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RESEARCH PAPER · Inorganic Chemistry · 2015

Synthesis and Characterization of Mid-Infrared Transparency Compounds: Acentric BaHgS2 and Centric Ba8Hg4S5Se7

Kui Wu, Xin Su, Shilie Pan, Zhihua Yang

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Synthesis and Characterization of Mid-Infrared Transparency Compounds: Acentric BaHgS2 and Centric Ba8Hg4S5Se7OriginalChemInform Abstract: Synthesis and Characterization of Mid‐Infrared Transparency Compounds: Acentric BaHgS2 and Centric Ba8Hg4S5Se7.0BaCdSnS 4 and Ba 3 CdSn 2 S 8 : syntheses, structures, and non-linear optical and photoluminescence properties97Crystal and electronic structures, and photoluminescence and photocatalytic properties of α-EuZrS 326Rb 2 SeOCl 4 ·H 2 O: a polar material among the alkali metal selenite halides with a strong SHG response18The structure and band gap design of high Si doping level Ag1−xGa1−xSixSe2 (x=1/2)15Na 2 Hg 3 M 2 S 8 (M = Si, Ge, and Sn): New Infrared Nonlinear Optical Materials with Strong Second Harmonic Generation Effects and High Laser-Damage Thresholds186Trigonal Planar [HgSe3]4– Unit: A New Kind of Basic Functional Group in IR Nonlinear Optical Materials with Large Susceptibility and Physicochemical Stability196Na 2 ZnGe 2 S 6 : A New Infrared Nonlinear Optical Material with Good Balance between Large Second-Harmonic Generation Response and High Laser Damage Threshold302Recent achievements on middle and far-infrared second-order nonlinear optical materials433Ba 6 Li 2 CdSn 4 S 16 : lithium substitution simultaneously enhances band gap and SHG intensity44Band gap tuning from an indirect EuGa 2 S 4 to a direct EuZnGeS 4 semiconductor: syntheses, crystal and electronic structures, and optical properties20Syntheses and characterization of three new sulfides with large band gaps: acentric Ba 4 Ga 4 SnS 12 , centric Ba 12 Sn 4 S 23 and Ba 7 Sn 3 S 1327Mid-Infrared Nonlinear Optical Materials Based on Metal Chalcogenides: Structure–Property Relationship338BaAu2S2: A Au-Based Intrinsic Photocatalyst for High-Performance Visible-Light Photocatalysis17Li2HgMS4 (M = Si, Ge, Sn): New Quaternary Diamond-Like Semiconductors for Infrared Laser Frequency Conversion64Spin-polarized Second Harmonic Generation from the Antiferromagnetic CaCoSO Single Crystal148Na2ZnSn2S6: A mixed-metal thiostannate with large second-harmonic generation response activated by penta-tetrahedral [ZnSn4S14]10− clusters10Hg-Based Infrared Nonlinear Optical Material KHg4Ga5Se12 Exhibits Good Phase-Matchability and Exceptional Second Harmonic Generation Response101Na 6 Zn 3 MIII2Q 9 (M III = Ga, In; Q = S, Se): four new supertetrahedron-layered chalcogenides with unprecedented vertex-sharing T 3 -clusters and desirable photoluminescence performances31Structural insights into T 2 -cluster-containing chalcogenides with vertex-, edge- and face-sharing connection modes of NaQ 6 ligands: Na 3 ZnM III Q 4 (M III = In, Ga; Q = S, Se)13From AgGaS2 to Li2ZnSiS4: Realizing Impressive High Laser Damage Threshold Together with Large Second-Harmonic Generation Response134Quaternary sulfide Ba5Cd2Ga2S10 containing chains of edge- and corner-sharing tetrahedra16Intriguing Structural Transition Inducing Variable Birefringences in ABa2MS4Cl (A = Rb, Cs; M = Ge, Sn)32Adjustable optical nonlinearity in d 10 cations containing chalcogenides via dp hybridization interaction13Investigation on two new antimony-based quaternary chalcogenides: Na 6 CdSb 4 S 10 and Na 3 CdSbSe 41Structural modulation induced by M IIIA metals in Ba 3 MQ 4 X (M = Al, Ga, In; Q = S, Se; X = Cl, Br): an experimental and computational analysis7[Ge2S5(S2)]4−, A NLO‐Active Unit Leading to an Asymmetric Structure Discovered in Li2Cs4Ge2S5(S2)Cl2: An Experimental and Theoretical study18Highly Polarizable Hg2+ Induced a Strong Second Harmonic Generation Signal and Large Birefringence in LiHgPO4265A highly distorted HgS 4 tetrahedron-induced moderate second-harmonic generation response of EuHgGeS 462Ba 6 In 6 Zn 4 Se 19 : a high performance infrared nonlinear optical crystal with [InSe 3 ] 3− trigonal planar functional motifs22New quaternary chalcogenide Ba 4 HgAs 2 S 10 originating from the combination of linear [HgS 2 ] 2− and tetrahedral [AsS 4 ] 3− modules8LiBa4Ga5Q12 (Q = S, Se): Noncentrosymmetric Metal Chalcogenides with a Cesium Chloride Topological Structure Displaying a Remarkable Laser Damage Threshold32Mild solvothermal syntheses and characterizations of four quaternary layered sulfides AAgCdS2 (A = K, Rb, Cs) and Cs2Cu2Cd2S413EuHgGeSe 4 and EuHgSnS 4 : Two Quaternary Eu-Based Infrared Nonlinear Optical Materials with Strong Second-Harmonic-Generation Responses55Intriguing Dimensional Transition Inducing Variable Birefringence in K2Na2Sn3S8 and Rb3NaSn3Se828Design and synthesis of Ba 3 SiSe 5 with suitable birefringence modulated via M IV atoms in the Ba–M IV –Q (M IV = Si, Ge; Q = S, Se) system3Temperature controlling valance changes of crystalline thioarsenates and thioantimonates21Transition-metal-based chalcogenides: A rich source of infrared nonlinear optical materials184Helical {[HgS]} n Chain-Induced Balanced Nonlinear-Optical Performance for Trigonal Mercury Sulfide29Hg-based chalcogenides: An intriguing class of infrared nonlinear optical materials128Achieving a strong second harmonic generation response and a wide band gap in a Hg-based material41Ba 2 HgTe 5 : a Hg-based telluride with giant birefringence induced by linear [HgTe 2 ] units17Ba 3 HgGa 2 S 7 : A Zero-Dimensional Quaternary Sulfide Featuring a Unique [Hg 2 Ga 4 S 14 ] 12– String and Exhibiting a High Photocurrent Response27Growth, Structure, and Dielectric and Optics Properties of a Novel Optical Crystal with High Optical Nonlinearity19HgB2S4: A d10 Metal Thioborate with Giant Birefringence and Wide Band Gap31NaMn3Ga3S8: Noncentrosymmetric inorganic metal chalcogenide with nonlinear optical response, antiferromagnetic, and photoluminescence performances13Design of Pentanary Mixed-Chalcogenides Ag2In2SiS6–xSex (x = 1, 2) Based on the Bucket Effect: Local Structural Difference and High-Performance Nonlinear-Optical Properties Realized by Partial Congener Substitution5Sr2HgGe2OS6: A Hg-Based Oxychalcogenide Infrared Nonlinear Optical Material Exhibiting Favorable Balance between a Large Band Gap and Strong Second Harmonic Generation Response10From Orthorhombic Cu8GeS6 to Cubic Cu6HgGeS6: Second-Harmonic Generation and Photocurrent Responses7Mild solvothermal syntheses, crystal structures, characterizations and properties of four ternary alkaline earth metal sulfides1Ba-based IR nonlinear optical materials: synthesis, growth, structures, and properties6From KBa 4 Ge 3 S 10 Cl to ABa 3 EuGe 3 S 11 (A = Na, K) Synthesized by Reactive Flux Assisted Metal Oxide-Boron-Chalcogen (MOBQ) Method: Effect of Cation/Anion Cosubstitution on Crystal Structure and Nonlinear Optical Properties0

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  1. ChemInform Abstract: Synthesis and Characterization of Mid‐Infrared Transparency Compounds: Acentric BaHgS2 and Centric Ba8Hg4S5Se7.

    ChemInform · 2015-05-15

    Kui Wu, Xin Su, Shilie Pan, Zhihua Yang

    Read original paper ↗ ·

  2. BaCdSnS 4 and Ba 3 CdSn 2 S 8 : syntheses, structures, and non-linear optical and photoluminescence properties

    Dalton Transactions · 2016-01-01

    Ni Zhen, Kui Wu, Ying Wang, Qiang Li, Wenhui Gao, Dianwei Hou, Zhihua Yang, Huaidong Jiang, Yongjun Dong, Shilie Pan

    Read original paper ↗ ·

  3. Crystal and electronic structures, and photoluminescence and photocatalytic properties of α-EuZrS 3

    New Journal of Chemistry · 2016-01-01

    Sheng‐Ping Guo, Yang Chi, Jian‐Ping Zou, Huaiguo Xue

    Read original paper ↗ ·

  4. Rb 2 SeOCl 4 ·H 2 O: a polar material among the alkali metal selenite halides with a strong SHG response

    Dalton Transactions · 2016-01-01

    Qi Wu, Hongming Liu, Lei Kang, Zheshuai Lin, Xiang‐Gao Meng, Xingguo Chen, Jingui Qin

    Read original paper ↗ ·

  5. The structure and band gap design of high Si doping level Ag1−xGa1−xSixSe2 (x=1/2)

    Journal of Solid State Chemistry · 2016-03-04

    Shiyan Zhang, Dajiang Mei, Xin Du, Zheshuai Lin, Junbo Zhong, Yuandong Wu, Jingli Xu

    Read original paper ↗ ·

  6. Na 2 Hg 3 M 2 S 8 (M = Si, Ge, and Sn): New Infrared Nonlinear Optical Materials with Strong Second Harmonic Generation Effects and High Laser-Damage Thresholds

    Chemistry of Materials · 2016-04-05

    Kui Wu, Zhihua Yang, Shilie Pan

    Read original paper ↗ ·

  7. Trigonal Planar [HgSe3]4– Unit: A New Kind of Basic Functional Group in IR Nonlinear Optical Materials with Large Susceptibility and Physicochemical Stability

    Journal of the American Chemical Society · 2016-05-03

    Chao Li, Wenlong Yin, Pifu Gong, Xiaoshuang Li, Molin Zhou, A. Mar, Zheshuai Lin, Jiyong Yao, Yicheng Wu, Chuangtian Chen

    Read original paper ↗ ·

  8. Na 2 ZnGe 2 S 6 : A New Infrared Nonlinear Optical Material with Good Balance between Large Second-Harmonic Generation Response and High Laser Damage Threshold

    Journal of the American Chemical Society · 2016-05-19

    Guangmao Li, Kui Wu, Qiong Liu, Zhihua Yang, Shilie Pan

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  9. Recent achievements on middle and far-infrared second-order nonlinear optical materials

    Coordination Chemistry Reviews · 2016-12-27

    Sheng‐Ping Guo, Yang Chi, Guo‐Cong Guo

    Read original paper ↗ ·

  10. Ba 6 Li 2 CdSn 4 S 16 : lithium substitution simultaneously enhances band gap and SHG intensity

    Journal of Materials Chemistry C · 2017-01-01

    Ruihuan Duan, Pengfei Liu, Hua Lin, Yi‐Wen Zheng, Ju‐Song Yu, Xin‐Tao Wu, Shangxiong Huangfu, Ling Chen

    Read original paper ↗ ·

  11. Band gap tuning from an indirect EuGa 2 S 4 to a direct EuZnGeS 4 semiconductor: syntheses, crystal and electronic structures, and optical properties

    RSC Advances · 2017-01-01

    Yang Chi, Sheng‐Ping Guo, Huaiguo Xue

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  12. Syntheses and characterization of three new sulfides with large band gaps: acentric Ba 4 Ga 4 SnS 12 , centric Ba 12 Sn 4 S 23 and Ba 7 Sn 3 S 13

    Dalton Transactions · 2017-01-01

    Ruihuan Duan, Pengfei Liu, Hua Lin, Shangxiong Huangfu, Li‐Ming Wu

    Read original paper ↗ ·

  13. Mid-Infrared Nonlinear Optical Materials Based on Metal Chalcogenides: Structure–Property Relationship

    Crystal Growth & Design · 2017-03-15

    Fei Liang, Lei Kang, Zheshuai Lin, Yicheng Wu

    Read original paper ↗ ·

  14. BaAu2S2: A Au-Based Intrinsic Photocatalyst for High-Performance Visible-Light Photocatalysis

    Inorganic Chemistry · 2017-04-12

    Molin Zhou, Xin Jiang, Xingxing Jiang, Ke Xiao, Yangwu Guo, Hongwei Huang, Zheshuai Lin, Jiyong Yao, Chen‐Ho Tung, Li‐Zhu Wu, Yicheng Wu

    Read original paper ↗ ·

  15. Li2HgMS4 (M = Si, Ge, Sn): New Quaternary Diamond-Like Semiconductors for Infrared Laser Frequency Conversion

    Crystals · 2017-04-12

    Kui Wu, Shilie Pan

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  16. Spin-polarized Second Harmonic Generation from the Antiferromagnetic CaCoSO Single Crystal

    Scientific Reports · 2017-04-13

    A.H. Reshak

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  17. Na2ZnSn2S6: A mixed-metal thiostannate with large second-harmonic generation response activated by penta-tetrahedral [ZnSn4S14]10− clusters

    Science China Technological Sciences · 2017-05-12

    Guangmao Li, Kui Wu, Qiong Liu, Zhihua Yang, Shilie Pan

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  18. Hg-Based Infrared Nonlinear Optical Material KHg4Ga5Se12 Exhibits Good Phase-Matchability and Exceptional Second Harmonic Generation Response

    Chemistry of Materials · 2017-08-29

    Molin Zhou, Yi Jin Yang, Yangwu Guo, Zheshuai Lin, Jiyong Yao, Yicheng Wu, Chuangtian Chen

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  19. Na 6 Zn 3 MIII2Q 9 (M III = Ga, In; Q = S, Se): four new supertetrahedron-layered chalcogenides with unprecedented vertex-sharing T 3 -clusters and desirable photoluminescence performances

    Inorganic Chemistry Frontiers · 2018-01-01

    Ailijiang Abudurusuli, Kui Wu, Yilimiranmu Rouzhahong, Zhihua Yang, Shilie Pan

    Read original paper ↗ ·

  20. Structural insights into T 2 -cluster-containing chalcogenides with vertex-, edge- and face-sharing connection modes of NaQ 6 ligands: Na 3 ZnM III Q 4 (M III = In, Ga; Q = S, Se)

    Dalton Transactions · 2018-01-01

    Ruijiao Chen, Xiaowen Wu, Zhi Su

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  21. From AgGaS2 to Li2ZnSiS4: Realizing Impressive High Laser Damage Threshold Together with Large Second-Harmonic Generation Response

    Chemistry of Materials · 2018-01-17

    Guangmao Li, Yu Chu, Zhongxiang Zhou

    Read original paper ↗ ·

  22. Quaternary sulfide Ba5Cd2Ga2S10 containing chains of edge- and corner-sharing tetrahedra

    Journal of Alloys and Compounds · 2018-06-22

    Mingjing Tang, Abishek K. Iyer, Dong Zhang, Wenlong Yin, A. Mar

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  23. Intriguing Structural Transition Inducing Variable Birefringences in ABa2MS4Cl (A = Rb, Cs; M = Ge, Sn)

    Inorganic Chemistry · 2018-08-24

    Yu Chu, Kui Wu, Xin Su, Jian Wei Han, Zhihua Yang, Shilie Pan

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  24. Adjustable optical nonlinearity in d 10 cations containing chalcogenides via dp hybridization interaction

    Dalton Transactions · 2019-01-01

    Jianian Cheng, Bing‐Hua Lei, Chen Zhou, Shilie Pan, Zhihua Yang

    Read original paper ↗ ·

  25. Investigation on two new antimony-based quaternary chalcogenides: Na 6 CdSb 4 S 10 and Na 3 CdSbSe 4

    New Journal of Chemistry · 2019-01-01

    Yi Huang, Xiaowen Wu, Sadeh Beysen

    Read original paper ↗ ·

  26. Structural modulation induced by M IIIA metals in Ba 3 MQ 4 X (M = Al, Ga, In; Q = S, Se; X = Cl, Br): an experimental and computational analysis

    Dalton Transactions · 2019-01-01

    Abudukadi Tudi, Shujuan Han, Ailijiang Abudurusuli, Haohai Yu, Zhihua Yang, Shilie Pan

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  27. [Ge2S5(S2)]4−, A NLO‐Active Unit Leading to an Asymmetric Structure Discovered in Li2Cs4Ge2S5(S2)Cl2: An Experimental and Theoretical study

    Chemistry - A European Journal · 2019-03-06

    Guangmao Li, Kui Wu, Yi Huang, Zhihua Yang, Shilie Pan

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  28. Highly Polarizable Hg2+ Induced a Strong Second Harmonic Generation Signal and Large Birefringence in LiHgPO4

    Journal of the American Chemical Society · 2019-06-16

    Baolin Wu, Chun‐Li Hu, Fei‐Fei Mao, Ru‐Ling Tang, Jiang‐Gao Mao

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  29. A highly distorted HgS 4 tetrahedron-induced moderate second-harmonic generation response of EuHgGeS 4

    Inorganic Chemistry Frontiers · 2020-01-01

    Mei Yan, Zongdong Sun, Wen‐Dong Yao, Wenfeng Zhou, Wenlong Liu, Sheng‐Ping Guo

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  30. Ba 6 In 6 Zn 4 Se 19 : a high performance infrared nonlinear optical crystal with [InSe 3 ] 3− trigonal planar functional motifs

    Journal of Materials Chemistry C · 2020-01-01

    Anyi Zhou, Chensheng Lin, Bingxuan Li, Wen‐Dan Cheng, Zhengxiao Guo, Zhufeng Hou, Fang-Yu Yuan, Guoliang Chai

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  31. New quaternary chalcogenide Ba 4 HgAs 2 S 10 originating from the combination of linear [HgS 2 ] 2− and tetrahedral [AsS 4 ] 3− modules

    Dalton Transactions · 2020-01-01

    Wenhao Xing, Naizheng Wang, Zhuang Li, Wenhao Liu, Jian Tang, Wenlong Yin, Zheshuai Lin, Bin Kang, Jiyong Yao

    Read original paper ↗ ·

  32. LiBa4Ga5Q12 (Q = S, Se): Noncentrosymmetric Metal Chalcogenides with a Cesium Chloride Topological Structure Displaying a Remarkable Laser Damage Threshold

    Inorganic Chemistry · 2020-04-04

    Ailijiang Abudurusuli, Junjie Li, Tinghao Tong, Zhihua Yang, Shilie Pan

    Read original paper ↗ ·

  33. Mild solvothermal syntheses and characterizations of four quaternary layered sulfides AAgCdS2 (A = K, Rb, Cs) and Cs2Cu2Cd2S4

    Journal of Alloys and Compounds · 2020-07-23

    Yan Liu, Yanhua Li, Yongkang Guo, Yu Feng Sun, Xiao‐Yu Cao, Min Ji, Zhong‐Lu You, Yong‐Lin An

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  34. EuHgGeSe 4 and EuHgSnS 4 : Two Quaternary Eu-Based Infrared Nonlinear Optical Materials with Strong Second-Harmonic-Generation Responses

    Inorganic Chemistry · 2020-11-30

    Wenhao Xing, Chunlan Tang, Naizheng Wang, Chunxiao Li, Zhuang Li, Jieyun Wu, Zheshuai Lin, Jiyong Yao, Wenlong Yin, Bin Kang

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  35. Intriguing Dimensional Transition Inducing Variable Birefringence in K2Na2Sn3S8 and Rb3NaSn3Se8

    Inorganic Chemistry · 2020-12-23

    Xiao Ji, Hongping Wu, Bingbing Zhang, Hongwei Yu, Zhanggui Hu, Jiyang Wang, Yicheng Wu

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  36. Design and synthesis of Ba 3 SiSe 5 with suitable birefringence modulated via M IV atoms in the Ba–M IV –Q (M IV = Si, Ge; Q = S, Se) system

    Dalton Transactions · 2021-01-01

    Huanhuan Cheng, Abudukadi Tudi, Peng Wang, Kewang Zhang, Zhihua Yang, Shilie Pan

    Read original paper ↗ ·

  37. Temperature controlling valance changes of crystalline thioarsenates and thioantimonates

    Journal of Alloys and Compounds · 2021-03-26

    Yanhua Li, Xuedan Song, Yiping Zhong, Yongkang Guo, Min Ji, Zhong‐Lu You, Yong‐Lin An

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  38. Transition-metal-based chalcogenides: A rich source of infrared nonlinear optical materials

    Coordination Chemistry Reviews · 2021-08-26

    Hong Chen, Wenbo Wei, Hua Lin, Xintao Wu

    Read original paper ↗ ·

  39. Helical {[HgS]} n Chain-Induced Balanced Nonlinear-Optical Performance for Trigonal Mercury Sulfide

    Inorganic Chemistry · 2021-10-29

    Mei Yan, Wen‐Dong Yao, Wenlong Liu, Ru‐Ling Tang, Sheng‐Ping Guo

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  40. Hg-based chalcogenides: An intriguing class of infrared nonlinear optical materials

    Coordination Chemistry Reviews · 2021-12-09

    Chunxiao Li, Xianghe Meng, Zhuang Li, Jiyong Yao

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  41. Achieving a strong second harmonic generation response and a wide band gap in a Hg-based material

    Inorganic Chemistry Frontiers · 2022-01-01

    Yu-Jie Zhang, Hongping Wu, Zhanggui Hu, Jiyang Wang, Yicheng Wu, Hongwei Yu

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  42. Ba 2 HgTe 5 : a Hg-based telluride with giant birefringence induced by linear [HgTe 2 ] units

    Inorganic Chemistry Frontiers · 2022-01-01

    Mengran Sun, Jiyong Yao

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  43. Ba 3 HgGa 2 S 7 : A Zero-Dimensional Quaternary Sulfide Featuring a Unique [Hg 2 Ga 4 S 14 ] 12– String and Exhibiting a High Photocurrent Response

    Inorganic Chemistry · 2022-08-10

    Xiao Fen Huang, Sihan Yang, Wenlong Liu, Sheng‐Ping Guo

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  44. Growth, Structure, and Dielectric and Optics Properties of a Novel Optical Crystal with High Optical Nonlinearity

    Crystal Growth & Design · 2022-08-30

    Tianhua Wang, Jinkang Ma, Kai Xu, Rui Chen, Lifeng Cao, Bing Teng

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  45. HgB2S4: A d10 Metal Thioborate with Giant Birefringence and Wide Band Gap

    Chemistry of Materials · 2023-05-24

    Yi Huang, Yong an Zhang, Dongdong Chu, Zhihua Yang, Guangmao Li, Shilie Pan

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  46. NaMn3Ga3S8: Noncentrosymmetric inorganic metal chalcogenide with nonlinear optical response, antiferromagnetic, and photoluminescence performances

    Materials Today Chemistry · 2023-09-20

    Pengcheng Yang, Hongping Wu, Zhanggui Hu, Jiyang Wang, Yicheng Wu, Hongwei Yu

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  47. Design of Pentanary Mixed-Chalcogenides Ag2In2SiS6–xSex (x = 1, 2) Based on the Bucket Effect: Local Structural Difference and High-Performance Nonlinear-Optical Properties Realized by Partial Congener Substitution

    Inorganic Chemistry · 2024-04-16

    Mingyang Li, Jun Li, Wen‐Dong Yao, Nan Zhang, Haiping Xu, Wenfeng Zhou, Sheng‐Ping Guo

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  48. Sr2HgGe2OS6: A Hg-Based Oxychalcogenide Infrared Nonlinear Optical Material Exhibiting Favorable Balance between a Large Band Gap and Strong Second Harmonic Generation Response

    Inorganic Chemistry · 2024-05-23

    Guili Wang, Chunxiao Li, Ming‐Hsien Lee, Jiyong Yao

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  49. From Orthorhombic Cu8GeS6 to Cubic Cu6HgGeS6: Second-Harmonic Generation and Photocurrent Responses

    Inorganic Chemistry · 2025-04-24

    Qiu-Yang Du, Shanshan Han, Wen‐Dong Yao, Xu-Bin Ni, Wenfeng Zhou, Wenlong Liu, Sheng‐Ping Guo

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  50. Mild solvothermal syntheses, crystal structures, characterizations and properties of four ternary alkaline earth metal sulfides

    Inorganic Chemistry Communications · 2025-04-26

    Ruibing Wang, Yu Zhong, Yiheng Cao, Haitao Li, Haitao Li, Yan Liu, Yanhua Li, Yan Liu, Yanhua Li

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