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RESEARCH PAPER · The Canadian Mineralogist · 2008

NEPTUNYL COMPOUNDS: POLYHEDRON GEOMETRIES, BOND-VALENCE PARAMETERS, AND STRUCTURAL HIERARCHY

Tori Z. Forbes, C. Wallace, Peter Carman Burns

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NEPTUNYL COMPOUNDS: POLYHEDRON GEOMETRIES, BOND-VALENCE PARAMETERS, AND STRUCTURAL HIERARCHYOriginalQuaternary Neptunium Compounds: Syntheses and Characterization of KCuNpS3, RbCuNpS3, CsCuNpS3, KAgNpS3, and CsAgNpS322Further insights into intermediate- and mixed-valency in neptunium oxoanion compounds: structure and absorption spectroscopy of K2[(NpO2)3B10O16(OH)2(NO3)2]52Hydrothermal Synthesis and Crystal Structures of Actinide Compounds2Neptunium Diverges Sharply from Uranium and Plutonium in Crystalline Borate Matrixes: Insights into the Complex Behavior of the Early Actinides Relevant to Nuclear Waste Storage74Neptunium Diverges Sharply from Uranium and Plutonium in Crystalline Borate Matrixes: Insights into the Complex Behavior of the Early Actinides Relevant to Nuclear Waste Storage8Crystal and Electronic Structure of a Mixed-Valent Np(IV)−Np(V) Compound: [BuMeIm]5[Np(NpO2)3(H2O)6Cl12]30Incorporation of Neptunium(V) and Iodate into a Uranyl Phosphate: Implications for Mitigating the Release of 237Np and 129I in Repositories23From extended solids to nano-scale actinide clusters25Boronic Acid Flux Synthesis and Crystal Growth of Uranium and Neptunium Boronates and Borates: A Low-Temperature Route to the First Neptunium(V) Borate41Advances in actinide solid-state and coordination chemistry37Recent progress in actinide borate chemistry94Nanoscale uranium-based cage clusters inspired by uranium mineralogy88Role of Anions and Reaction Conditions in the Preparation of Uranium(VI), Neptunium(VI), and Plutonium(VI) Borates56U(VI) Uranyl Cation−Cation Interactions in Framework Germanates47Np-incorporation into uranyl phases: A quantum–mechanical evaluation22Cation–Cation Interactions: Crystal Structures of Neptunyl(V) Selenate Hydrates, (NpO2)2(SeO4)(H2O)n (n = 1, 2, and 4)36K(NpO2)3(H2O)Cl4: A Channel Structure Assembled by Two- and Three-Center Cation–Cation Interactions of Neptunyl Cations23Two New Neptunyl(V) Selenites: A Novel Cation–Cation Interaction Framework in (NpO2)3(OH)(SeO3)(H2O)2·H2O and a Uranophane-Type Sheet in Na(NpO2)(SeO3)(H2O)29New Neptunium(V) Borates That Exhibit the Alexandrite Effect20Stabilising pentavalent actinides—visible–near infrared and X-ray absorption spectroscopic studies of the utility of the [(Np 3 W 4 O 15 )(H 2 O) 3 (MW 9 O 33 ) 3 ] 18 − (M = Sb, Bi) structural type13Three New Sodium Neptunyl(V) Selenate Hydrates: Structures, Raman Spectroscopy, and Magnetism35Preparation, Stability, and Structural Characterization of Plutonium(VII) in Alkaline Aqueous Solution41(UO2)2[UO4(trz)2](OH)2: A U(VI) Coordination Intermediate between a Tetraoxido Core and a Uranyl Ion with Cation–Cation Interactions43Cation–Cation Interactions between Neptunyl(VI) Units24Mineralogic controls on aqueous neptunium(V) concentrations in silicate systems10One-Dimensional Uranyl-2,2′-bipyridine Coordination Polymer with Cation–Cation Interactions: (UO2)2(2,2′-bpy)(CH3CO2)(O)(OH)44Incorporation of Neptunium(VI) into a Uranyl Selenite14Clusters of Actinides with Oxide, Peroxide, or Hydroxide Bridges344Solution and Solid-State Structural Chemistry of Actinide Hydrates and Their Hydrolysis and Condensation Products372New Reactivity of the Uranyl(VI) Ion116Synthetic Influences on Neptunium Incorporation in Naturally Occurring Copper Uranyl Phosphates11Transuranium Inorganic Chemistry4Synthesis and Characterization of the First 2 D Neptunyl Structure Stabilized by Side‐on Cation–Cation Interactions23Mixed-Valent Neptunium(IV/V) Compound with Cation–Cation-Bound Six-Membered Neptunyl Rings24Crystal growth, structural characterization, cation–cation interaction classification, and optical properties of uranium( vi ) containing oxychlorides, A 4 U 5 O 16 Cl 2 (A = K, Rb), Cs 5 U 7 O 22 Cl 3 , and AUO 3 Cl (A = Rb, Cs)27Cation–cation interactions and cation exchange in a series of isostructural framework uranyl tungstates17Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials15Incorporation of Np(V) and U(VI) in carbonate and sulfate minerals crystallized from aqueous solution26Structural and Morphological Influences on Neptunium Incorporation in Uranyl Molybdates1A Revised and Expanded Structure Hierarchy of Natural and Synthetic Hexavalent Uranium Compounds172Oxo Clusters of 5f Elements24Effects of Titanium Doping in Titanomagnetite on Neptunium Sorption and Speciation19Three-Dimensional Network of Cation–Cation-Bound Neptunyl(V) Squares: Synthesis and in Situ Raman Spectroscopy Studies18Evaluation of f-element borate chemistry76A first principles study of energetics and electronic structural responses of uranium-based coordination polymers to Np incorporation5Synthesis and Study of the First Zeolitic Uranium Borate22A neptunium( v )-mediated interwoven transuranium-rotaxane network incorporating a mechanically interlocked [ c 2]daisy chain unit25Impacts of Oxo Interactions on Np(V) Crown Ether Complexes19Mixed-Valent Cyanoplatinates Featuring Neptunyl–Neptunyl Cation–Cation Interactions6Actinides: Crystallography0Rb2[Ca(NpO2)2(PO4)2], the First Mixed Alkali–Alkaline Earth Metals Neptunyl(V) Phosphate: Crystal Chemistry and Sheet Stereoisomerism7Actinyl-cation interactions: experimental and theoretical assessment of [Np( vi )O 2 Cl 4 ] 2− and [U( vi )O 2 Cl 4 ] 2− systems27Mixed-valent neptunium oligomer complexes based on cation–cation interactions4A Novel Family of Np(VI) Oxysalts: Crystal Structures, Calorimetry, Thermal Behavior, and Comparison with U(VI) Compounds9Structural Evolution in the Rare-Earth Uranyl Vanadates Ln2[(UO2)2V2O8]3·nH2O, Singularity of the Lanthanum Compound, and Single-Crystal to Single-Crystal Partial Dehydration7Thermochemical study of tetravalent metal sulfate tetrahydrates: A4+(SO4)2(H2O)4 (A4+ = Zr, Ce, U)4Determination of complex formation constants of neptunium(V) with propionate and lactate in 0.5–2.6 m NaCl solutions at 22–60°C using a solvent extraction technique2In Situ Formation of Unprecedented Neptunium-Oxide Wheel Clusters Stabilized in a Metal–Organic Framework47Quantum-mechanical determination of the incorporation of pentavalent plutonium into carbonate and sulfate minerals6Hydrated Uranium Oxides3Insights into the Structural Chemistry of Anhydrous and Hydrous Hexavalent Uranium and Neptunium Dinitrato, Trinitrato, and Tetranitrato Complexes16Molecular oxides of high-valent actinides18Effects of ageing on the occurrence form of uranium in vertical soil layers near an uranium tailing reservoir2The crystal and coordination chemistry of neptunium in all its oxidation states: An expanded structural hierarchy of neptunium compounds41Unusual Metal–Organic Framework Topology and Radiation Resistance through Neptunyl Coordination Chemistry32Electronic Structures and Unusual Chemical Bonding in Actinyl Peroxide Dimers [An2O6]2+ and [(An2O6)(12-crown-4 ether)2]2+ (An = U, Np, and Pu)4Density Functional Theory Guided Investigation of Ligand‐Induced Neptunyl‐Neptunyl Interactions5Modularity, polytypism, topology, and complexity of crystal structures of inorganic compounds (Review)32Cation-cation interaction in Np(V) o-chlorobenzoate complexes with 1,10-phenanthroline and 2,2′-bipyridine3Hydrothermal synthesis and structure of organically templated layered neptunyl( vi ) phosphate (NpO 2 ) 3 (PO 4 ) 2 (Terpy)0Improving Understanding of Npo2 and Np2o5 Through Vibrational Spectroscopy0Plutonium and Cerium Perrhenate/Pertechnetate Coordination Polymers and Frameworks6Improving understanding of NpO2 and Np2O5 through vibrational spectroscopy11How novel is protactinium: Insights into the structure and properties of (PaO) 2 (SO 4 ) 3 (H 2 O) 21Cation–Cation Interactions in Neptunium(V,VI)-diglycolamide System0Breaking the Neptunyl Barrier: Direct Access to Neptunium(IV) in Aqueous Solution via Polyoxometalate-Mediated Reduction and Stabilization9The first bimetallic Np( v ) MOF with a Np 4 Cs 2 O 8 structural unit: sorption properties and thermal and radiation stability0

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  1. Quaternary Neptunium Compounds: Syntheses and Characterization of KCuNpS3, RbCuNpS3, CsCuNpS3, KAgNpS3, and CsAgNpS3

    Inorganic Chemistry · 2009-08-25

    Daniel M. Wells, Geng Bang Jin, S. Skanthakumar, Richard Geoffrey Haire, L. Soderholm, James A. Ibers

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  2. Further insights into intermediate- and mixed-valency in neptunium oxoanion compounds: structure and absorption spectroscopy of K2[(NpO2)3B10O16(OH)2(NO3)2]

    Chemical Communications · 2010-01-01

    Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  3. Hydrothermal Synthesis and Crystal Structures of Actinide Compounds

    Springer eBooks · 2010-01-01

    Wolfgang Runde, Mary P. Neu

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  4. Neptunium Diverges Sharply from Uranium and Plutonium in Crystalline Borate Matrixes: Insights into the Complex Behavior of the Early Actinides Relevant to Nuclear Waste Storage

    Angewandte Chemie International Edition · 2010-01-18

    Shuao Wang, Evgeny V. Alekseev, Jie Ling, S. Skanthakumar, L. Soderholm, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  5. Neptunium Diverges Sharply from Uranium and Plutonium in Crystalline Borate Matrixes: Insights into the Complex Behavior of the Early Actinides Relevant to Nuclear Waste Storage

    Angewandte Chemie · 2010-01-18

    Shuao Wang, Evgeny V. Alekseev, Jie Ling, S. Skanthakumar, L. Soderholm, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  6. Crystal and Electronic Structure of a Mixed-Valent Np(IV)−Np(V) Compound: [BuMeIm]5[Np(NpO2)3(H2O)6Cl12]

    Inorganic Chemistry · 2010-01-25

    I. A. Charushnikova, Émilie Bossé, Dominique Guillaumont, Philippe Moisy

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  7. Incorporation of Neptunium(V) and Iodate into a Uranyl Phosphate: Implications for Mitigating the Release of 237Np and 129I in Repositories

    Environmental Science & Technology · 2010-03-12

    Shijun Wu, Fanrong Chen, Antonio Simonetti, Thomas E. Albrecht‐Schmitt

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  8. From extended solids to nano-scale actinide clusters

    Comptes Rendus Chimie · 2010-03-24

    Peter Carman Burns

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  9. Boronic Acid Flux Synthesis and Crystal Growth of Uranium and Neptunium Boronates and Borates: A Low-Temperature Route to the First Neptunium(V) Borate

    Inorganic Chemistry · 2010-10-04

    Shuao Wang, Evgeny V. Alekseev, Hannah Marie Miller, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  10. Advances in actinide solid-state and coordination chemistry

    MRS Bulletin · 2010-11-01

    Peter Carman Burns, Yasuhisa Ikeda, Ken Czerwinski

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  11. Recent progress in actinide borate chemistry

    Chemical Communications · 2011-01-01

    Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  12. Nanoscale uranium-based cage clusters inspired by uranium mineralogy

    Mineralogical Magazine · 2011-02-01

    Peter Carman Burns

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  13. Role of Anions and Reaction Conditions in the Preparation of Uranium(VI), Neptunium(VI), and Plutonium(VI) Borates

    Inorganic Chemistry · 2011-02-03

    Shuao Wang, Eric M. Villa, Juan Diwu, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  14. U(VI) Uranyl Cation−Cation Interactions in Framework Germanates

    Inorganic Chemistry · 2011-02-03

    Jessica M. Morrison, L. Moore-Shay, Peter Carman Burns

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  15. Np-incorporation into uranyl phases: A quantum–mechanical evaluation

    Journal of Nuclear Materials · 2011-04-23

    Lindsay Shuller‐Nickles, Rodney Charles Ewing, Udo Becker

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  16. Cation–Cation Interactions: Crystal Structures of Neptunyl(V) Selenate Hydrates, (NpO2)2(SeO4)(H2O)n (n = 1, 2, and 4)

    Inorganic Chemistry · 2011-04-26

    Geng Bang Jin, S. Skanthakumar, L. Soderholm

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  17. K(NpO2)3(H2O)Cl4: A Channel Structure Assembled by Two- and Three-Center Cation–Cation Interactions of Neptunyl Cations

    Inorganic Chemistry · 2011-05-09

    Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  18. Two New Neptunyl(V) Selenites: A Novel Cation–Cation Interaction Framework in (NpO2)3(OH)(SeO3)(H2O)2·H2O and a Uranophane-Type Sheet in Na(NpO2)(SeO3)(H2O)

    Inorganic Chemistry · 2011-06-07

    Geng Bang Jin, S. Skanthakumar, L. Soderholm

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  19. New Neptunium(V) Borates That Exhibit the Alexandrite Effect

    Inorganic Chemistry · 2011-12-06

    Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  20. Stabilising pentavalent actinides—visible–near infrared and X-ray absorption spectroscopic studies of the utility of the [(Np 3 W 4 O 15 )(H 2 O) 3 (MW 9 O 33 ) 3 ] 18 − (M = Sb, Bi) structural type

    Dalton Transactions · 2011-12-21

    Kevin S. Boland, Steven D. Conradson, Alison L. Costello, Andrew J. Gaunt, Stosh A. Kozimor, Iain May, Sean D. Reilly, David D. Schnaars

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  21. Three New Sodium Neptunyl(V) Selenate Hydrates: Structures, Raman Spectroscopy, and Magnetism

    Inorganic Chemistry · 2012-02-22

    Geng Bang Jin, S. Skanthakumar, L. Soderholm

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  22. Preparation, Stability, and Structural Characterization of Plutonium(VII) in Alkaline Aqueous Solution

    Inorganic Chemistry · 2012-04-23

    Mark R. Antonio, C.W. Williams, James A. Sullivan, S. Skanthakumar, Yung‐Jin Hu, L. Soderholm

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  23. (UO2)2[UO4(trz)2](OH)2: A U(VI) Coordination Intermediate between a Tetraoxido Core and a Uranyl Ion with Cation–Cation Interactions

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    Zhehui Weng, Shuao Wang, Jie Ling, Jessica M. Morrison, Peter Carman Burns

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  24. Cation–Cation Interactions between Neptunyl(VI) Units

    Inorganic Chemistry · 2012-06-11

    Shuao Wang, Juan Diwu, Evgeny V. Alekseev, Laurent J. Jouffret, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  25. Mineralogic controls on aqueous neptunium(V) concentrations in silicate systems

    Journal of Nuclear Materials · 2012-09-13

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  26. One-Dimensional Uranyl-2,2′-bipyridine Coordination Polymer with Cation–Cation Interactions: (UO2)2(2,2′-bpy)(CH3CO2)(O)(OH)

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  27. Incorporation of Neptunium(VI) into a Uranyl Selenite

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    Nathan A. Meredith, Matthew J. Polinski, Jian Hung Lin, Antonio Simonetti, Thomas E. Albrecht‐Schmitt

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  28. Clusters of Actinides with Oxide, Peroxide, or Hydroxide Bridges

    Chemical Reviews · 2012-10-24

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  29. Solution and Solid-State Structural Chemistry of Actinide Hydrates and Their Hydrolysis and Condensation Products

    Chemical Reviews · 2012-10-29

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  30. New Reactivity of the Uranyl(VI) Ion

    Chemistry - A European Journal · 2012-11-14

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  31. Synthetic Influences on Neptunium Incorporation in Naturally Occurring Copper Uranyl Phosphates

    Crystal Growth & Design · 2012-12-05

    Nathan A. Meredith, Matthew J. Polinski, Justin N. Cross, Eric M. Villa, Antonio Simonetti, Thomas E. Albrecht‐Schmitt

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  32. Transuranium Inorganic Chemistry

    Elsevier eBooks · 2013-01-01

    Matthew J. Polinski, Peter Carman Burns, Thomas E. Albrecht‐Schmitt

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  33. Synthesis and Characterization of the First 2 D Neptunyl Structure Stabilized by Side‐on Cation–Cation Interactions

    Chemistry - A European Journal · 2013-01-30

    Bess Vlaisavljevich, Pere Miró, Dongxia Ma, Ginger E. Sigmon, Peter Carman Burns, Christopher J. Cramer, Laura Gagliardi

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  34. Mixed-Valent Neptunium(IV/V) Compound with Cation–Cation-Bound Six-Membered Neptunyl Rings

    Inorganic Chemistry · 2013-10-24

    Geng Bang Jin

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  35. Crystal growth, structural characterization, cation–cation interaction classification, and optical properties of uranium( vi ) containing oxychlorides, A 4 U 5 O 16 Cl 2 (A = K, Rb), Cs 5 U 7 O 22 Cl 3 , and AUO 3 Cl (A = Rb, Cs)

    CrystEngComm · 2014-01-01

    Cory Michael Read, Jeongho Yeon, Mark D. Smith, Hans‐Conrad zur Loye

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  36. Cation–cation interactions and cation exchange in a series of isostructural framework uranyl tungstates

    Journal of Solid State Chemistry · 2014-02-10

    Enrica Balboni, Peter Carman Burns

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  37. Straightforward Reductive Routes to Air-Stable Uranium(III) and Neptunium(III) Materials

    Inorganic Chemistry · 2014-06-25

    Justin N. Cross, Eric M. Villa, Victoria R. Darling, Matthew J. Polinski, Jian Hung Lin, Xiaoyan Tan, Naoki Kikugawa, Michael Shatruk, Ryan Baumbach, Thomas E. Albrecht‐Schmitt

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  38. Incorporation of Np(V) and U(VI) in carbonate and sulfate minerals crystallized from aqueous solution

    Geochimica et Cosmochimica Acta · 2014-12-24

    Enrica Balboni, Jessica M. Morrison, Zhe-Ming Wang, Mark Engelhard, Peter Carman Burns

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  39. Structural and Morphological Influences on Neptunium Incorporation in Uranyl Molybdates

    Crystal Growth & Design · 2015-09-22

    Nathan A. Meredith, Ginger E. Sigmon, Antonio Simonetti, Peter Carman Burns

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  40. A Revised and Expanded Structure Hierarchy of Natural and Synthetic Hexavalent Uranium Compounds

    The Canadian Mineralogist · 2016-01-01

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  41. Oxo Clusters of 5f Elements

    Structure and bonding · 2016-01-01

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  42. Effects of Titanium Doping in Titanomagnetite on Neptunium Sorption and Speciation

    Environmental Science & Technology · 2016-01-12

    Ernest M. Wylie, Daniel T. Olive, Brian A. Powell

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  43. Three-Dimensional Network of Cation–Cation-Bound Neptunyl(V) Squares: Synthesis and in Situ Raman Spectroscopy Studies

    Inorganic Chemistry · 2016-02-17

    Geng Bang Jin

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  44. Evaluation of f-element borate chemistry

    Coordination Chemistry Reviews · 2016-03-19

    Mark A. Silver, Thomas E. Albrecht‐Schmitt

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  45. A first principles study of energetics and electronic structural responses of uranium-based coordination polymers to Np incorporation

    Radiochimica Acta · 2017-06-29

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  46. Synthesis and Study of the First Zeolitic Uranium Borate

    Crystal Growth & Design · 2017-11-28

    Yucheng Hao, Vladislav V. Klepov, Philip Kegler, Giuseppe Modolo, Dirk Bosbach, Thomas E. Albrecht‐Schmitt, Shuao Wang, Evgeny V. Alekseev

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  47. A neptunium( v )-mediated interwoven transuranium-rotaxane network incorporating a mechanically interlocked [ c 2]daisy chain unit

    Chemical Communications · 2018-01-01

    Lei Mei, Chao Xu, Qun‐Yan Wu, Kong‐Qiu Hu, Li‐Yong Yuan, Jing Chen, Chengliang Xiao, Shuao Wang, Zhifang Chai, Wei‐Qun Shi

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  48. Impacts of Oxo Interactions on Np(V) Crown Ether Complexes

    Inorganic Chemistry · 2018-05-07

    Madeline Basile, Erica Cole, Tori Z. Forbes

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  49. Mixed-Valent Cyanoplatinates Featuring Neptunyl–Neptunyl Cation–Cation Interactions

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  50. Actinides: Crystallography

    Encyclopedia of Inorganic and Bioinorganic Chemistry · 2018-09-14

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