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RESEARCH PAPER · Particle & Particle Systems Characterization · 2013

In Situ Synchrotron X‐Ray Techniques for Real‐Time Probing of Colloidal Nanoparticle Synthesis

Yugang Sun, Yang Ren

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In Situ Synchrotron X‐Ray Techniques for Real‐Time Probing of Colloidal Nanoparticle SynthesisOriginalLow temperature survival of slender naiad (Najas flexilis) seeds.4A comprehensive study of the crystallization mechanism involved in the nonaqueous formation of tungstite33Observation of growth of metal nanoparticles146Watching materials form:in situtotal scattering studies of nanoparticle synthesis0Watching materials form:in situtotal scattering studies of nanoparticle synthesis1Quantitative determination of fragmentation kinetics and thermodynamics of colloidal silver nanowires by in situ high-energy synchrotron X-ray diffraction22In Situ Studies of Solvothermal Synthesis of Energy Materials159COLLOIDAL PREPARATION OF MONODISPERSE NANOCRYSTALS7Controlling Allotropism in Ruthenium Nanoparticles: A Pulsed-Flow Supercritical Synthesis and in Situ Synchrotron X-ray Diffraction Study41In Situ Powder Diffraction Study of the Hydrothermal Synthesis of ZnO Nanoparticles49Colloidal nanoparticles as advanced biological sensors1024On the Two-Step Mechanism for Synthesis of Transition-Metal Nanoparticles40Oriented attachment of particles: 100 years of investigations of non-classical crystal growth214Silver chlorobromide nanocubes with significantly improved uniformity: synthesis and assembly into photonic crystals24Pulsed-Flow Near-Critical and Supercritical Synthesis of Carbon-Supported Platinum Nanoparticles and In Situ X-ray Diffraction Study of Their Formation and Growth9In situ high-energy synchrotron X-ray diffraction revealing precipitation reaction kinetics of silver ions with mixed halide ions9Ultrathin Gold Nanowires: Soft-Templating versus Liquid Phase Synthesis, a Quantitative Study51Real-Time in Situ Probing of High-Temperature Quantum Dots Solution Synthesis106Interfaced heterogeneous nanodimers89Analysis of Particle Size Distributions of Quantum Dots: From Theory to Application33Quantifying the Nucleation and Growth Kinetics of Microwave Nanochemistry Enabled by in Situ High-Energy X-ray Scattering53Detection and characterisation of sub-critical nuclei during reactive Pd metal nucleation by X-ray absorption spectroscopy11Three‐Dimensional Self Assembly of Semiconducting Colloidal Nanocrystals: From Fundamental Forces to Collective Optical Properties34Revealing Complexity of Nanoparticle Synthesis in Solution by in Situ Hard X-ray Spectroscopy─Today and Beyond52Energy dispersive-EXAFS of Pd nucleation at a liquid/liquid interface6Liquid Cell Transmission Electron Microscopy155Organic Phase Syntheses of Magnetic Nanoparticles and Their Applications601Synthesis of Semiconductor Nanocrystals, Focusing on Nontoxic and Earth-Abundant Materials635Quantitatively in Situ Imaging Silver Nanowire Hollowing Kinetics27Interlayer-expanded MoS 2381Well-Defined Metal Nanoparticles for Electrocatalysis10In situ XAFS Study of Palladium Electrodeposition at the Liquid/Liquid Interface12Perspectives on in situ electron microscopy38Quantitative 3D evolution of colloidal nanoparticle oxidation in solution150Ternary Silver Halide Nanocrystals52Surface plasmon band tailoring of plasmonic nanostructure under the effect of water radiolysis by synchrotron radiation10Ionic Conductivity Measurements—A Powerful Tool for Monitoring Polyol Reduction Reactions10Tuning Precursor Reactivity toward Nanometer-Size Control in Palladium Nanoparticles Studied by in Situ Small Angle X-ray Scattering48Wet‐Chemical Synthesis of Pd‐Au Core‐Shell Nanoparticles (8 nm): From Nanostructure to Biological Properties18Facile Low Temperature Hydrothermal Synthesis of BaTiO3 Nanoparticles Studied by In Situ X-ray Diffraction21In Situ Techniques for Probing Kinetics and Mechanism of Hollowing Nanostructures through Direct Chemical Transformations14Anisotropic Assembly during Heat‐Up: The Early Stage Hydrothermal Synthesis of TiO2 from a Complexed Precursor1On the Formation of Palladium (II) Iodide Nanoparticles: An In Situ SAXS/XAS Study and Catalytic Evaluation on an Aryl Alkenylation Reaction in Water Medium8An extreme-condition model for quantifying growth kinetics of colloidal metal nanoparticles10In Situ Synchrotron X‐ray Characterization Shining Light on the Nucleation and Growth Kinetics of Colloidal Nanoparticles53In Situ Synchrotron X‐ray Characterization Shining Light on the Nucleation and Growth Kinetics of Colloidal Nanoparticles4Insights into the Formation Mechanism of CdSe Nanoplatelets Using in Situ X-ray Scattering43Insights into Reaction Intermediates to Predict Synthetic Pathways for Shape-Controlled Metal Nanocrystals82Nanoengineering of Gold Nanoparticles: Green Synthesis, Characterization, and Applications42Advances in carbon dots: from the perspective of traditional quantum dots411Selective magnetometry of superparamagnetic iron oxide nanoparticles in liquids8From platinum atoms in molecules to colloidal nanoparticles: A review on reduction, nucleation and growth mechanisms108Insights into Growth Kinetics of Colloidal Gold Nanoparticles: In Situ SAXS and UV–Vis Evaluation39Dynamics of the nanocrystal structure and composition in growth solutions monitored by in situ lab-scale X-ray diffraction6Magnetic nanoparticles10Particle formation mechanisms supported by in situ synchrotron XAFS and SAXS studies: a review of metal, metal-oxide, semiconductor and selected other nanoparticle formation reactions36Identification of LiH and nanocrystalline LiF in the solid–electrolyte interphase of lithium metal anodes318Biological and Medical Applications of Calcium Phosphate Nanoparticles151In Situ Synchrotron X‐Ray Absorption Spectroscopy Studies of Anode Materials for Rechargeable Batteries47Insights into Nucleation and Growth of Colloidal Quaternary Nanocrystals by Multimodal X-ray Analysis29Nanoparticle Formation Kinetics, Mechanisms, and Accurate Rate Constants: Examination of a Second-Generation Ir(0)n Particle Formation System by Five Monitoring Methods Plus Initial Mechanism-Enabled Population Balance Modeling10In situ scattering studies of material formation during wet-chemical syntheses1A combined TEM and SAXS study of the growth and self-assembly of ultrathin Pt nanowires3In Situ Kinetic Observations on Crystal Nucleation and Growth386Synthesis and Self-Assembly of colloidal nanoparticles into two-dimensional superlattices0Case Studies: Time-Resolved X-Ray Absorption Spectroscopy (XAS)11Formation of intermetallic PdIn nanoparticles: influence of surfactants on nanoparticle atomic structure5Recent advances in microfluidics-enabled controlled reaction, assembly and exfoliation of inorganic nanomaterials6Advanced Characterization Techniques and Theoretical Calculation2The Nanoscience Paradigm: “Size Matters!”3Fluorine Chemistry in Rechargeable Batteries: Challenges, Progress, and Perspectives255Real-Time Multiscale Imaging of Heterogeneous Multistage Reactions: Insights into Nanoscale TiO2 Synthesis9Li Alloy/Li Halide Mixed Layer: An Emerging Star for Electro-Chemo-Mechanically Stable Li/Electrolyte Interface23Operando Synchrotron X‐Ray Absorption Spectroscopy: A Key Tool for Cathode Material Studies in Next‐Generation Batteries55Principles and Practices for Quantum Dots Synthesis0

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  1. Low temperature survival of slender naiad (Najas flexilis) seeds.

    PubMed · 2002-07-31

    F.R. Hay, J SK Muir

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  2. A comprehensive study of the crystallization mechanism involved in the nonaqueous formation of tungstite

    Nanoscale · 2013-01-01

    Inga Olliges‐Stadler, Marta D. Rossell, Martin Süess, Bettina Ludi, Oliver Bunk, Jan Skov Pedersen, Henrik Birkedal, Markus Niederberger

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  3. Observation of growth of metal nanoparticles

    Chemical Communications · 2013-01-01

    Hong‐Gang Liao, Kai‐Yang Niu, Haimei Zheng

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  4. Watching materials form:in situtotal scattering studies of nanoparticle synthesis

    Acta Crystallographica Section A Foundations of Crystallography · 2013-08-25

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Mogens Christensen, Espen Drath Bøjesen, Nina Lock, Simon J. L. Billinge, Bo B. Iversen

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  5. Watching materials form:in situtotal scattering studies of nanoparticle synthesis

    Acta Crystallographica Section A Foundations of Crystallography · 2013-08-25

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Mogens Christensen, Espen Drath Bøjesen, Nina Lock, Simon J. L. Billinge, Bo B. Iversen

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  6. Quantitative determination of fragmentation kinetics and thermodynamics of colloidal silver nanowires by in situ high-energy synchrotron X-ray diffraction

    Nanoscale · 2013-10-22

    Zheng Li, John Okasinski, Jonathan Almer, Yang Ren, Xiaobing Zuo, Yugang Sun

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  7. In Situ Studies of Solvothermal Synthesis of Energy Materials

    ChemSusChem · 2014-03-05

    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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  8. COLLOIDAL PREPARATION OF MONODISPERSE NANOCRYSTALS

    Journal of Molecular and Engineering Materials · 2014-03-12

    Shuang‐Yuan Zhang, Michelle D. Regulacio, Kwok Wei Shah, Thammanoon Sreethawong, Yuangang Zheng, Ming‐Yong Han

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  9. Controlling Allotropism in Ruthenium Nanoparticles: A Pulsed-Flow Supercritical Synthesis and in Situ Synchrotron X-ray Diffraction Study

    The Journal of Physical Chemistry C · 2014-04-07

    Jianli Mi, Yanbin Shen, Jacob Becker, Martin Bremholm, Bo B. Iversen

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  10. In Situ Powder Diffraction Study of the Hydrothermal Synthesis of ZnO Nanoparticles

    Crystal Growth & Design · 2014-04-16

    Espen Drath Bøjesen, Kirsten M. Ø. Jensen, Christoffer Tyrsted, Nina Lock, Mogens Christensen, Bo B. Iversen

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  11. Colloidal nanoparticles as advanced biological sensors

    Science · 2014-10-02

    Philip D. Howes, Rona Chandrawati, Molly M. Stevens

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  12. On the Two-Step Mechanism for Synthesis of Transition-Metal Nanoparticles

    Langmuir · 2014-10-02

    Siva Rama Krishna Perala, Sanjeev Kumar

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  13. Oriented attachment of particles: 100 years of investigations of non-classical crystal growth

    Russian Chemical Reviews · 2014-10-08

    Vladimir K. Ivanov, П. П. Федоров, Alexander E. Baranchikov, Vyacheslav V Osiko

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  14. Silver chlorobromide nanocubes with significantly improved uniformity: synthesis and assembly into photonic crystals

    Journal of Materials Chemistry C · 2014-10-27

    Zheng Li, John Okasinski, David J. Gosztola, Yang Ren, Yugang Sun

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  15. Pulsed-Flow Near-Critical and Supercritical Synthesis of Carbon-Supported Platinum Nanoparticles and In Situ X-ray Diffraction Study of Their Formation and Growth

    Chemistry of Materials · 2014-12-22

    Jianli Mi, Henrik Fanø Clausen, Martin Bremholm, Mette Stokkebro Schmøkel, Patricia Hernandez-Fernandez, Jacob Becker, Bo B. Iversen

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  16. In situ high-energy synchrotron X-ray diffraction revealing precipitation reaction kinetics of silver ions with mixed halide ions

    Journal of Materials Chemistry C · 2015-01-01

    Qi Liu, Zheng Li, John Okasinski, Yang Ren, Yugang Sun

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  17. Ultrathin Gold Nanowires: Soft-Templating versus Liquid Phase Synthesis, a Quantitative Study

    The Journal of Physical Chemistry C · 2015-02-04

    Anaïs Loubat, Lise‐Marie Lacroix, Antoine Robert, Marianne Impéror‐Clerc, Romuald Poteau, Laurent Maron, Raúl Arenal, Brigitte Pansu, Guillaume Viau

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  18. Real-Time in Situ Probing of High-Temperature Quantum Dots Solution Synthesis

    Nano Letters · 2015-03-27

    Benjamin Abécassis, Cécile Bouet, Cyril Garnero, Doru Constantin, Nicolas Lequeux, Sandrine Ithurria, Benoît Dubertret, Brian Richard Pauw, Diego Pontoni

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  19. Interfaced heterogeneous nanodimers

    National Science Review · 2015-07-12

    Yugang Sun

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  20. Analysis of Particle Size Distributions of Quantum Dots: From Theory to Application

    KONA Powder and Particle Journal · 2015-09-09

    Doris Segets

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  21. Quantifying the Nucleation and Growth Kinetics of Microwave Nanochemistry Enabled by in Situ High-Energy X-ray Scattering

    Nano Letters · 2015-12-01

    Qi Liu, Min‐Rui Gao, Yuzi Liu, John Okasinski, Yang Ren, Yugang Sun

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  22. Detection and characterisation of sub-critical nuclei during reactive Pd metal nucleation by X-ray absorption spectroscopy

    CrystEngComm · 2015-12-03

    Sin-Yuen Chang, Yvonne Gründer, Samuel Guy Booth, L. B. Molleta, Akihiro Uehara, J. Frederick W. Mosselmans, Giannantonio Cibin, Van‐Thai Pham, Lucie Nataf, Robert A. W. Dryfe, Sven L. M. Schroeder

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  23. Three‐Dimensional Self Assembly of Semiconducting Colloidal Nanocrystals: From Fundamental Forces to Collective Optical Properties

    ChemPhysChem · 2015-12-11

    Benjamin Abécassis

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  24. Revealing Complexity of Nanoparticle Synthesis in Solution by in Situ Hard X-ray Spectroscopy─Today and Beyond

    Chemistry of Materials · 2016-04-08

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  25. Energy dispersive-EXAFS of Pd nucleation at a liquid/liquid interface

    Journal of Physics Conference Series · 2016-05-01

    S-Y Chang, Samuel Guy Booth, Akihiro Uehara, J. Frederick W. Mosselmans, Giannantonio Cibin, V-T Pham, Lucie Nataf, Robert A. W. Dryfe, Sven L. M. Schroeder

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  26. Liquid Cell Transmission Electron Microscopy

    Annual Review of Physical Chemistry · 2016-05-24

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  27. Organic Phase Syntheses of Magnetic Nanoparticles and Their Applications

    Chemical Reviews · 2016-06-29

    Liheng Wu, Adriana Mendoza‐Garcia, Qing Li, Shouheng Sun

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  28. Synthesis of Semiconductor Nanocrystals, Focusing on Nontoxic and Earth-Abundant Materials

    Chemical Reviews · 2016-07-08

    Peter Reiß, Marie Carrière, Christophe Lincheneau, Louis Vaure, Sudarsan Tamang

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  29. Quantitatively in Situ Imaging Silver Nanowire Hollowing Kinetics

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    Le Yu, Zhongying Yan, Zhonghou Cai, Dongtang Zhang, Ping Han, Xuemei M. Cheng, Yugang Sun

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  30. Interlayer-expanded MoS 2

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  31. Well-Defined Metal Nanoparticles for Electrocatalysis

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  32. In situ XAFS Study of Palladium Electrodeposition at the Liquid/Liquid Interface

    Electrochimica Acta · 2017-03-14

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  33. Perspectives on in situ electron microscopy

    Ultramicroscopy · 2017-03-29

    Haimei Zheng, Yimei Zhu

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  34. Quantitative 3D evolution of colloidal nanoparticle oxidation in solution

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    Yugang Sun, Xiaobing Zuo, Subramanian K. R. S. Sankaranarayanan, Sheng Peng, Badri Narayanan, Ganesh Kamath

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  35. Ternary Silver Halide Nanocrystals

    Accounts of Chemical Research · 2017-06-27

    Sasitha C. Abeyweera, Kowsalya Devi Rasamani, Yugang Sun

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  36. Surface plasmon band tailoring of plasmonic nanostructure under the effect of water radiolysis by synchrotron radiation

    Journal of Synchrotron Radiation · 2017-10-17

    Amardeep Bharti, Ashish Kumar Agrawal, Balwant Singh, Sanjeev Gautam, Navdeep Goyal

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  37. Ionic Conductivity Measurements—A Powerful Tool for Monitoring Polyol Reduction Reactions

    Langmuir · 2017-10-30

    Hany A. El‐Sayed, Veronika M. Burger, Melanie Miller, Klaus F. Wagenbauer, Manuel F. Wagenhofer, Hubert Andreas Gasteiger

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  38. Tuning Precursor Reactivity toward Nanometer-Size Control in Palladium Nanoparticles Studied by in Situ Small Angle X-ray Scattering

    Chemistry of Materials · 2018-01-04

    Liheng Wu, Huada Lian, Joshua J. Willis, Emmett D. Goodman, Ian S. McKay, Jian Qin, Christopher J. Tassone, Matteo Cargnello

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  39. Wet‐Chemical Synthesis of Pd‐Au Core‐Shell Nanoparticles (8 nm): From Nanostructure to Biological Properties

    ChemistrySelect · 2018-05-07

    Alexander Rostek, Marina Breisch, Kateryna Loza, Paulo R. A. F. Garcia, Cristiano L. P. Oliveira, Oleg Prymak, Marc Heggen, Manfred Köller, Christina Sengstock, Matthias Epple

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  40. Facile Low Temperature Hydrothermal Synthesis of BaTiO3 Nanoparticles Studied by In Situ X-ray Diffraction

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    Ola G. Grendal, Anders B. Blichfeld, Susanne Linn Skjærvø, Wouter van Beek, Sverre M. Selbach, Tor Grande, Mari‐Ann Einarsrud

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  41. In Situ Techniques for Probing Kinetics and Mechanism of Hollowing Nanostructures through Direct Chemical Transformations

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  42. Anisotropic Assembly during Heat‐Up: The Early Stage Hydrothermal Synthesis of TiO2 from a Complexed Precursor

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  43. On the Formation of Palladium (II) Iodide Nanoparticles: An In Situ SAXS/XAS Study and Catalytic Evaluation on an Aryl Alkenylation Reaction in Water Medium

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  44. An extreme-condition model for quantifying growth kinetics of colloidal metal nanoparticles

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  45. In Situ Synchrotron X‐ray Characterization Shining Light on the Nucleation and Growth Kinetics of Colloidal Nanoparticles

    Angewandte Chemie International Edition · 2019-03-04

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  46. In Situ Synchrotron X‐ray Characterization Shining Light on the Nucleation and Growth Kinetics of Colloidal Nanoparticles

    Angewandte Chemie · 2019-03-04

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  47. Insights into the Formation Mechanism of CdSe Nanoplatelets Using in Situ X-ray Scattering

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    Nicolò Castro, Cécile Bouet, Sandrine Ithurria, Nicolas Lequeux, Doru Constantin, Pierre Levitz, Diego Pontoni, Benjamin Abécassis

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  48. Insights into Reaction Intermediates to Predict Synthetic Pathways for Shape-Controlled Metal Nanocrystals

    Journal of the American Chemical Society · 2019-09-21

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  49. Nanoengineering of Gold Nanoparticles: Green Synthesis, Characterization, and Applications

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  50. Advances in carbon dots: from the perspective of traditional quantum dots

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