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RESEARCH PAPER · Inorganic Chemistry · 2007

Critical Role of Water Content in the Formation and Reactivity of Uranium, Neptunium, and Plutonium Iodates under Hydrothermal Conditions: Implications for the Oxidative Dissolution of Spent Nuclear Fuel

Travis H. Bray, Jie Ling, Eun Sang Choi, J. S. Brooks, James V. Beitz, Richard E. Sykora, Richard Geoffrey Haire, David M. Stanbury, Thomas E. Albrecht‐Schmitt

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Critical Role of Water Content in the Formation and Reactivity of Uranium, Neptunium, and Plutonium Iodates under Hydrothermal Conditions: Implications for the Oxidative Dissolution of Spent Nuclear FuelOriginalCritical Role of Water Content in the Formation and Reactivity of Uranium, Neptunium, and Plutonium Iodates under Hydrothermal Conditions: Implications for the Oxidative Dissolution of Spent Nuclear Fuel.0In Situ Hydrothermal Reduction of Neptunium(VI) as a Route to Neptunium(IV) Phosphonates34Hydrothermal synthesis, structure, and magnetic properties of Pu(SeO3)212Capitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate40Capitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate7Periodic Trends in Actinide Phosphonates: Divergence and Convergence between Thorium, Uranium, Neptunium, and Plutonium Systems47Hydrothermal Synthesis and Crystal Structures of Actinide Compounds2USING PHOSPHONATES TO PROBE STRUCTURAL DIFFERENCES BETWEEN TRANSURANIUM ELEMENTS AND THEIR PROPOSED SURROGATES24Cerium(IV), Neptunium(IV), and Plutonium(IV) 1,2-Phenylenediphosphonates: Correlations and Differences between Early Transuranium Elements and Their Proposed Surrogates54Recent progress in actinide borate chemistry94Role of Anions and Reaction Conditions in the Preparation of Uranium(VI), Neptunium(VI), and Plutonium(VI) Borates56Facile Routes to ThIV, UIV, and NpIV Phosphites and Phosphates23Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) Phosphates43Incorporation of Neptunium(VI) into a Uranyl Selenite14Structural changes within the alkaline earth uranyl phosphites9From Order to Disorder and Back Again: In Situ Hydrothermal Redox Reactions of Uranium Phosphites and Phosphates28Syntheses, Structures, and Comparisons of Thallium Uranium Phosphites, Mixed Phosphate-Phosphites, and Phosphate22In[IO3](OH)2 – New member of hydrous and anhydrous iodate family with indium6Expansion of the Rich Structures and Magnetic Properties of Neptunium Selenites: Soft Ferromagnetism in Np(SeO3)213Monomers, Dimers, and Helices: Complexities of Cerium and Plutonium Phenanthrolinecarboxylates22Systematic Investigation of the in Situ Reduction Process from U(VI) to U(IV) in a Phosphonate System under Mild Solvothermal Conditions23Electronic Structure and Properties of Berkelium Iodates38Mild Periodic Acid Flux and Hydrothermal Methods for the Synthesis of Crystalline f-Element-Bearing Iodate Compounds20Unexpected Behavior of Np in Oxo-selenate/Oxo-selenite Systems9Synthesis, structure and characterization of M(IO 3 ) 2 (HIO 3 ) (M = Ca, Sr) as new anhydrous alkaline earth metal bis-iodate hydrogeniodate compounds16The first actinide polyiodate: a complex multifunctional compound with promising X-ray luminescence properties and proton conductivity17Natural and Anthropogenic Analogues for High-Level Nuclear Waste Disposal Repositories: A Review7The crystal and coordination chemistry of neptunium in all its oxidation states: An expanded structural hierarchy of neptunium compounds41Samarium Hydrogen Iodate, Sm(IO3)3·HIO3: Synthesis and Characterization0

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  1. Critical Role of Water Content in the Formation and Reactivity of Uranium, Neptunium, and Plutonium Iodates under Hydrothermal Conditions: Implications for the Oxidative Dissolution of Spent Nuclear Fuel.

    ChemInform · 2007-07-04

    Travis H. Bray, Jie Ling, Eun Sang Choi, J. S. Brooks, James V. Beitz, Richard E. Sykora, Richard Geoffrey Haire, David M. Stanbury, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  2. In Situ Hydrothermal Reduction of Neptunium(VI) as a Route to Neptunium(IV) Phosphonates

    Inorganic Chemistry · 2007-11-21

    Travis H. Bray, Anna‐Gay D. Nelson, Geng Bang Jin, Richard Geoffrey Haire, Thomas E. Albrecht‐Schmitt

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  3. Hydrothermal synthesis, structure, and magnetic properties of Pu(SeO3)2

    Journal of Solid State Chemistry · 2008-01-02

    Travis H. Bray, S. Skanthakumar, L. Soderholm, Richard E. Sykora, Richard Geoffrey Haire, Thomas E. Albrecht‐Schmitt

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  4. Capitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate

    Angewandte Chemie International Edition · 2008-07-09

    Anna‐Gay D. Nelson, Travis H. Bray, Thomas E. Albrecht‐Schmitt

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  5. Capitalizing on Differing Coordination Environments and Redox Potentials to Prepare an Ordered Heterobimetallic UVI/NpIV Diphosphonate

    Angewandte Chemie · 2008-07-09

    Anna‐Gay D. Nelson, Travis H. Bray, Thomas E. Albrecht‐Schmitt

    Read original paper ↗ ·

  6. Periodic Trends in Actinide Phosphonates: Divergence and Convergence between Thorium, Uranium, Neptunium, and Plutonium Systems

    Inorganic Chemistry · 2009-04-06

    Anna‐Gay D. Nelson, Travis H. Bray, Forrest A. Stanley, Thomas E. Albrecht‐Schmitt

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  7. Hydrothermal Synthesis and Crystal Structures of Actinide Compounds

    Springer eBooks · 2010-01-01

    Wolfgang Runde, Mary P. Neu

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  8. USING PHOSPHONATES TO PROBE STRUCTURAL DIFFERENCES BETWEEN TRANSURANIUM ELEMENTS AND THEIR PROPOSED SURROGATES

    Comments on Inorganic Chemistry · 2010-03-30

    Juan Diwu, Anna‐Gay D. Nelson, Thomas E. Albrecht‐Schmitt

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  9. Cerium(IV), Neptunium(IV), and Plutonium(IV) 1,2-Phenylenediphosphonates: Correlations and Differences between Early Transuranium Elements and Their Proposed Surrogates

    Inorganic Chemistry · 2010-10-04

    Juan Diwu, Shuao Wang, Zuolei Liao, Peter Carman Burns, Thomas E. Albrecht‐Schmitt

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  10. Recent progress in actinide borate chemistry

    Chemical Communications · 2011-01-01

    Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  11. Role of Anions and Reaction Conditions in the Preparation of Uranium(VI), Neptunium(VI), and Plutonium(VI) Borates

    Inorganic Chemistry · 2011-02-03

    Shuao Wang, Eric M. Villa, Juan Diwu, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  12. Facile Routes to ThIV, UIV, and NpIV Phosphites and Phosphates

    European Journal of Inorganic Chemistry · 2011-08-05

    Eric M. Villa, Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  13. Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) Phosphates

    Inorganic Chemistry · 2012-05-30

    Eric M. Villa, Connor J. Marr, Laurent J. Jouffret, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  14. Incorporation of Neptunium(VI) into a Uranyl Selenite

    Inorganic Chemistry · 2012-10-02

    Nathan A. Meredith, Matthew J. Polinski, Jian Hung Lin, Antonio Simonetti, Thomas E. Albrecht‐Schmitt

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  15. Structural changes within the alkaline earth uranyl phosphites

    Dalton Transactions · 2013-01-01

    Eric M. Villa, Juan Diwu, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  16. From Order to Disorder and Back Again: In Situ Hydrothermal Redox Reactions of Uranium Phosphites and Phosphates

    Inorganic Chemistry · 2013-01-09

    Eric M. Villa, Connor J. Marr, Juan Diwu, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  17. Syntheses, Structures, and Comparisons of Thallium Uranium Phosphites, Mixed Phosphate-Phosphites, and Phosphate

    Crystal Growth & Design · 2013-03-08

    Eric M. Villa, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  18. In[IO3](OH)2 – New member of hydrous and anhydrous iodate family with indium

    Solid State Sciences · 2014-06-12

    Elena L. Belokoneva, Olga V. Dimitrova, Anatoly S. Volkov

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  19. Expansion of the Rich Structures and Magnetic Properties of Neptunium Selenites: Soft Ferromagnetism in Np(SeO3)2

    Inorganic Chemistry · 2014-06-25

    Kariem Diefenbach, Jian Hung Lin, Justin N. Cross, Naresh S. Dalal, Michael Shatruk, Thomas E. Albrecht‐Schmitt

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  20. Monomers, Dimers, and Helices: Complexities of Cerium and Plutonium Phenanthrolinecarboxylates

    Inorganic Chemistry · 2016-04-12

    Samantha K. Cary, Maryline G. Ferrier, Ryan Baumbach, Mark A. Silver, Juan S. Lezama-Pacheco, Stosh A. Kozimor, Henry S. La Pierre, Benjamin William Stein, Alexandra A. Arico, Danielle L. Gray, Thomas E. Albrecht‐Schmitt

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  21. Systematic Investigation of the in Situ Reduction Process from U(VI) to U(IV) in a Phosphonate System under Mild Solvothermal Conditions

    Inorganic Chemistry · 2017-05-26

    Lanhua Chen, Juan Diwu, Daxiang Gui, Yaxing Wang, Zhehui Weng, Zhifang Chai, Thomas E. Albrecht‐Schmitt, Shuao Wang

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  22. Electronic Structure and Properties of Berkelium Iodates

    Journal of the American Chemical Society · 2017-08-17

    Mark A. Silver, Samantha K. Cary, Alejandro J. Garza, Ryan Baumbach, Alexandra A. Arico, Gregory A. Galmin, Kuan-Wen Chen, Jason A. Johnson, Jamie C. Wang, Ronald Jene Clark, Alexander T. Chemey, Teresa M. Eaton, Matthew L. Marsh, Kevin Seidler, Shane S. Galley, Lambertus J. van de Burgt, Ashley L. Gray, David E. Hobart, Kenneth Hanson, Shelley M. Van Cleve, Frédéric Gendron, Jochen Autschbach, Gustavo E. Scuseria, Laurent Maron, Manfred Speldrich, Paul Kögerler, Cristian Celis‐Barros, Dayán Páez‐Hernández, Ramiro Arratia‐Pérez, Michael Ruf, Thomas E. Albrecht‐Schmitt

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  23. Mild Periodic Acid Flux and Hydrothermal Methods for the Synthesis of Crystalline f-Element-Bearing Iodate Compounds

    Inorganic Chemistry · 2017-10-09

    Yaxing Wang, Tao Duan, Zhehui Weng, Jie Ling, Xuemiao Yin, Lanhua Chen, Daopeng Sheng, Juan Diwu, Zhifang Chai, Ning Liu, Shuao Wang

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  24. Unexpected Behavior of Np in Oxo-selenate/Oxo-selenite Systems

    Inorganic Chemistry · 2018-01-22

    Eike M. Langer, Olaf Walter, Jean‐Yves Colle, Dirk Bosbach, Evgeny V. Alekseev

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  25. Synthesis, structure and characterization of M(IO 3 ) 2 (HIO 3 ) (M = Ca, Sr) as new anhydrous alkaline earth metal bis-iodate hydrogeniodate compounds

    Dalton Transactions · 2019-01-01

    Yawen An, Yang Zhong, Tongqing Sun, Haijun Wang, Zhenpeng Hu, Hongde Liu, Shiguo Liu, Yongfa Kong, Jingjun Xu

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  26. The first actinide polyiodate: a complex multifunctional compound with promising X-ray luminescence properties and proton conductivity

    Chemical Communications · 2020-12-17

    Gabriel L. Murphy, Yaxing Wang, Philip Kegler, Yumin Wang, Shuao Wang, Evgeny V. Alekseev

    Read original paper ↗ ·

  27. Natural and Anthropogenic Analogues for High-Level Nuclear Waste Disposal Repositories: A Review

    The Canadian Mineralogist · 2021-01-01

    Mostafa Fayek, Julie J. Brown

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  28. The crystal and coordination chemistry of neptunium in all its oxidation states: An expanded structural hierarchy of neptunium compounds

    Coordination Chemistry Reviews · 2021-06-05

    Sara E. Gilson, Peter Carman Burns

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  29. Samarium Hydrogen Iodate, Sm(IO3)3·HIO3: Synthesis and Characterization

    Journal of Structural Chemistry · 2024-10-01

    Oksana P. Grigorieva, Т. Б. Шаталова, Peter S. Berdonosov, Dmitri O. Charkin, A.A. Gippius, A. V. Tkachev, Е. А. Кравченко, В. А. Долгих, Konstantin Alexandrovich Lyssenko

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