographica Section C Structural Chemistry · 2015-12-22

    Cameron Black, Philip Lightfoot

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  47. Bimetallic MOFs (H 3 O) x [Cu(MF 6 )(pyrazine) 2 ]·(4 − x)H 2 O (M = V 4+ , x = 0; M = Ga 3+ , x = 1): co-existence of ordered and disordered quantum spins in the V 4+ system

    Chemical Communications · 2016-01-01

    Jamie L. Manson, John A. Schlueter, Kerry E. Garrett, Paul Goddard, Tom Lancaster, Johannes S. Möller, Stephen J. Blundell, Andrew J. Steele, Isabel Franke, Francis Laurence Pratt, John Singleton, Jesper Bendix, Saul H. Lapidus, M. Uhlarz, Oscar E. Ayala-Valenzuela, R. McDonald, Mary Gurak, C. Baines

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  48. Revealing the electronic structure and optical properties of K6[Mo4O8F10] novel molybdenum oxyfluoride materials

    The Philosophical Magazine A Journal of Theoretical Experimental and Applied Physics · 2016-08-31

    A.H. Reshak

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  49. Complexes of vanadium(IV) oxide difluoride with neutral N- and O-donor ligands

    Journal of Fluorine Chemistry · 2016-10-09

    Yao‐Pang Chang, Liam Furness, William Levason, Gillian Reid, Wenjian Zhang

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  50. Design and Assembly of Covalently Functionalised Polyoxofluorovanadate Molecular Hybrids

    Chemistry - A European Journal · 2018-01-10

    Maria Nicolaou, Michael G. Papanikolaou, Athanassios C. Tsipis, Themistoklis A. Kabanos, Anastasios D. Keramidas, Stephen A. Sproules, Haralampos N. Miras

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