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RESEARCH PAPER · Angewandte Chemie International Edition · 2005

Actinide Materials Adopt Curvature: Nanotubules and Nanospheres

Thomas E. Albrecht‐Schmitt

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Actinide Materials Adopt Curvature: Nanotubules and NanospheresOriginalNanostructures in Uranium Oxocompounds1Actinide Materials Adopt Curvature: Nanotubules and Nanospheres0Oxoneptunium(v) as part of the framework of a polyoxometalate35The vitality of uranium molecular chemistry at the dawn of the XXIst century314Extended networks, porous sheets, and chiral frameworks. Thorium materials containing mixed geometry anions: Structures and properties of Th(SeO3)(SeO4), Th(IO3)2(SeO4)(H2O)3·H2O, and Th(CrO4)(IO3)244Syntheses, spectroscopic and X-ray structure analyses of two dioxouranium (VI) complexes: supramolecular framework built from O—H…O, C—H…O and stacking interactions11Topology of inorganic complexes as a function of amine molecular structure in layered uranyl selenates37Na2Li8[(UO2)11O12(WO5)2]: Three Different Uranyl‐Ion Coordination Geometries and Cation–Cation Interactions71Na2Li8[(UO2)11O12(WO5)2]: Three Different Uranyl‐Ion Coordination Geometries and Cation–Cation Interactions17Nanostructured actinide compounds36Actinyl chemistry at the Centre for Radiochemistry Research7Nanostructured actinide compounds: an introduction3An Ordered Assembly of Filled Nanoscale Tubules of Europium Seleno-silicate in the Crystal Structure of a Quaternary Compound17Charge-density matching in organic–inorganic uranyl compounds25Self‐Assembly of Polyoxo Clusters and Extended Frameworks by Controlled Hydrolysis of Low‐Valent Uranium101Self‐Assembly of Polyoxo Clusters and Extended Frameworks by Controlled Hydrolysis of Low‐Valent Uranium30One-Dimensional Array of Two- and Three-Center Cation−Cation Bonds in the Structure of Li4[(UO2)10O10(Mo2O8)]63One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands32A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds90A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds11Crystal Chemistry of Selenates with Mineral-Like Structures: V. Crystal Structures of (H 3 O) 2 ((UO 2 )(SeO 4 ) 2 (H 2 O))(H 2 O) 2 and (H 3 O) 2 ((UO 2 )(SeO 4 ) 2 (H 2 O))(H 2 O), New Compounds0Synthesis of uranium oxide nanoparticles and their catalytic performance for benzyl alcohol conversion to benzaldehyde77Synthesis, structure, and characterization of a new thorium–organic framework material, Th3F5[(C10H14)(CH2CO2)2]3(NO3)53The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies26TOF-2: A Large 1D Channel Thorium Organic Framework140Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif31Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif9Crystal chemistry of selenates with mineral-like structures: V. Crystal structures of (H3O)2[(UO2)(SeO4)2(H2O)](H2O)2 and (H3O)2[(UO2)(SeO4)2(H2O)](H2O), new compounds with rhomboclase and goldichite topology8Amine-templated uranyl selenates with chiral [(UO2)2(SeO4)3(H2O)]2– layers: topology, isomerism, structural relationships31Stable Pentavalent Uranyl Species and Selective Assembly of a Polymetallic Mixed‐Valent Uranyl Complex by Cation–Cation Interactions114Stable Pentavalent Uranyl Species and Selective Assembly of a Polymetallic Mixed‐Valent Uranyl Complex by Cation–Cation Interactions32Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?18Cubic and rhombohedral heterobimetallic networks constructed from uranium, transition metals, and phosphonoacetate: new methods for constructing porous materials113Crystal Chemistry of the Potassium and Rubidium Uranyl Borate Families Derived from Boric Acid Fluxes49Synthesis, Structure, and Solid-State Transformation Studies of Phosphonoacetate Based Hybrid Compounds of Uranium and Thorium48Differential Ion Exchange in Elliptical Uranyl Diphosphonate Nanotubules106Differential Ion Exchange in Elliptical Uranyl Diphosphonate Nanotubules9Advances in actinide solid-state and coordination chemistry37Morphology controlled uranium oxide hydroxide hydrate for catalysis, luminescence and SERS studies43Exploring the Uranyl Organometallic Chemistry: From Single to Double Uranium−Carbon Bonds135Metal-Controlled Assembly of Uranyl Diphosphonates toward the Design of Functional Uranyl Nanotubules77Synthesis and structure of a new uranyl selenate complex with 1-butylamine [CH3(CH2)3NH3](H5O2)[(UO2)2(SeO4)3(H2O)]6Copper uranyl phosphate and arsenate incorporating an organic ligand with a pillared layer structure: [Cu(4,4′-bpy)(UO2)0.5(HPO4)(H2PO4)]·H2O and [Cu(4,4′-bpy)(UO2)0.5(HAsO4)(H2AsO4)]·1.5H2O15Nanoscale Hemispheres in Novel Mixed-Valent Uranyl Chromate(V,VI), (C3NH10)10[(UO2)13(Cr125+O42)(Cr6+O4)6(H2O)6](H2O)618Na1.515EuGeS4, A Three-Dimensional Crystalline Assembly of Empty Nanotubules Constructed with Europium(II/III) Mixed Valence Ions18Hybrid Uranyl Arsonate Coordination Nanocages18Reactivity of U3+ Metallocene Allyl Complexes Leads to a Nanometer-Sized Uranium Carbonate, [(C5Me5)2U]6(μ-κ1:κ2-CO3)623MOFs of Uranium and the Actinides95Truncated trigonal prismatic tubular crystals consisting of a zeolite L-mimic metal–organic framework17A Highly Adjustable Coordination System: Nanotubular and Molecular Cage Species in Uranyl Ion Complexes with Kemp’s Triacid46Increasing Complexity in the Uranyl Ion–Kemp’s Triacid System: From One- and Two-Dimensional Polymers to Uranyl–Copper(II) Dodeca- and Hexadecanuclear Species47Uranyl Ion Complexes with all-cis-1,3,5-Cyclohexanetricarboxylate: Unexpected Framework and Nanotubular Assemblies55Template‐Free Synthesis and Mechanistic Study of Porous Three‐Dimensional Hierarchical Uranium‐Containing and Uranium Oxide Microspheres26Design and synthesis of a chiral uranium-based microporous metal organic framework with high SHG efficiency and sequestration potential for low-valent actinides58Uranyl peroxide clusters stabilized by dicarboxylate ligands: A pentagonal ring and a dimer with extensive uranyl–cation interactions9Silver Ion-Mediated Heterometallic Three-Fold Interpenetrating Uranyl–Organic Framework52Inorganic Synthesis of Actinides3Microporous uranyl chromates successively formed by evaporation from acidic solution9The Propensity of Uranium-Peroxide Systems to Preserve Nanosized Assemblies20Uranyl Sulfate Nanotubules Templated by N-phenylglycine16Supramolecular and Macrocyclic Chemistry of the Actinides2Specific Features of the Crystal Chemistry of Layered Uranyl Compounds with the Ratio UO2: TO4 = 5 : 8 (T = S6+, Cr6+, Se6+, Mo6+)9Structural Snapshots of Cluster Growth from {U6} to {U38} During the Hydrolysis of UCl439Structural Snapshots of Cluster Growth from {U6} to {U38} During the Hydrolysis of UCl46Utilizing Autoxidation of Solvents To Promote the Formation of Uranyl Peroxide Materials16Hybrid Uranyl–Phosphonate Coordination Nanocage8Syntheses and crystal structures of two uranyl peroxide nanoclusters with a diphosphonate linker ligand2Successive Crystallization of Organically Templated Uranyl Sulfates: Synthesis and Crystal Structures of [pyH](H3O)[(UO2)3(SO4)4(H2O)2], [pyH]2[(UO2)6(SO4)7(H2O)], and [pyH]2[(UO2)2(SO4)3]3Actinide Coordination Chemistry on Surfaces: Synthesis, Manipulation, and Properties of Thorium Bis(porphyrinato) Complexes17Results of 25-Year Studies of Uranium Compounds at the Department of Crystallography of St. Petersburg State University3Uranyl Nanotubules and Nanospheres: Inspired by Curvature in Phosphonates and Arsonates0

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  1. Nanostructures in Uranium Oxocompounds

    MRS Proceedings · 2005-01-01

    Sergey V. Krivovichev, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  2. Actinide Materials Adopt Curvature: Nanotubules and Nanospheres

    ChemInform · 2005-09-13

    Thomas E. Albrecht‐Schmitt

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  3. Oxoneptunium(v) as part of the framework of a polyoxometalate

    Chemical Communications · 2006-01-01

    Roy Copping, Andrew J. Gaunt, Iain May, Clint A. Sharrad, David Collison, M. Helliwell, O. Danny Fox, Chris J. Jones

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  4. The vitality of uranium molecular chemistry at the dawn of the XXIst century

    Dalton Transactions · 2006-01-01

    M. Ephritikhine

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  5. Extended networks, porous sheets, and chiral frameworks. Thorium materials containing mixed geometry anions: Structures and properties of Th(SeO3)(SeO4), Th(IO3)2(SeO4)(H2O)3·H2O, and Th(CrO4)(IO3)2

    Journal of Solid State Chemistry · 2006-02-08

    Tyler A. Sullens, Philip M. Almond, Jessica A. Byrd, James V. Beitz, Travis H. Bray, Thomas E. Albrecht‐Schmitt

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  6. Syntheses, spectroscopic and X-ray structure analyses of two dioxouranium (VI) complexes: supramolecular framework built from O—H…O, C—H…O and stacking interactions

    Zeitschrift für Kristallographie - Crystalline Materials · 2006-07-01

    Santu Chakraborty, Subhajit Dinda, Ramgopal Bhattacharyya, Alok K. Mukherjee

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  7. Topology of inorganic complexes as a function of amine molecular structure in layered uranyl selenates

    Doklady Physical Chemistry · 2006-08-01

    Sergey V. Krivovichev, В. В. Гуржий, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  8. Na2Li8[(UO2)11O12(WO5)2]: Three Different Uranyl‐Ion Coordination Geometries and Cation–Cation Interactions

    Angewandte Chemie International Edition · 2006-09-15

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier, Oleg I. Siidra, Karsten Knorr, Evgeny V. Suleimanov, Evgeny V. Chuprunov

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  9. Na2Li8[(UO2)11O12(WO5)2]: Three Different Uranyl‐Ion Coordination Geometries and Cation–Cation Interactions

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    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier, Oleg I. Siidra, Karsten Knorr, Evgeny V. Suleimanov, Evgeny V. Chuprunov

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  10. Nanostructured actinide compounds

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  11. Actinyl chemistry at the Centre for Radiochemistry Research

    Journal of Alloys and Compounds · 2006-12-05

    Iain May, Roy Copping, S.M. Cornet, Caytie E. Talbot-Eeckelaers, Andrew J. Gaunt, Gordon H. John, M.P. Redmond, Clint A. Sharrad, Andrew D. Sutton, David Collison, O. Danny Fox, Chris J. Jones, Mark J. Sarsfield, Robin J. Taylor

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  12. Nanostructured actinide compounds: an introduction

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    Sergey V. Krivovichev, Peter Carman Burns, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  13. An Ordered Assembly of Filled Nanoscale Tubules of Europium Seleno-silicate in the Crystal Structure of a Quaternary Compound

    Journal of the American Chemical Society · 2007-07-11

    Amitava Choudhury, Peter K. Dorhout

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  14. Charge-density matching in organic–inorganic uranyl compounds

    Comptes Rendus Chimie · 2007-07-16

    Sergey V. Krivovichev, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  15. Self‐Assembly of Polyoxo Clusters and Extended Frameworks by Controlled Hydrolysis of Low‐Valent Uranium

    Angewandte Chemie International Edition · 2007-08-25

    Grégory Nocton, Fabien Burdet, Jacques Pécaut, Marinella Mazzanti

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  16. Self‐Assembly of Polyoxo Clusters and Extended Frameworks by Controlled Hydrolysis of Low‐Valent Uranium

    Angewandte Chemie · 2007-08-25

    Grégory Nocton, Fabien Burdet, Jacques Pécaut, Marinella Mazzanti

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  17. One-Dimensional Array of Two- and Three-Center Cation−Cation Bonds in the Structure of Li4[(UO2)10O10(Mo2O8)]

    Inorganic Chemistry · 2007-09-11

    Evgeny V. Alekseev, Sergey V. Krivovichev, Thomas Malcherek, Wulf Depmeier

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  18. One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands

    Inorganic Chemistry · 2007-11-01

    Yaqin Yu, Wei Zhan, Thomas E. Albrecht‐Schmitt

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  19. A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds

    Angewandte Chemie International Edition · 2007-12-03

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

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  20. A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds

    Angewandte Chemie · 2007-12-03

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

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  21. Crystal Chemistry of Selenates with Mineral-Like Structures: V. Crystal Structures of (H 3 O) 2 ((UO 2 )(SeO 4 ) 2 (H 2 O))(H 2 O) 2 and (H 3 O) 2 ((UO 2 )(SeO 4 ) 2 (H 2 O))(H 2 O), New Compounds

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  22. Synthesis of uranium oxide nanoparticles and their catalytic performance for benzyl alcohol conversion to benzaldehyde

    Journal of Materials Chemistry · 2008-01-01

    Qun Wang, Guodong Li, Shuang Xu, Jixue Li, Jie‐Sheng Chen

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  23. Synthesis, structure, and characterization of a new thorium–organic framework material, Th3F5[(C10H14)(CH2CO2)2]3(NO3)

    Dalton Transactions · 2008-01-01

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  24. The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies

    Chemistry of Materials · 2008-01-01

    Yu-Lun Lai, Ray‐Kuang Chiang, Kwang‐Hwa Lii, Sue‐Lein Wang

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  25. TOF-2: A Large 1D Channel Thorium Organic Framework

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    Kang Min Ok, Jaeyoung Sung, Gang Hu, Robert M. J. Jacobs, Dermot M. O'Hare

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  26. Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif

    Angewandte Chemie International Edition · 2008-06-23

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  27. Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif

    Angewandte Chemie · 2008-06-23

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  28. Crystal chemistry of selenates with mineral-like structures: V. Crystal structures of (H3O)2[(UO2)(SeO4)2(H2O)](H2O)2 and (H3O)2[(UO2)(SeO4)2(H2O)](H2O), new compounds with rhomboclase and goldichite topology

    Geology of Ore Deposits · 2008-12-01

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  29. Amine-templated uranyl selenates with chiral [(UO2)2(SeO4)3(H2O)]2– layers: topology, isomerism, structural relationships

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  30. Stable Pentavalent Uranyl Species and Selective Assembly of a Polymetallic Mixed‐Valent Uranyl Complex by Cation–Cation Interactions

    Angewandte Chemie International Edition · 2009-09-08

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  31. Stable Pentavalent Uranyl Species and Selective Assembly of a Polymetallic Mixed‐Valent Uranyl Complex by Cation–Cation Interactions

    Angewandte Chemie · 2009-09-08

    Victor Mougel, Paweł Horeglad, Grégory Nocton, Jacques Pécaut, Marinella Mazzanti

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  32. Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?

    Inorganic Chemistry · 2009-10-30

    Jie Ling, Shijun Wu, Fanrong Chen, Antonio Simonetti, J. T. Shafer, Thomas E. Albrecht‐Schmitt

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  33. Cubic and rhombohedral heterobimetallic networks constructed from uranium, transition metals, and phosphonoacetate: new methods for constructing porous materials

    Chemical Communications · 2010-01-01

    A.N. Alsobrook, Brad G. Hauser, Joseph T. Hupp, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  34. Crystal Chemistry of the Potassium and Rubidium Uranyl Borate Families Derived from Boric Acid Fluxes

    Inorganic Chemistry · 2010-06-18

    Shuao Wang, Evgeny V. Alekseev, Jared T. Stritzinger, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  35. Synthesis, Structure, and Solid-State Transformation Studies of Phosphonoacetate Based Hybrid Compounds of Uranium and Thorium

    Inorganic Chemistry · 2010-07-27

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  36. Differential Ion Exchange in Elliptical Uranyl Diphosphonate Nanotubules

    Angewandte Chemie International Edition · 2010-10-12

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  37. Differential Ion Exchange in Elliptical Uranyl Diphosphonate Nanotubules

    Angewandte Chemie · 2010-10-12

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  38. Advances in actinide solid-state and coordination chemistry

    MRS Bulletin · 2010-11-01

    Peter Carman Burns, Yasuhisa Ikeda, Ken Czerwinski

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  39. Morphology controlled uranium oxide hydroxide hydrate for catalysis, luminescence and SERS studies

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  40. Exploring the Uranyl Organometallic Chemistry: From Single to Double Uranium−Carbon Bonds

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  41. Metal-Controlled Assembly of Uranyl Diphosphonates toward the Design of Functional Uranyl Nanotubules

    Inorganic Chemistry · 2011-11-03

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  42. Synthesis and structure of a new uranyl selenate complex with 1-butylamine [CH3(CH2)3NH3](H5O2)[(UO2)2(SeO4)3(H2O)]

    Russian Journal of General Chemistry · 2012-01-01

    Vladislav V. Gurzhiy, Pavel A. Mikhaylenko, Sergey V. Krivovichev, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  43. Copper uranyl phosphate and arsenate incorporating an organic ligand with a pillared layer structure: [Cu(4,4′-bpy)(UO2)0.5(HPO4)(H2PO4)]·H2O and [Cu(4,4′-bpy)(UO2)0.5(HAsO4)(H2AsO4)]·1.5H2O

    Journal of Solid State Chemistry · 2012-08-20

    Chih-Min Wang, Kwang‐Hwa Lii

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  44. Nanoscale Hemispheres in Novel Mixed-Valent Uranyl Chromate(V,VI), (C3NH10)10[(UO2)13(Cr125+O42)(Cr6+O4)6(H2O)6](H2O)6

    Inorganic Chemistry · 2012-08-20

    Oleg I. Siidra, Еvgeny V. Nazarchuk, Anatoly A. Petrunin, Roman A. Kayukov, Sergey V. Krivovichev

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  45. Na1.515EuGeS4, A Three-Dimensional Crystalline Assembly of Empty Nanotubules Constructed with Europium(II/III) Mixed Valence Ions

    Inorganic Chemistry · 2012-10-16

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  46. Hybrid Uranyl Arsonate Coordination Nanocages

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  47. Reactivity of U3+ Metallocene Allyl Complexes Leads to a Nanometer-Sized Uranium Carbonate, [(C5Me5)2U]6(μ-κ1:κ2-CO3)6

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  48. MOFs of Uranium and the Actinides

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  49. Truncated trigonal prismatic tubular crystals consisting of a zeolite L-mimic metal–organic framework

    Chemical Communications · 2014-01-01

    Tae Hwan Noh, Jaeseong Jang, Woosik Hong, Haeri Lee, Ok‐Sang Jung

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  50. A Highly Adjustable Coordination System: Nanotubular and Molecular Cage Species in Uranyl Ion Complexes with Kemp’s Triacid

    Crystal Growth & Design · 2014-02-11

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