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RESEARCH PAPER · Inorganic Chemistry · 2008

Hydrothermal Synthesis of Vanadium Oxyfluoride Chains Incorporating Covalently Bound Copper Coordination Complexes

Thushitha Mahenthirarajah, Yang Li, Philip Lightfoot

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Hydrothermal Synthesis of Vanadium Oxyfluoride Chains Incorporating Covalently Bound Copper Coordination ComplexesOriginalChemInform Abstract: Hydrothermal Synthesis of Vanadium Oxyfluoride Chains Incorporating Covalently Bound Copper Coordination Complexes.0The Hydrothermal and Structural Chemistry of Oxovanadium−Arylphosphonate Networks and Frameworks72Organic–inorganic hybrid chains and layers constructed from copper-amine cations and early transition metal (Nb, Mo) oxyfluoride anions21Novel building units with bimetallic rings in inorganic/organic hybrid chains and layers2Solvatothermal chemistry of organically-templated vanadium fluorides and oxyfluorides21Hydrothermal synthesis and structural characterization of bimetallic organic–inorganic hybrid materials: Copper vanadate–1,4-Carboxy-phenylphosphonate phases15Structural chemistry of organically-templated metal fluorides61Hydrothermal synthesis and structure of a two-dimensional bimetallic copper–molybdophosphonate, [{Cu4(H2O)2(phenbisterpy)2(HO3P(CH2)4PO3H)}(Mo4FO12)2{O3P(CH2)4PO3}]·4H2O, constructed from {Mo4FO12}1− clusters and copper-ligand chains (phenbisterpy = 1,4-bis(2,2′:6′,2′′-terpyridin-4′-yl)benzene)15Four divalent transition metal carboxyarylphosphonate compounds: Hydrothermal synthesis, structural chemistry and generalized 2D FTIR correlation spectroscopy studies16A three-dimensional heterometallic CuI/VIV1,2-bis(1,2,4-triazol-4-yl)ethane framework: a new insight into the structure of vanadium oxyfluoride coordination hybrids2Mixed metalII–metalIV hybrid fluorides11Hydrothermal syntheses and structures of vanadium oxyfluorides templated by organic and metal organic cations9The Role of Polar, Lamdba (Λ)-Shaped Building Units in Noncentrosymmetric Inorganic Structures139AgI/VV Heterobimetallic Frameworks Generated from Novel-Type {Ag2(VO2F2)2(triazole)4} Secondary Building Blocks: A New Aspect in the Design of SVOF Hybrids59Influence of Hydrofluoric Acid Formation on Lithium Ion Insertion in Nanostructured V2O516Solid state coordination chemistry: Structural consequences of varying diphosphonate tether length and fluoride incorporation in the copper–bisterpy/oxomolybdenum/organodiphosphonate system (bisterpy = 2,2′:4′,4″:2″,2″′-quarterpyridyl-6′,6″-di-2-pyridine)16The dimeric [V2O2F8]4− anion: Structural characterization of a magnetic basic-building-unit18Structural diversity in hybrid vanadium( iv ) oxyfluorides based on a common building block27Structural consequences of fluoride incorporation into oxovanadium-xylyldiphosphonates with charge compensating copper(II)-imine components13[ReF6]2−: A Robust Module for the Design of Molecule‐Based Magnetic Materials110[ReF6]2−: A Robust Module for the Design of Molecule‐Based Magnetic Materials20Synthesis, Crystal Structure, Vibrational and Optical Properties of (Hdea)4(V7O19F)∙0.42H2O, an Original (V7O19F)4− Cluster Oxyfluoride9A New Vanadium (V) Coordination Based on [(H2C4O4)VO2F] n 2n− Polymeric Chains and Diethylammonium Cations, Synthesis, Crystal Structure, Vibrational and Optical Properties2Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 617Fluoride-coordination chemistry in molecular and low-dimensional magnetism67Bimetallic MOFs (H 3 O) x [Cu(MF 6 )(pyrazine) 2 ]·(4 − x)H 2 O (M = V 4+ , x = 0; M = Ga 3+ , x = 1): co-existence of ordered and disordered quantum spins in the V 4+ system6Divanadate-based inorganic-organic hybrid compound: {[Cu(En)2]2V2O7} · 4H2O1Design and Assembly of Covalently Functionalised Polyoxofluorovanadate Molecular Hybrids10Controlled one pot synthesis of polyoxofluorovanadate molecular hybrids exhibiting peroxidase like activity4Theoretical studies of structural, electronic, and magnetic properties for small V2Fn0,− (2 ≤ n ≤ 7) clusters using first-principles calculations2Crystal structure of tetrakis[μ-3-carboxy-1-(1,2,4-triazol-4-yl)adamantane-κ2 N 1:N 2]tetrafluoridodi-μ2-oxido-dioxidodisilver(I)divanadium(V) tetrahydrate3Influence of structure-directing polyhedra and heterocyclic ligands on the chain structures and O/F ordering in a series of zinc vanadium oxyfluorides1Thermal properties of the hybrid compound [Cu(en)2(VO3)2]•3H2O — phase analysis upon heating and cooling. Crystal structure characterization of its two polymorphic modifications1Controllable Syntheses, Crystal Structure Evolution, and Photoluminescence of Polymorphic Zirconium Oxyfluorides6Synthesis and characterisation of Vanadium(III) fluorides α-BaVF5 and BaV(F,OH)5 with an S = 1 spin chain structure1

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  1. ChemInform Abstract: Hydrothermal Synthesis of Vanadium Oxyfluoride Chains Incorporating Covalently Bound Copper Coordination Complexes.

    ChemInform · 2008-11-20

    Thushitha Mahenthirarajah, Yang Li, Philip Lightfoot

    Read original paper ↗ ·

  2. The Hydrothermal and Structural Chemistry of Oxovanadium−Arylphosphonate Networks and Frameworks

    Inorganic Chemistry · 2008-12-23

    W. Ouellette, Guangbin Wang, Hongxue Liu, G.T. Yee, Charles J. O’Connor, Jon A. Zubieta

    Read original paper ↗ ·

  3. Organic–inorganic hybrid chains and layers constructed from copper-amine cations and early transition metal (Nb, Mo) oxyfluoride anions

    Dalton Transactions · 2009-01-01

    Thushitha Mahenthirarajah, Yang Li, Philip Lightfoot

    Read original paper ↗ ·

  4. Novel building units with bimetallic rings in inorganic/organic hybrid chains and layers

    Journal of Solid State Chemistry · 2009-09-10

    Thushitha Mahenthirarajah, Yang Li, Philip Lightfoot

    Read original paper ↗ ·

  5. Solvatothermal chemistry of organically-templated vanadium fluorides and oxyfluorides

    Inorganica Chimica Acta · 2009-10-15

    P. DeBurgomaster, W. Ouellette, Hongxue Liu, Charles J. O’Connor, G.T. Yee, Jon A. Zubieta

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  6. Hydrothermal synthesis and structural characterization of bimetallic organic–inorganic hybrid materials: Copper vanadate–1,4-Carboxy-phenylphosphonate phases

    Inorganica Chimica Acta · 2009-10-30

    P. DeBurgomaster, Hongxue Liu, Charles J. O’Connor, Jon A. Zubieta

    Read original paper ↗ ·

  7. Structural chemistry of organically-templated metal fluorides

    Dalton Transactions · 2010-01-01

    Karim Adil, M. Leblanc, V. Maisonneuve, Philip Lightfoot

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  8. Hydrothermal synthesis and structure of a two-dimensional bimetallic copper–molybdophosphonate, [{Cu4(H2O)2(phenbisterpy)2(HO3P(CH2)4PO3H)}(Mo4FO12)2{O3P(CH2)4PO3}]·4H2O, constructed from {Mo4FO12}1− clusters and copper-ligand chains (phenbisterpy = 1,4-bis(2,2′:6′,2′′-terpyridin-4′-yl)benzene)

    Inorganic Chemistry Communications · 2010-02-05

    Stephanie Jones, Hongxue Liu, W. Ouellette, Katherine Schmidtke, Charles J. O’Connor, Jon A. Zubieta

    Read original paper ↗ ·

  9. Four divalent transition metal carboxyarylphosphonate compounds: Hydrothermal synthesis, structural chemistry and generalized 2D FTIR correlation spectroscopy studies

    Journal of Solid State Chemistry · 2010-05-01

    Lei Ran, Xiao‐Chuan Chai, Hong-Xin Mei, Han-Hui Zhang, Yi‐Ping Chen, Yan‐Qiong Sun

    Read original paper ↗ ·

  10. A three-dimensional heterometallic CuI/VIV1,2-bis(1,2,4-triazol-4-yl)ethane framework: a new insight into the structure of vanadium oxyfluoride coordination hybrids

    Acta Crystallographica Section C Crystal Structure Communications · 2010-08-27

    Olena V. Sharga, A.B. Lysenko, Harald Krautscheid, K.V. Domasevitch

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  11. Mixed metalII–metalIV hybrid fluorides

    Journal of Fluorine Chemistry · 2011-05-02

    Jérôme Lhoste, Karim Adil, Armel Le Bail, M. Leblanc, Annie Hémon‐Ribaud, V. Maisonneuve

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  12. Hydrothermal syntheses and structures of vanadium oxyfluorides templated by organic and metal organic cations

    Inorganica Chimica Acta · 2011-09-10

    Tiffany M. Smith, Michael Tichenor, Jose Marcelo Vargas, Charles J. O’Connor, Jon A. Zubieta

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  13. The Role of Polar, Lamdba (Λ)-Shaped Building Units in Noncentrosymmetric Inorganic Structures

    Journal of the American Chemical Society · 2012-02-15

    Martin D. Donakowski, Romain Gautier, Jeongho Yeon, Donald T. Moore, Juan C. Nino, P. Shiv Halasyamani, Kenneth Reinhard Poeppelmeier

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  14. AgI/VV Heterobimetallic Frameworks Generated from Novel-Type {Ag2(VO2F2)2(triazole)4} Secondary Building Blocks: A New Aspect in the Design of SVOF Hybrids

    Inorganic Chemistry · 2012-07-25

    Ganna A. Senchyk, Valerii Bukhanko, A.B. Lysenko, Harald Krautscheid, Eduard B. Rusanov, A.N. Chernega, Mirosław Karbowiak, K.V. Domasevitch

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  15. Influence of Hydrofluoric Acid Formation on Lithium Ion Insertion in Nanostructured V2O5

    The Journal of Physical Chemistry C · 2012-09-12

    Jing Wu, Nellymar Membreño, Wen‐Yueh Yu, Jaclyn D. Wiggins-Camacho, David W. Flaherty, Charles Buddie Mullins, Keith J. Stevenson

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  16. Solid state coordination chemistry: Structural consequences of varying diphosphonate tether length and fluoride incorporation in the copper–bisterpy/oxomolybdenum/organodiphosphonate system (bisterpy = 2,2′:4′,4″:2″,2″′-quarterpyridyl-6′,6″-di-2-pyridine)

    Inorganica Chimica Acta · 2012-11-02

    Stephanie Jones, Jose Marcelo Vargas, Steven Pellizzeri, Charles J. O’Connor, Jon A. Zubieta

    Read original paper ↗ ·

  17. The dimeric [V2O2F8]4− anion: Structural characterization of a magnetic basic-building-unit

    Journal of Solid State Chemistry · 2013-01-26

    Hongcheng Lu, Romain Gautier, Zuo-Xi Li, Wanqi Jie, Zheng‐Tang Liu, Kenneth Reinhard Poeppelmeier

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  18. Structural diversity in hybrid vanadium( iv ) oxyfluorides based on a common building block

    Dalton Transactions · 2013-10-07

    Farida H. Aidoudi, Cameron Black, Kasun S. Athukorala Arachchige, Alexandra M. Z. Slawin, Russell E. Morris, Philip Lightfoot

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  19. Structural consequences of fluoride incorporation into oxovanadium-xylyldiphosphonates with charge compensating copper(II)-imine components

    Inorganica Chimica Acta · 2013-11-28

    Tiffany M. Smith, Luke Strauskulage, Kathryn Perrin, Diona Symester, Steve R. Freund, Jose Marcelo Vargas, Leonard Spînu, Jon A. Zubieta

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  20. [ReF6]2−: A Robust Module for the Design of Molecule‐Based Magnetic Materials

    Angewandte Chemie International Edition · 2014-01-21

    Kasper S. Pedersen, Marc Sigrist, Mikkel A. Sørensen, Anne‐Laure Barra, Thomas Weyhermüller, Stergios Piligkos, Christian Aa. Thuesen, Morten G. Vinum, H. Mutka, Høgni Weihe, Rodolphe Clérac, Jesper Bendix

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  21. [ReF6]2−: A Robust Module for the Design of Molecule‐Based Magnetic Materials

    Angewandte Chemie · 2014-01-21

    Kasper S. Pedersen, Marc Sigrist, Mikkel A. Sørensen, Anne‐Laure Barra, Thomas Weyhermüller, Stergios Piligkos, Christian Aa. Thuesen, Morten G. Vinum, H. Mutka, Høgni Weihe, Rodolphe Clérac, Jesper Bendix

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  22. Synthesis, Crystal Structure, Vibrational and Optical Properties of (Hdea)4(V7O19F)∙0.42H2O, an Original (V7O19F)4− Cluster Oxyfluoride

    Journal of Cluster Science · 2014-08-14

    Issam Omri, Mohsen Graia, Tahar Mhiri

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  23. A New Vanadium (V) Coordination Based on [(H2C4O4)VO2F] n 2n− Polymeric Chains and Diethylammonium Cations, Synthesis, Crystal Structure, Vibrational and Optical Properties

    Journal of Cluster Science · 2014-11-08

    Issam Omri, Tahar Mhiri, Mohsen Graia

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  24. Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 6

    CrystEngComm · 2015-01-01

    Jeongho Yeon, Justin B. Felder, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

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  25. Fluoride-coordination chemistry in molecular and low-dimensional magnetism

    Coordination Chemistry Reviews · 2015-04-10

    Kasper S. Pedersen, Mikkel A. Sørensen, Jesper Bendix

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  26. Bimetallic MOFs (H 3 O) x [Cu(MF 6 )(pyrazine) 2 ]·(4 − x)H 2 O (M = V 4+ , x = 0; M = Ga 3+ , x = 1): co-existence of ordered and disordered quantum spins in the V 4+ system

    Chemical Communications · 2016-01-01

    Jamie L. Manson, John A. Schlueter, Kerry E. Garrett, Paul Goddard, Tom Lancaster, Johannes S. Möller, Stephen J. Blundell, Andrew J. Steele, Isabel Franke, Francis Laurence Pratt, John Singleton, Jesper Bendix, Saul H. Lapidus, M. Uhlarz, Oscar E. Ayala-Valenzuela, R. McDonald, Mary Gurak, C. Baines

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  27. Divanadate-based inorganic-organic hybrid compound: {[Cu(En)2]2V2O7} · 4H2O

    Russian Journal of Coordination Chemistry · 2017-11-01

    K. Wang, Jing Li, Zhijie Liang, P. T. Ma, Diaodiao Zhang, Jingyang Niu, J. P. Wang

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  28. Design and Assembly of Covalently Functionalised Polyoxofluorovanadate Molecular Hybrids

    Chemistry - A European Journal · 2018-01-10

    Maria Nicolaou, Michael G. Papanikolaou, Athanassios C. Tsipis, Themistoklis A. Kabanos, Anastasios D. Keramidas, Stephen A. Sproules, Haralampos N. Miras

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  29. Controlled one pot synthesis of polyoxofluorovanadate molecular hybrids exhibiting peroxidase like activity

    New Journal of Chemistry · 2019-01-01

    Maria Nicolaou, Chryssoula Drouza, Anastasios D. Keramidas

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  30. Theoretical studies of structural, electronic, and magnetic properties for small V2Fn0,− (2 ≤ n ≤ 7) clusters using first-principles calculations

    Journal of Nanoparticle Research · 2019-05-01

    Si‐Ying Zhong, Shao-Yi Wu, Peng Li, Guijun Chen, Qing Zhang, Xiao-Hong Chen

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  31. Crystal structure of tetrakis[μ-3-carboxy-1-(1,2,4-triazol-4-yl)adamantane-κ2 N 1:N 2]tetrafluoridodi-μ2-oxido-dioxidodisilver(I)divanadium(V) tetrahydrate

    Acta Crystallographica Section E Crystallographic Communications · 2019-05-17

    Ganna A. Senchyk, A.B. Lysenko, Eduard B. Rusanov, K.V. Domasevitch

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  32. Influence of structure-directing polyhedra and heterocyclic ligands on the chain structures and O/F ordering in a series of zinc vanadium oxyfluorides

    CrystEngComm · 2020-01-01

    Belal Ahmed, Hongil Jo, Suheon Lee, Kwang‐Yong Choi, Kang Min Ok

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  33. Thermal properties of the hybrid compound [Cu(en)2(VO3)2]•3H2O — phase analysis upon heating and cooling. Crystal structure characterization of its two polymorphic modifications

    Journal of Molecular Structure · 2021-01-13

    Gabriela Stehlíková, Róbert Gyepes, Roman Bystrický, M. Škrátek, P. Vaněk, Jozef Tatiersky

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  34. Controllable Syntheses, Crystal Structure Evolution, and Photoluminescence of Polymorphic Zirconium Oxyfluorides

    Inorganic Chemistry · 2021-09-01

    Chen Li, Ting Bin Wen, Ke Liu, Dequan Jiang, Zimin Jiang, Yonggang Wang

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  35. Synthesis and characterisation of Vanadium(III) fluorides α-BaVF5 and BaV(F,OH)5 with an S = 1 spin chain structure

    Journal of Solid State Chemistry · 2024-11-08

    Qingqing Huang, Xiedong Cheng, Feifan Li, Yaping Li, Rui Cui, Minfeng Lü

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