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RESEARCH PAPER · Angewandte Chemie International Edition · 2007

Self‐Assembly of Polyoxo Clusters and Extended Frameworks by Controlled Hydrolysis of Low‐Valent Uranium

Grégory Nocton, Fabien Burdet, Jacques Pécaut, Marinella Mazzanti

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Self‐Assembly of Polyoxo Clusters and Extended Frameworks by Controlled Hydrolysis of Low‐Valent UraniumOriginalThe actinides0A Nitrido‐Centered Uranium Azido Cluster Obtained from a Uranium Azide119A Nitrido‐Centered Uranium Azido Cluster Obtained from a Uranium Azide23Mixed Valency in a Uranium Multimetallic Complex58Mixed Valency in a Uranium Multimetallic Complex12Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif31Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif91,4‐Dicyanobenzene as a Scaffold for the Preparation of Bimetallic Actinide Complexes Exhibiting Metal–Metal Communication54Pentavalent Uranium Oxide via Reduction of [UO 2 ] 2+ Under Hydrothermal Reaction Conditions †83Polyimido Clusters of Neodymium and Uranium, Including a Cluster with an M6(μ3‐N)8 Core35Magnetic Exchange Coupling in Actinide-Containing Molecules129Stable Pentavalent Uranyl Species and Selective Assembly of a Polymetallic Mixed‐Valent Uranyl Complex by Cation–Cation Interactions114Stable Pentavalent Uranyl Species and Selective Assembly of a Polymetallic Mixed‐Valent Uranyl Complex by Cation–Cation Interactions32First Hexanuclear U IV and Th IV Formate Complexes – Structure and Stability Range in Aqueous Solution134Hydration and Hydrolysis of Thorium(IV) in Aqueous Solution and the Structures of Two Crystalline Thorium(IV) Hydrates131Ligand assisted cleavage of uranium oxo-clusters46New insights into the acid mediated disproportionation of pentavalent uranyl71Comparative Study of f-Element Electronic Structure across a Series of Multimetallic Actinide and Lanthanoid-Actinide Complexes Possessing Redox-Active Bridging Ligands58Tetranuclear Uranium Clusters by Reductive Cleavage of 3,5‐Dimethylpyrazolate20Tetranuclear Uranium Clusters by Reductive Cleavage of 3,5‐Dimethylpyrazolate6Actinyl Compounds with Hexavalent Elements (S, Cr, Se, Mo) – Structural Diversity, Nanoscale Chemistry, and Cellular Automata Modeling69Formation of Uranium(IV) Oxide Clusters from Uranocene [U(η8-C8H8)2] and Uranyl [UO2X2] Compounds38Nanoscale Chemistry of Uranyl Selenates1Base‐Driven Assembly of Large Uranium Oxo/Hydroxo Clusters78Base‐Driven Assembly of Large Uranium Oxo/Hydroxo Clusters22Rapid Self-Assembly of Uranyl Polyhedra into Crown Clusters69Hydration, Solvation and Hydrolysis of Multicharged Metal Ions4Thorium(IV) Molecular Clusters with a Hexanuclear Th Core154[U(TpMe2)2(bipy)]+: A Cationic Uranium(III) Complex with Single-Molecule-Magnet Behavior123Metal–Organic-Framework-Type 1D-Channel Open Network of a Tetravalent Uranium Trimesate56Synthesis and Characterization of a Novel Tetranuclear 5f Compound: A New Synthon for Exploring U(IV) Chemistry34New polynuclear U( iv )–U( v ) complexes from U( iv ) mediated uranyl( v ) disproportionation71Time-Resolved Self-Assembly of a Fullerene-Topology Core–Shell Cluster Containing 68 Uranyl Polyhedra59Structure and stability range of a hexanuclear Th(iv)–glycine complex83Uranyl peroxide pyrophosphate cage clusters with oxalate and nitrate bridges27Formation of Soluble Hexanuclear Neptunium(IV) Nanoclusters in Aqueous Solution: Growth Termination of Actinide(IV) Hydrous Oxides by Carboxylates75Thorium(IV)–Selenate Clusters Containing an Octanuclear Th(IV) Hydroxide/Oxide Core76Periodic Trends in Hexanuclear Actinide Clusters42Uranyl Heteropolyoxometalate: Synthesis, Structure, and Spectroscopic Properties37Relativistic Density Functional Study on Uranium(IV) and Thorium(IV) Oxide Clusters of Zonohedral Geometry13Synthesis of a Uranyl Persulfide Complex and Quantum Chemical Studies of Formation and Topologies of Hypothetical Uranyl Persulfide Cage Clusters25The coordination and organometallic chemistry of UI3 and U{N(SiMe3)2}3: Synthetic reagents par excellence40Clusters of Actinides with Oxide, Peroxide, or Hydroxide Bridges344Solution and Solid-State Structural Chemistry of Actinide Hydrates and Their Hydrolysis and Condensation Products372Recent Developments in Synthesis and Structural Chemistry of Nonaqueous Actinide Complexes323Sulfonate Complexes of Actinide Ions: Structural Diversity in Uranyl Complexes with 2-Sulfobenzoate71Time-Resolved Assembly of Chiral Uranyl Peroxo Cage Clusters Containing Belts of Polyhedra35Emission spectroscopy of uranium(iv) compounds: a combined synthetic, spectroscopic and computational study66Fingerprinting the oxidation state of U(iv) by emission spectroscopy15Three‐Dimensional MOF‐Type Architectures with Tetravalent Uranium Hexanuclear Motifs (U6O8)127Mixed Formate-Dicarboxylate Coordination Polymers with Tetravalent Uranium: Occurrence of Tetranuclear {U4O4} and Hexanuclear {U6O4(OH)4} Motifs66The crystal chemistry of uranium carboxylates394Crystal Structure and Solution Species of Ce(III) and Ce(IV) Formates: From Mononuclear to Hexanuclear Complexes104Isolation of the Large {Actinide}38 Poly-oxo Cluster with Uranium94Well-defined molecular uranium( iii ) chloride complexes29Redox and environmentally relevant aspects of actinide(IV) coordination chemistry113Cation–cation interactions and cation exchange in a series of isostructural framework uranyl tungstates17Activation of Small Molecules by Molecular Uranium Complexes119Two‐Electron Reductive Carbonylation of Terminal Uranium(V) and Uranium(VI) Nitrides to Cyanate by Carbon Monoxide104Coordination polymers of uranium( iv ) terephthalates42Centrosymmetric and chiral porous thorium organic frameworks exhibiting uncommon thorium coordination environments45Thorium Terephthalates Coordination Polymers Synthesized in Solvothermal DMF/H2O System143Ex‐Situ Kinetic Investigations of the Formation of the Poly‐Oxo Cluster U3827Comparative study of the lanthanide (Ln) and actinide (An) triflate complexes M(OTf) n1Metal Oxido Clusters of Group 13–15 Elements18Oxo Clusters of 5f Elements24First Evidence of a Water‐Soluble Plutonium(IV) Hexanuclear Cluster37Two actinide-organic frameworks constructed by a tripodal flexible ligand: Occurrence of infinite {(UO2)O2(OH)3}4n and hexanuclear {Th6O4(OH)4} motifs14The Key Role of U 28 in the Aqueous Self‐Assembly of Uranyl Peroxide Nanocages49Isolation of a Star‐Shaped Uranium(V/VI) Cluster from the Anaerobic Photochemical Reduction of Uranyl(VI)29Isolation of a Star‐Shaped Uranium(V/VI) Cluster from the Anaerobic Photochemical Reduction of Uranyl(VI)11Solution Species and Crystal Structure of Zr(IV) Acetate96Synthesis of Coordination Polymers of Tetravalent Actinides (Uranium and Neptunium) with a Phthalate or Mellitate Ligand in an Aqueous Medium34Coordination of Tetravalent Actinides (An=ThIV, UIV, NpIV, PuIV) with DOTA: From Dimers to Hexamers72Network Dimensionality of Selected Uranyl(VI) Coordination Polymers and Octopus-like Uranium(IV) Clusters16Synthèse et étude cristallochimique de carboxylates d'actinides tétravalents (Th, U, Np) : polymères de coordination et entités moléculaires à haute nucléarité0{Np 38 } clusters: the missing link in the largest poly-oxo cluster series of tetravalent actinides40Captivation with encapsulation: a dozen years of exploring uranyl peroxide capsules95Formation of a new type of uranium( iv ) poly-oxo cluster {U 38 } based on a controlled release of water via esterification reaction44One-dimensional chain structures of hexanuclear uranium( iv ) clusters bridged by formate ligands9Small molecule activation with divalent samarium triflate: a synergistic effort to cleave O 221In Situ Reduction from Uranyl Ion into a Tetravalent Uranium Trimer and Hexamer Featuring Ion-Exchange Properties and the Alexandrite Effect16Synthèse d’assemblages multimétalliques de lanthanides : des propriétés électroniques des précurseurs divalents au contrôle de leur réactivité0Mixed-valent neptunium oligomer complexes based on cation–cation interactions4Time-controlled synthesis of the 3D coordination polymer U(1,2,3-Hbtc) 2 followed by the formation of molecular poly-oxo cluster {U 14 } containing hemimellitate uranium( iv )14Structural Snapshots of Cluster Growth from {U6} to {U38} During the Hydrolysis of UCl439Structural Snapshots of Cluster Growth from {U6} to {U38} During the Hydrolysis of UCl46Extension of the Plutonium Oxide Nanocluster Family to Include {Pu16} and {Pu22}43Structural properties of ultra-small thorium and uranium dioxide nanoparticles embedded in a covalent organic framework45Mononuclear to Polynuclear UIV Structural Units: Effects of Reaction Conditions on U‐Furoate Phase Formation23Crystal Chemistry and Structural Complexity of Uranium(IV) Sulfates: Synthesis of U3H2(SO4)7(H2O)5·3H2O and U3(UO2)0.2(SO4)6(OH)0.4·2.3H2O with Framework Structures by the Photochemical Reduction of Uranyl8Beyond structural motifs: the frontier of actinide-containing metal–organic frameworks65Intrinsic Semiconducting Behavior in a Large Mixed‐Valent Uranium(V/VI) Cluster64Intrinsic Semiconducting Behavior in a Large Mixed‐Valent Uranium(V/VI) Cluster4Effect of Background Electrolyte Composition on the Interfacial Formation of Th(IV) Nanoparticles on the Muscovite (001) Basal Plane8Electronic structure studies reveal 4f/5d mixing and its effect on bonding characteristics in Ce-imido and -oxo complexes33Characterization of a Hexanuclear Plutonium(IV) Nanostructure in an Acetate Solution via Visible–Near Infrared Absorption Spectroscopy, Extended X-ray Absorption Fine Structure Spectroscopy, and Density Functional Theory15Structural evolution and stability of plutonium oxide clusters2Crystallographic Evidence for Formation of M 6 O 8 /M 6 O 9 f-Element Clusters in Hydrolysis Reactions6M6O8 metal oxo clusters: A key structural motif across the periodic table8Mechanism‐Guided Precision Hydrolysis of Early Transition Metals to Access (Mixed‐Metal) Oxo Clusters1

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  1. The actinides

    Annual Reports Section A (Inorganic Chemistry) · 2008-01-01

    S. A. Cotton

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  2. A Nitrido‐Centered Uranium Azido Cluster Obtained from a Uranium Azide

    Angewandte Chemie International Edition · 2008-03-10

    Grégory Nocton, Jacques Pécaut, Marinella Mazzanti

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  3. A Nitrido‐Centered Uranium Azido Cluster Obtained from a Uranium Azide

    Angewandte Chemie · 2008-03-10

    Grégory Nocton, Jacques Pécaut, Marinella Mazzanti

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  4. Mixed Valency in a Uranium Multimetallic Complex

    Angewandte Chemie International Edition · 2008-03-12

    Eric J. Schelter, Ruilian Wu, Brian L. Scott, Joe D. Thompson, David E. Morris, Jaqueline L. Kiplinger

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  5. Mixed Valency in a Uranium Multimetallic Complex

    Angewandte Chemie · 2008-03-12

    Eric J. Schelter, Ruilian Wu, Brian L. Scott, Joe D. Thompson, David E. Morris, Jaqueline L. Kiplinger

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  6. Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif

    Angewandte Chemie International Edition · 2008-06-23

    J.‐C. Berthet, P. Thuéry, M. Ephritikhine

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  7. Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif

    Angewandte Chemie · 2008-06-23

    J.‐C. Berthet, P. Thuéry, M. Ephritikhine

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  8. 1,4‐Dicyanobenzene as a Scaffold for the Preparation of Bimetallic Actinide Complexes Exhibiting Metal–Metal Communication

    Chemistry - A European Journal · 2008-08-07

    Eric J. Schelter, Jacqueline M. Veauthier, Christopher R. Graves, Kevin D. John, Brian L. Scott, Joe D. Thompson, Jaime A. Pool, David E. Morris, Jaqueline L. Kiplinger

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  9. Pentavalent Uranium Oxide via Reduction of [UO 2 ] 2+ Under Hydrothermal Reaction Conditions †

    Inorganic Chemistry · 2008-10-09

    Nebebech Belai, M. Frisch, Eugene S. Ilton, Bruce Ravel, Christopher L. Cahill

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  10. Polyimido Clusters of Neodymium and Uranium, Including a Cluster with an M6(μ3‐N)8 Core

    European Journal of Inorganic Chemistry · 2008-11-04

    J.‐C. Berthet, P. Thuéry, M. Ephritikhine

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  11. Magnetic Exchange Coupling in Actinide-Containing Molecules

    Inorganic Chemistry · 2009-04-13

    Jeffrey D. Rinehart, T. David Harris, Stosh A. Kozimor, Bart M. Bartlett, Jeffrey R. Long

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  12. Stable Pentavalent Uranyl Species and Selective Assembly of a Polymetallic Mixed‐Valent Uranyl Complex by Cation–Cation Interactions

    Angewandte Chemie International Edition · 2009-09-08

    Victor Mougel, Paweł Horeglad, Grégory Nocton, Jacques Pécaut, Marinella Mazzanti

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  13. Stable Pentavalent Uranyl Species and Selective Assembly of a Polymetallic Mixed‐Valent Uranyl Complex by Cation–Cation Interactions

    Angewandte Chemie · 2009-09-08

    Victor Mougel, Paweł Horeglad, Grégory Nocton, Jacques Pécaut, Marinella Mazzanti

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  14. First Hexanuclear U IV and Th IV Formate Complexes – Structure and Stability Range in Aqueous Solution

    European Journal of Inorganic Chemistry · 2009-10-10

    Shinobu Takao, Koichiro Takao, Werner Kraus, Franziska Emmerling, Andreas C. Scheinost, Gert Bernhard, Christoph Hennig

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  15. Hydration and Hydrolysis of Thorium(IV) in Aqueous Solution and the Structures of Two Crystalline Thorium(IV) Hydrates

    Inorganic Chemistry · 2009-11-18

    Natallia Torapava, Ingmar Persson, Lars Eriksson, Daniel Lundberg

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  16. Ligand assisted cleavage of uranium oxo-clusters

    Chemical Communications · 2010-01-01

    Grégory Nocton, Jacques Pécaut, Yaroslav E. Filinchuk, Marinella Mazzanti

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  17. New insights into the acid mediated disproportionation of pentavalent uranyl

    Chemical Communications · 2010-01-01

    Victor Mougel, Biplab Biswas, Jacques Pécaut, Marinella Mazzanti

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  18. Comparative Study of f-Element Electronic Structure across a Series of Multimetallic Actinide and Lanthanoid-Actinide Complexes Possessing Redox-Active Bridging Ligands

    Inorganic Chemistry · 2010-01-20

    Eric J. Schelter, Ruilian Wu, Jacqueline M. Veauthier, Eric D. Bauer, Corwin H. Booth, Robert K. Thomson, Christopher R. Graves, Kevin D. John, Brian L. Scott, Joe D. Thompson, David E. Morris, Jaqueline L. Kiplinger

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  19. Tetranuclear Uranium Clusters by Reductive Cleavage of 3,5‐Dimethylpyrazolate

    Angewandte Chemie International Edition · 2010-03-02

    Jeffrey D. Rinehart, Stosh A. Kozimor, Jeffrey R. Long

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  20. Tetranuclear Uranium Clusters by Reductive Cleavage of 3,5‐Dimethylpyrazolate

    Angewandte Chemie · 2010-03-02

    Jeffrey D. Rinehart, Stosh A. Kozimor, Jeffrey R. Long

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  21. Actinyl Compounds with Hexavalent Elements (S, Cr, Se, Mo) – Structural Diversity, Nanoscale Chemistry, and Cellular Automata Modeling

    European Journal of Inorganic Chemistry · 2010-05-25

    Sergey V. Krivovichev

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  22. Formation of Uranium(IV) Oxide Clusters from Uranocene [U(η8-C8H8)2] and Uranyl [UO2X2] Compounds

    Inorganic Chemistry · 2010-07-26

    J.‐C. Berthet, P. Thuéry, M. Ephritikhine

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  23. Nanoscale Chemistry of Uranyl Selenates

    Springer eBooks · 2011-01-01

    Sergey V. Krivovichev, Vladislav V. Gurzhiy, Ivan Gundarovich Tananaev, Boris F. Myasoedov

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  24. Base‐Driven Assembly of Large Uranium Oxo/Hydroxo Clusters

    Angewandte Chemie International Edition · 2011-05-12

    Biplab Biswas, Victor Mougel, Jacques Pécaut, Marinella Mazzanti

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  25. Base‐Driven Assembly of Large Uranium Oxo/Hydroxo Clusters

    Angewandte Chemie · 2011-05-12

    Biplab Biswas, Victor Mougel, Jacques Pécaut, Marinella Mazzanti

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  26. Rapid Self-Assembly of Uranyl Polyhedra into Crown Clusters

    Journal of the American Chemical Society · 2011-05-24

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  27. Hydration, Solvation and Hydrolysis of Multicharged Metal Ions

    Epsilon Open Archive (Sveriges lantbruksuniversitet biblioteket (Swedish University of Agricultural Sciences)) · 2011-08-26

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  28. Thorium(IV) Molecular Clusters with a Hexanuclear Th Core

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  29. [U(TpMe2)2(bipy)]+: A Cationic Uranium(III) Complex with Single-Molecule-Magnet Behavior

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  30. Metal–Organic-Framework-Type 1D-Channel Open Network of a Tetravalent Uranium Trimesate

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  31. Synthesis and Characterization of a Novel Tetranuclear 5f Compound: A New Synthon for Exploring U(IV) Chemistry

    Inorganic Chemistry · 2011-10-28

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  32. New polynuclear U( iv )–U( v ) complexes from U( iv ) mediated uranyl( v ) disproportionation

    Chemical Communications · 2011-11-18

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  33. Time-Resolved Self-Assembly of a Fullerene-Topology Core–Shell Cluster Containing 68 Uranyl Polyhedra

    Journal of the American Chemical Society · 2011-12-21

    Jie Qiu, Jie Ling, Audrey Sui, Jennifer E. S. Szymanowski, Antonio Simonetti, Peter Carman Burns

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  34. Structure and stability range of a hexanuclear Th(iv)–glycine complex

    Dalton Transactions · 2012-01-01

    Christoph Hennig, Shinobu Takao, Koichiro Takao, Stephan Weiß, Werner Kraus, Franziska Emmerling, Andreas C. Scheinost

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  35. Uranyl peroxide pyrophosphate cage clusters with oxalate and nitrate bridges

    Dalton Transactions · 2012-01-01

    Jie Ling, Michael P. Ozga, Megan Stoffer, Peter Carman Burns

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  36. Formation of Soluble Hexanuclear Neptunium(IV) Nanoclusters in Aqueous Solution: Growth Termination of Actinide(IV) Hydrous Oxides by Carboxylates

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  37. Thorium(IV)–Selenate Clusters Containing an Octanuclear Th(IV) Hydroxide/Oxide Core

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  38. Periodic Trends in Hexanuclear Actinide Clusters

    Inorganic Chemistry · 2012-03-21

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  39. Uranyl Heteropolyoxometalate: Synthesis, Structure, and Spectroscopic Properties

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  40. Relativistic Density Functional Study on Uranium(IV) and Thorium(IV) Oxide Clusters of Zonohedral Geometry

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  41. Synthesis of a Uranyl Persulfide Complex and Quantum Chemical Studies of Formation and Topologies of Hypothetical Uranyl Persulfide Cage Clusters

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  42. The coordination and organometallic chemistry of UI3 and U{N(SiMe3)2}3: Synthetic reagents par excellence

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  43. Clusters of Actinides with Oxide, Peroxide, or Hydroxide Bridges

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  44. Solution and Solid-State Structural Chemistry of Actinide Hydrates and Their Hydrolysis and Condensation Products

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  45. Recent Developments in Synthesis and Structural Chemistry of Nonaqueous Actinide Complexes

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  46. Sulfonate Complexes of Actinide Ions: Structural Diversity in Uranyl Complexes with 2-Sulfobenzoate

    Inorganic Chemistry · 2012-12-07

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  47. Time-Resolved Assembly of Chiral Uranyl Peroxo Cage Clusters Containing Belts of Polyhedra

    Inorganic Chemistry · 2012-12-11

    Jie Qiu, Kévin Nguyen, Laurent J. Jouffret, Jennifer E. S. Szymanowski, Peter Carman Burns

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  48. Emission spectroscopy of uranium(iv) compounds: a combined synthetic, spectroscopic and computational study

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  49. Fingerprinting the oxidation state of U(iv) by emission spectroscopy

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  50. Three‐Dimensional MOF‐Type Architectures with Tetravalent Uranium Hexanuclear Motifs (U6O8)

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