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RESEARCH PAPER · Dalton Transactions · 2011

Synthesis, characterization and magnetic properties of four new organically templated metal sulfates [C5H14N2][MII(H2O)6](SO4)2, (MII = Mn, Fe, Co, Ni)

Fadhel Hajlaoui, Houcine Naı̈li, S. Yahyaoui, Mark M. Turnbull, Tahar Mhiri, Thierry Bataille B

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Synthesis, characterization and magnetic properties of four new organically templated metal sulfates [C5H14N2][MII(H2O)6](SO4)2, (MII = Mn, Fe, Co, Ni)OriginalNoncentrosymmetry in new 2-methylpiperazinediium hexaaquazinc(II) bis(sulfate)42-Dihydromethylpiperazinediium-M II (M II = Cu II , Fe II , Co II , Zn II ) double sulfates and their catalytic activity in diastereoselective nitroaldol (Henry) reaction49The structural transformation of monoclinic [(R)-C5H14N2][Cu(SO4)2(H2O)4]·2H2O into orthorhombic [(R)-C5H14N2]2[Cu(H2O)6](SO4)3: crystal structures and thermal behavior3A new organically templated magnesium sulfate: structure, spectroscopic analysis, and thermal behaviour7Encapsulation of a double-helical water–nitrate chain inside unique double helical chiral channels formed from Keggin POM and hexaquo-cobalt(II) units4Bis(4-aminopyridinium) hexaaquanickel(II) bis(sulfate)1The synthesis, structure and magnetic properties of two cobalt phosphonate salts2Inorganic layered structures in hybrid double sulfates: related phases and thermal reactivity13Crystal structure of 2-methylpiperazine-1,4-diium bis(hydrogen maleate)2Layered structure of a supramolecular hybrid sulfate salts: Thermal stability and magnetic behavior13Crystallisation, thermal analysis and acetal protection activity of new layered Zn( ii ) hybrid polymorphs7Synthesis, crystal structure and disorder–order phase transition of a new diamine templated metal sulfate, (C 3 H 12 N 2 ) 2 [Cu(H 2 O) 4 (SO 4 ) 2 ](HSO 4 ) 212Structural features, thermal behavior and biological activities of two new organically templated (CoII, NiII) sulfates12Reactions of metal salts with bronsted acidic ionic liquid: Formations of imidazole template metal sulfates or imidazole-metal complexes6Topological analysis of metal–ligand and hydrogen bonds in transition metal hybrid structures – A computational study5Synthesis, structural characterization, IR- and Raman spectroscopy, magnetic properties of new organically templated metal sulfates with 4-aminopyridinium20Structural characterization and physicochemical features of a new arsenate salt templated by mono and di-protonated 4-aminopyridine cations: (C 5 H 7 N 2 )(C 5 H 8 N 2 )[AsO 4 ]·H 2 O12Phase Transition Originating from Disorder–Order Transformation Coupled with Reorientation in the Organic–Inorganic Hybrid Compound (C4H14N2)[Cd2(H2O)6(SO4)3]7Thermal decomposition and biological activity of two supramolecular hybrid nitrates templated by piperazine5Investigations on (C6H9N2)2[MIIBr4] halogenometallate complexes with MII = Co, Cu and Zn: Crystal structure, thermal behavior and magnetic properties23Synthesis, structural determination and antimicrobial evaluation of two novel CoII and ZnII halogenometallates as efficient catalysts for the acetalization reaction of aldehydes22Crystal packing, vibrational studies, DFT calculations of a new hybrid nickel (II)‐complex and its application in Heck and Sonogashira cross‐ coupling reactions9Synthesis, characterization and temperature-triggered phase transition of organic-inorganic hybrid compound: (C6H18N2)(HSO4)211A new mononuclear nickel complex with 5,5′-dimethyl-2,2′-bipyridine: Synthesis, structural investigation and catalytic properties13Synthesis of L10 alloy nanoparticles. Potential and versatility of the pre-ordered Precursor Reduction strategy14Design, synthesis and physico-chemical studies of a Co(II)/Co(III) mixed-valence complex: An experimental and DFT approach25Synthesis, characterization and thermal properties of organic-inorganic hybrid layered materials based on metal sulfates and aromatic diamines: M(diamine)xSO4, (M = Fe, Co; x = 1, 2)1Physico-chemical characterizations and biological evaluation of a new semiconducting metal–organic compound based on pyrimidine frameworks8Co(II) and 2-amino-perimidinium based new generation hybrid material promoted facile dimerization of aroyl chloride: A route to α-diketone9Layered Co–O Cluster Applied to Photocatalytic CO2 Reduction3An original zero-dimensional material: 1, (2-aminoethyl) piperazinuim) tetrabromidomercurate (II) monohydrate, characterization and molecular docking3Exploring the white light emission properties and biological activities of a cobalt based mixed halide hybrid material3Synthesis, Structural, Magnetic, Optical, and Electronic Studies of a Novel Honeycomb Kagome Polyoxometalate‐Based Copper(II) Complex0Double sulfates with 1-methylpiperazinediium and divalent cations: Synthesis, structures, spectroscopic characterization, thermal stability, and topological features of (C5H14N2)[M(H2O)6](SO4)2∙H2O (M = Mg, Mn, Fe, Co, Ni, Zn, and Cd) and (C5H14N2)(SO4)∙H2O2Multifunctional hybrid nickel compound: Crystal engineering, semiconducting behavior, and dielectric performance0

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  1. Noncentrosymmetry in new 2-methylpiperazinediium hexaaquazinc(II) bis(sulfate)

    Journal of Coordination Chemistry · 2012-03-13

    Houcine Naı̈li

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  2. 2-Dihydromethylpiperazinediium-M II (M II = Cu II , Fe II , Co II , Zn II ) double sulfates and their catalytic activity in diastereoselective nitroaldol (Henry) reaction

    Dalton Transactions · 2012-09-19

    Houcine Naı̈li, Fadhel Hajlaoui, Tahar Mhiri, Tatiana C. O. Mac Leod, Maximilian N. Kopylovich, Kamran T. Mahmudov⧫, Armando J. L. Pombeiro

    Read original paper ↗ ·

  3. The structural transformation of monoclinic [(R)-C5H14N2][Cu(SO4)2(H2O)4]·2H2O into orthorhombic [(R)-C5H14N2]2[Cu(H2O)6](SO4)3: crystal structures and thermal behavior

    Phase Transitions · 2013-05-23

    Salem Saïd, Noureddine Mhadhbi, Fadhel Hajlaoui, S. Yahyaoui, Alexander J. Norquist, Tahar Mhiri, Thierry Bataille B, Houcine Naı̈li

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  4. A new organically templated magnesium sulfate: structure, spectroscopic analysis, and thermal behaviour

    Chemical Papers · 2013-06-21

    Dhouha Ben Hassan, Walid Rekik, Houcine Naı̈li, Tahar Mhiri

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  5. Encapsulation of a double-helical water–nitrate chain inside unique double helical chiral channels formed from Keggin POM and hexaquo-cobalt(II) units

    Polyhedron · 2013-11-01

    Rajarshi Chatterjee, Luna Paul, Dipak Kumar Hazra, Nabanita Pal, Atish Dipankar Jana, Monika Mukherjee, Mahammad Ali

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  6. Bis(4-aminopyridinium) hexaaquanickel(II) bis(sulfate)

    Acta Crystallographica Section E Structure Reports Online · 2013-12-06

    Thameur Sahbani, Wajda Smirani Sta, Mohamed Rzaigui A

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  7. The synthesis, structure and magnetic properties of two cobalt phosphonate salts

    Polyhedron · 2014-06-03

    Piotr Garczarek, Jan Janczak, Marek Duczmal, Jerzy Zoń

    Read original paper ↗ ·

  8. Inorganic layered structures in hybrid double sulfates: related phases and thermal reactivity

    New Journal of Chemistry · 2015-01-01

    Omar Kammoun, Walid Rekik, Houcine Naı̈li, Thierry Bataille B

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  9. Crystal structure of 2-methylpiperazine-1,4-diium bis(hydrogen maleate)

    Acta Crystallographica Section E Crystallographic Communications · 2015-02-20

    Intissar Wecharine, Arto Valkonen, Mohamed Rzaigui A, Wajda Smirani Sta

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  10. Layered structure of a supramolecular hybrid sulfate salts: Thermal stability and magnetic behavior

    Inorganica Chimica Acta · 2015-06-12

    Omar Kammoun, Houcine Naı̈li, Walid Rekik, Thierry Bataille B

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  11. Crystallisation, thermal analysis and acetal protection activity of new layered Zn( ii ) hybrid polymorphs

    CrystEngComm · 2016-01-01

    Salem Saïd, Houcine Naı̈li, Thierry Bataille B, Raquel P. Herrera

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  12. Synthesis, crystal structure and disorder–order phase transition of a new diamine templated metal sulfate, (C 3 H 12 N 2 ) 2 [Cu(H 2 O) 4 (SO 4 ) 2 ](HSO 4 ) 2

    CrystEngComm · 2016-01-01

    Chun‐Hong Chen, Rong Mu, Li Zhang, Guan‐Cheng Xu

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  13. Structural features, thermal behavior and biological activities of two new organically templated (CoII, NiII) sulfates

    Journal of Organometallic Chemistry · 2016-02-21

    Salem Saïd, Rihab Ben Abdallah Kolsi, Houcine Naı̈li

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  14. Reactions of metal salts with bronsted acidic ionic liquid: Formations of imidazole template metal sulfates or imidazole-metal complexes

    Inorganica Chimica Acta · 2016-03-26

    Qianqian Luo, Hechun Lin, Yuanyuan Zhang, Hui Peng

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  15. Topological analysis of metal–ligand and hydrogen bonds in transition metal hybrid structures – A computational study

    Polyhedron · 2016-05-10

    Subramaniam Kavitha, P. Deepa, Mylsamy Karthika, Ramasamy Kanakaraju

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  16. Synthesis, structural characterization, IR- and Raman spectroscopy, magnetic properties of new organically templated metal sulfates with 4-aminopyridinium

    Journal of Molecular Structure · 2016-05-11

    Tamara J. Bednarchuk, Vasyl Kinzhybalo, Oleksandr Bednarchuk, A. Pietraszko

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  17. Structural characterization and physicochemical features of a new arsenate salt templated by mono and di-protonated 4-aminopyridine cations: (C 5 H 7 N 2 )(C 5 H 8 N 2 )[AsO 4 ]·H 2 O

    Physica E Low-dimensional Systems and Nanostructures · 2016-11-28

    Noureddine Mhadhbi, Houcine Naı̈li, Khaled Jarraya

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  18. Phase Transition Originating from Disorder–Order Transformation Coupled with Reorientation in the Organic–Inorganic Hybrid Compound (C4H14N2)[Cd2(H2O)6(SO4)3]

    European Journal of Inorganic Chemistry · 2016-12-09

    Rong Mu, Chun‐Hong Chen, Li Zhang, Dianzeng Jia, Guan‐Cheng Xu

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  19. Thermal decomposition and biological activity of two supramolecular hybrid nitrates templated by piperazine

    Journal of Thermal Analysis and Calorimetry · 2016-12-29

    Dhouha Ben Hassan, Walid Rekik, Fedia Ben Mefteh, Houcine Naı̈li

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  20. Investigations on (C6H9N2)2[MIIBr4] halogenometallate complexes with MII = Co, Cu and Zn: Crystal structure, thermal behavior and magnetic properties

    Journal of Alloys and Compounds · 2017-07-29

    Souad Dgachi, Assila Maâtar Ben Salah, Mark M. Turnbull, Thierry Bataille B, Houcine Naı̈li

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  21. Synthesis, structural determination and antimicrobial evaluation of two novel CoII and ZnII halogenometallates as efficient catalysts for the acetalization reaction of aldehydes

    Chemistry Central Journal · 2018-02-28

    Assila Maâtar Ben Salah, Lilia Belghith‐Fendri, Thierry Bataille B, Raquel P. Herrera, Houcine Naı̈li

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  22. Crystal packing, vibrational studies, DFT calculations of a new hybrid nickel (II)‐complex and its application in Heck and Sonogashira cross‐ coupling reactions

    Applied Organometallic Chemistry · 2018-04-06

    Rim Jaballi, Wassim Maalej, Dhieb Atoui, Habib Feki, Ridha Ben Salem, Zakaria Elaoud

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  23. Synthesis, characterization and temperature-triggered phase transition of organic-inorganic hybrid compound: (C6H18N2)(HSO4)2

    Journal of Molecular Structure · 2018-08-20

    Ying-Ying Zhang, Chunhong Chen, Guan‐Cheng Xu, Wen‐Bo Xin

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  24. A new mononuclear nickel complex with 5,5′-dimethyl-2,2′-bipyridine: Synthesis, structural investigation and catalytic properties

    Journal of Molecular Structure · 2020-06-01

    Rim Jaballi, Dhieb Atoui, Wassim Maalej, Artem A. Babaryk, Patricia Horcajada, Ridha Ben Salem, Zakaria Elaoud

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  25. Synthesis of L10 alloy nanoparticles. Potential and versatility of the pre-ordered Precursor Reduction strategy

    Journal of Alloys and Compounds · 2020-07-06

    Gaspare Varvaro, Patrizia Imperatori, S. Laureti, Carla Cannas, Andrea Ardu, Paolo Plescia, Aldo Capobianchi

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  26. Design, synthesis and physico-chemical studies of a Co(II)/Co(III) mixed-valence complex: An experimental and DFT approach

    Journal of Molecular Structure · 2021-04-07

    Intissar Hamdi, Noureddine Mhadhbi, Noureddine Issaoui, Andreas Roodt, Mark M. Turnbull, Houcine Naı̈li

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  27. Synthesis, characterization and thermal properties of organic-inorganic hybrid layered materials based on metal sulfates and aromatic diamines: M(diamine)xSO4, (M = Fe, Co; x = 1, 2)

    Polyhedron · 2021-06-09

    A. González Guillén, Marcin Oszajca, Wiesław Łasocha

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  28. Physico-chemical characterizations and biological evaluation of a new semiconducting metal–organic compound based on pyrimidine frameworks

    Inorganic Chemistry Communications · 2022-03-07

    Wiem Jabeur, Marcus Korb, Jamelah Saleh Al-Otaibi, Erik Čižmár, Riadh Badraoui, Vladimı́r Zeleňák, Houcine Naı̈li

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  29. Co(II) and 2-amino-perimidinium based new generation hybrid material promoted facile dimerization of aroyl chloride: A route to α-diketone

    Journal of Molecular Structure · 2022-08-24

    Preethi Raja, Tapas Ghatak

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  30. Layered Co–O Cluster Applied to Photocatalytic CO2 Reduction

    Inorganic Chemistry · 2023-03-23

    Xin-Ying Xiang, Jiu-Lin Zhou, Qin Wang, Yin-Hua Zhu, Zhentao Zhang, Tian-Cheng Ye, Ji‐Lei Wang, Qiaoling Chen, Yan Xu

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  31. An original zero-dimensional material: 1, (2-aminoethyl) piperazinuim) tetrabromidomercurate (II) monohydrate, characterization and molecular docking

    Structural Chemistry · 2023-06-03

    Mouna Harzallah, Mouna Medimagh, Noureddine Issaoui, Werner Kaminsky, Brahim Ayed

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  32. Exploring the white light emission properties and biological activities of a cobalt based mixed halide hybrid material

    Inorganic Chemistry Communications · 2024-12-24

    Ameni Ben Nasr, Slim Elleuch, Olfa Majdoub, Mongi Saoudi, Hajir Wahbi, Fatma Aouaini, Beriham Ibrahim Basha, Walid Rekik, Houcine Naı̈li

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  33. Synthesis, Structural, Magnetic, Optical, and Electronic Studies of a Novel Honeycomb Kagome Polyoxometalate‐Based Copper(II) Complex

    European Journal of Inorganic Chemistry · 2025-08-22

    Y. Ammari, N. Baaalla, E.K. Hlil, Rachid Masrour, Sonia Abid

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  34. Double sulfates with 1-methylpiperazinediium and divalent cations: Synthesis, structures, spectroscopic characterization, thermal stability, and topological features of (C5H14N2)[M(H2O)6](SO4)2∙H2O (M = Mg, Mn, Fe, Co, Ni, Zn, and Cd) and (C5H14N2)(SO4)∙H2O

    Polyhedron · 2025-09-05

    Dmitri O. Charkin, Alevtina N. Gosteva, Vadim A. Kireev, A. M. Banaru, Dmitri N. Dmitriev, Dina V. Deyneko, Nikita Sergeyevich Tsvetov, Ivan Gundarovich Tananaev, Sergey M. Aksenov

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  35. Multifunctional hybrid nickel compound: Crystal engineering, semiconducting behavior, and dielectric performance

    Journal of Molecular Structure · 2026-03-11

    Rim Jaballi, Sawssan Jaballi, Wassim Maalej, Abderrazek Oueslati, Salih Salem Al-Juaid, Anouar Njeh, Zakaria Elaoud

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