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RESEARCH PAPER · Chemistry of Materials · 2004

Time-Resolved, In Situ X-ray Diffraction Studies of Staging during Phosphonic Acid Intercalation into [LiAl2(OH)6]Cl·H2O

Gareth R. Williams, Alexander J. Norquist, Dermot O’Hare

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Time-Resolved, In Situ X-ray Diffraction Studies of Staging during Phosphonic Acid Intercalation into [LiAl2(OH)6]Cl·H2OOriginalHydroxy Double Salt Anion Exchange Kinetics: Effects of Precursor Structure and Anion Size51Factors Influencing Staging during Anion-Exchange Intercalation into [LiAl2(OH)6]X·mH2O (X = Cl-, Br-, NO3-)59Mechanism of the anion exchange reactions of the layered double hydroxides (LDHs) of Ca and Mg with Al164Preparation of Layered Double Hydroxides362Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time-resolved, In-situ X-ray Powder Diffraction57Structural Aspects of Layered Double Hydroxides705Intercalation chemistry of the novel layered double hydroxides [MAl4(OH)12](NO3)2·yH2O (M = Zn, Cu, Ni and Co). 1: New organic intercalates and reaction mechanisms68Towards understanding, control and application of layered double hydroxide chemistry582New phosphonate intercalates of [Ca2Al(OH)6]NO3⋅yH2O: A synthetic and kinetic study30A Kinetic Study of the Intercalation of Lithium Salts into Al(OH)354Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time‐Resolved, in situ X‐Ray Powder Diffraction15Probing the interaction between di- and tri-functionalized carboxy-phosphonic acid and LDH layer structure14Factors influencing the hydration of layered double hydroxides (LDHs) and the appearance of an intermediate second staging phase139Staging during anion-exchange intercalation into [LiAl2(OH)6]Cl·yH2O: structural and mechanistic insights37Preparation and characterization of l-cystine and l-cysteine intercalated layered double hydroxides41Conservation of Order, Disorder, and “Crystallinity” during Anion-Exchange Reactions among Layered Double Hydroxides (LDHs) of Zn with Al112Second staging of tartrate and carbonate anions in Mg–Al layered double hydroxide22Application of layered double hydroxides for removal of oxyanions: A review1708Hydrotalcites and their role in coordination of anions in Bayer liquors: Anion binding in layered double hydroxides236Computer Simulation Study of the Structural Stability and Materials Properties of DNA-Intercalated Layered Double Hydroxides126Intercalation of l -Dopa into Layered Double Hydroxides: Enhancement of Both Chemical and Stereochemical Stabilities of a Drug through Host−Guest Interactions120Role of Host Layer Flexibility in DNA Guest Intercalation Revealed by Computer Simulation of Layered Nanomaterials63Observation of Staging during Intercalation in Layered α-Cobalt Hydroxides: A Synthetic and Kinetic Study29A thermodynamically stable layered double hydroxide heterostructure11Incorporation of phosphorus oxyacids into layered double hydroxides21Thermal decomposition of silylated layered double hydroxides20Recent Developments in the Use of Layered Double Hydroxides as Host Materials for the Storage and Triggered Release of Functional Anions144Intercalation chemistry in a LDH system: anion exchange process and staging phenomenon investigated by means of time-resolved, in situ X-ray diffraction54Observation and Isolation of Layered and Framework Ytterbium Hydroxide Phases Using In Situ Energy-Dispersive X-ray Diffraction56Origin of CO32– Shortage in MgAl Layered Double Hydroxides with Mg/Al < 230Structural and microstructural changes during anion exchange of CoAl layered double hydroxides: anin situX-ray powder diffraction study25Layered intercalated functional materials based on efficient utilization of magnesium resources in China14The intercalation of bicyclic and tricyclic carboxylates into layered double hydroxides12Assembly Chemistry of Anion-intercalated Layered Materials29Anion Exchange Kinetics of Nanodimensional Layered Metal Hydroxides: Use of Isoconversional Analysis14Modelling of X-ray diffraction profiles35Structural adjustment during intercalation of macrocyclic crown ether into LDH via swelling/restoration reaction: staging formation and mechanism insights31The application of statistical methodology to the analysis of time-resolved X-ray diffraction data12Structure and Catalytic Property of Li–Al Metal Oxides from Layered Double Hydroxide Precursors Prepared via a Facile Solution Route44Kinetics and mechanism of ionic intercalation/de-intercalation during the formation of α-cobalt hydroxide and its polymorphic transition to β-cobalt hydroxide: reaction–diffusion framework44Structural change from homogenous structure to staging in benzoic acid intercalated LDH: experimental and molecular dynamics simulation insights17The selective intercalation of organic carboxylates and sulfonates into hydroxy double salts23A new method for fast intercalation of bulk crown ether guest into LDH23Co‐Assembly of LDH Nanosheets with Crown Ethers: Structural Transformation and Water‐Adsorption Behavior13Solvothermal synthesis of Li–Al layered double hydroxides and their electrochemical performance43Dispersion-Enhanced Supported Pd Catalysts for Efficient Growth of Carbon Nanotubes through Chemical Vapor Deposition11An effect of alginate on the stability of LDH nanosheets in aqueous solution and preparation of alginate/LDH nanocomposites66Kinetic and Mechanistic Study of COF-1 Phase Change from a Staggered to Eclipsed Model upon Partial Removal of Mesitylene46Ion exchange and intercalation properties of layered double hydroxides towards halide anions63Combined In Situ and In Silico Studies of Guest Intercalation into the Layered Double Hydroxide [LiAl2(OH)6]X·yH2O4X-ray diffraction and X-ray absorption spectroscopic analyses for intercalative nanohybrids with low crystallinity32Hydroxy double salts loaded with bioactive ions: Synthesis, intercalation mechanisms, and functional performance14Morphology and Thermal Property of Poly(L-Lactide)/Layered Double Hydroxides Nanocomposites via Melt Intercalation4Molecular Orientation of Intercalants Stabilized in the Interlayer Space of Layered Ceramics: 1-D Electron Density Simulation5Functional Host–Guest Materials8Mechano-hydrothermal preparation of Li-Al-OH layered double hydroxides45LiAl2(OH)6OH.2H2O solubility product and dihydrogen radiolytic production rate under γ-irradiation20Highly efficient extraction of lithium from salt lake brine by LiAl-layered double hydroxides as lithium-ion-selective capturing material129Development of a Novel Time-Resolved Synchrotron-Radiation X-ray Diffraction Measurement System for In Situ Observation of Crystal Structure in Aqueous Solution during Chemical Reaction: Application to the Anion-Exchange Reaction of a Layered Double Hydroxide from Chloride to Nitrate9Reversible hydration of the perchlorate-intercalated layered double hydroxides of Li and Al: structure models for the dehydrated phases3Solid state NMR studies of layered double hydroxides16Why is aluminum‐based lithium adsorbent ineffective in Li + extraction from sulfate‐type brines41Efficient Step-by-Step Desorption to Reduce Boron in Brine Lithium Extraction11A review of Al-based lithium adsorbents for efficient lithium recovery from salty brine: adsorption mechanism and application progress7Recrystallization Behavior of MgAl Layered Double Hydroxide Films on Anodized Magnesium Alloys During Phytic Acid Loading0

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  1. Hydroxy Double Salt Anion Exchange Kinetics: Effects of Precursor Structure and Anion Size

    The Journal of Physical Chemistry B · 2005-02-12

    Everson Kandare, Jeanne M. Hossenlopp

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  2. Factors Influencing Staging during Anion-Exchange Intercalation into [LiAl2(OH)6]X·mH2O (X = Cl-, Br-, NO3-)

    Chemistry of Materials · 2005-04-22

    Gareth R. Williams, Dermot O’Hare

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  3. Mechanism of the anion exchange reactions of the layered double hydroxides (LDHs) of Ca and Mg with Al

    Solid State Sciences · 2005-07-06

    A.V. Radha, P. Vishnu Kamath, Chikkadasappa Shivakumara

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  4. Preparation of Layered Double Hydroxides

    Structure and bonding · 2005-09-28

    Jing He, Min Wei, Bo Li, Yu Kang, David G. Evans, Xue Duan

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  5. Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time-resolved, In-situ X-ray Powder Diffraction

    Structure and bonding · 2005-11-08

    Gareth R. Williams, Aamir I. Khan, Dermot O’Hare

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  6. Structural Aspects of Layered Double Hydroxides

    Structure and bonding · 2005-12-02

    David G. Evans, Rct Slade

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  7. Intercalation chemistry of the novel layered double hydroxides [MAl4(OH)12](NO3)2·yH2O (M = Zn, Cu, Ni and Co). 1: New organic intercalates and reaction mechanisms

    Journal of Materials Chemistry · 2006-01-01

    Gareth R. Williams, Thomas G. Dunbar, Andrew J. Beer, Andrew M. Fogg, Dermot O’Hare

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  8. Towards understanding, control and application of layered double hydroxide chemistry

    Journal of Materials Chemistry · 2006-01-01

    Gareth R. Williams, Dermot O’Hare

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  9. New phosphonate intercalates of [Ca2Al(OH)6]NO3⋅yH2O: A synthetic and kinetic study

    Solid State Sciences · 2006-05-05

    Gareth R. Williams, Dermot O’Hare

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  10. A Kinetic Study of the Intercalation of Lithium Salts into Al(OH)3

    The Journal of Physical Chemistry B · 2006-05-13

    Gareth R. Williams, Dermot O’Hare

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  11. Mechanistic and Kinetic Studies of Guest Ion Intercalation into Layered Double Hydroxides Using Time‐Resolved, in situ X‐Ray Powder Diffraction

    ChemInform · 2006-05-23

    Gareth R. Williams, Aamir I. Khan, Dermot O’Hare

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  12. Probing the interaction between di- and tri-functionalized carboxy-phosphonic acid and LDH layer structure

    Journal of Physics and Chemistry of Solids · 2006-09-07

    El Mouloudi Sabbar, M.E. de Roy, Fabrice Leroux

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  13. Factors influencing the hydration of layered double hydroxides (LDHs) and the appearance of an intermediate second staging phase

    Applied Clay Science · 2006-10-18

    Nobuo Iyi, Kazuko Fujii, K OKAMOTO, Takayoshi Sasaki

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  14. Staging during anion-exchange intercalation into [LiAl2(OH)6]Cl·yH2O: structural and mechanistic insights

    Dalton Transactions · 2007-01-01

    Gareth R. Williams, Andrew M. Fogg, Jeremy Sloan, Christine Taviot‐Guého, Dermot O’Hare

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  15. Preparation and characterization of l-cystine and l-cysteine intercalated layered double hydroxides

    Journal of Materials Science · 2007-01-03

    Min Wei, Jian Ting Guo, Zhiyu Shi, Qi Yuan, Min Pu, Guoying Rao, Xue Duan

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  16. Conservation of Order, Disorder, and “Crystallinity” during Anion-Exchange Reactions among Layered Double Hydroxides (LDHs) of Zn with Al

    The Journal of Physical Chemistry B · 2007-03-09

    A.V. Radha, P. Vishnu Kamath, Chikkadasappa Shivakumara

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  17. Second staging of tartrate and carbonate anions in Mg–Al layered double hydroxide

    Applied Clay Science · 2007-06-06

    Wenhui Zhang, Jing He, Canxiong Guo

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  18. Application of layered double hydroxides for removal of oxyanions: A review

    Water Research · 2007-11-09

    Kok-Hui Goh, Teik‐Thye Lim, Zhili Dong

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  19. Hydrotalcites and their role in coordination of anions in Bayer liquors: Anion binding in layered double hydroxides

    Coordination Chemistry Reviews · 2008-01-18

    Sara J. Palmer, Raymond L. Frost, Tiến Vinh Nguyễn

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  20. Computer Simulation Study of the Structural Stability and Materials Properties of DNA-Intercalated Layered Double Hydroxides

    Journal of the American Chemical Society · 2008-03-18

    Mary-Ann Thyveetil, Peter V. Coveney, H. Chris Greenwell, James L. Suter

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  21. Intercalation of l -Dopa into Layered Double Hydroxides: Enhancement of Both Chemical and Stereochemical Stabilities of a Drug through Host−Guest Interactions

    Chemistry of Materials · 2008-07-30

    Min Wei, Min Pu, Jian Ting Guo, Jingbin Han, Feng Li, Jing He, David G. Evans, Xue Duan

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  22. Role of Host Layer Flexibility in DNA Guest Intercalation Revealed by Computer Simulation of Layered Nanomaterials

    Journal of the American Chemical Society · 2008-08-23

    Mary-Ann Thyveetil, Peter V. Coveney, H. Chris Greenwell, James L. Suter

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  23. Observation of Staging during Intercalation in Layered α-Cobalt Hydroxides: A Synthetic and Kinetic Study

    Inorganic Chemistry · 2008-11-14

    Yi Ping Du, Dermot O’Hare

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  24. A thermodynamically stable layered double hydroxide heterostructure

    Journal of Materials Chemistry · 2009-01-01

    Anusha Ragavan, Gareth R. Williams, Dermot O’Hare

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  25. Incorporation of phosphorus oxyacids into layered double hydroxides

    Solid State Sciences · 2009-04-06

    Gareth R. Williams, Nicholas H. Rees, Dermot O’Hare

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  26. Thermal decomposition of silylated layered double hydroxides

    Journal of Thermal Analysis and Calorimetry · 2009-11-04

    Qi Tao, Hongping He, Ray L. Frost, Peng Yuan, Jianxi Zhu

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  27. Recent Developments in the Use of Layered Double Hydroxides as Host Materials for the Storage and Triggered Release of Functional Anions

    Industrial & Engineering Chemistry Research · 2009-11-10

    Aamir I. Khan, Anusha Ragavan, Bonnie L. Fong, Charles Markland, Mark O’Brien, Thomas G. Dunbar, Gareth R. Williams, Dermot O’Hare

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  28. Intercalation chemistry in a LDH system: anion exchange process and staging phenomenon investigated by means of time-resolved, in situ X-ray diffraction

    Dalton Transactions · 2010-01-01

    Christine Taviot‐Guého, Yongjun Feng, Azzam Faour, Fabrice Leroux

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  29. Observation and Isolation of Layered and Framework Ytterbium Hydroxide Phases Using In Situ Energy-Dispersive X-ray Diffraction

    Chemistry of Materials · 2010-03-04

    Laura J. McIntyre, Timothy J. Prior, Andrew M. Fogg

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  30. Origin of CO32– Shortage in MgAl Layered Double Hydroxides with Mg/Al < 2

    European Journal of Inorganic Chemistry · 2010-04-13

    Shulan Ma, Cuihong Fan, Gailing Huang, Yumei Li, Xiaojing Yang, Kenta Ooi

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  31. Structural and microstructural changes during anion exchange of CoAl layered double hydroxides: anin situX-ray powder diffraction study

    Journal of Applied Crystallography · 2010-04-30

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  32. Layered intercalated functional materials based on efficient utilization of magnesium resources in China

    Science China Chemistry · 2010-07-01

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  33. The intercalation of bicyclic and tricyclic carboxylates into layered double hydroxides

    Journal of Solid State Chemistry · 2010-10-02

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  34. Assembly Chemistry of Anion-intercalated Layered Materials

    Elsevier eBooks · 2010-11-12

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  35. Anion Exchange Kinetics of Nanodimensional Layered Metal Hydroxides: Use of Isoconversional Analysis

    The Journal of Physical Chemistry A · 2010-11-16

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  36. Modelling of X-ray diffraction profiles

    Mineralogical Society of Great Britain and Ireland eBooks · 2011-01-01

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  37. Structural adjustment during intercalation of macrocyclic crown ether into LDH via swelling/restoration reaction: staging formation and mechanism insights

    Dalton Transactions · 2011-01-01

    Shulan Ma, Li Du, Juan Wang, Nankai Chu, Yahong Sun, Genban Sun, Xiaojing Yang, Kenta Ooi

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  38. The application of statistical methodology to the analysis of time-resolved X-ray diffraction data

    Analytical Methods · 2011-01-01

    J. Burley, Dermot O’Hare, Gareth R. Williams

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  39. Structure and Catalytic Property of Li–Al Metal Oxides from Layered Double Hydroxide Precursors Prepared via a Facile Solution Route

    Industrial & Engineering Chemistry Research · 2011-05-11

    Jia Wang, Zhiyi Lei, Hua Qin, Lihong Zhang, Feng Li

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  40. Kinetics and mechanism of ionic intercalation/de-intercalation during the formation of α-cobalt hydroxide and its polymorphic transition to β-cobalt hydroxide: reaction–diffusion framework

    Journal of Materials Chemistry · 2012-01-01

    Janane F. Rahbani, Niveen M. Khashab, Digambara Patra, Mazen Al‐Ghoul

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  41. Structural change from homogenous structure to staging in benzoic acid intercalated LDH: experimental and molecular dynamics simulation insights

    Physical Chemistry Chemical Physics · 2012-01-01

    Yanru Zhang, Hongwei Tan, Jingxiang Zhao, Xinxin Li, Hui Ma, Xiaoduan Chen, Xiaojing Yang

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  42. The selective intercalation of organic carboxylates and sulfonates into hydroxy double salts

    Journal of Materials Chemistry · 2012-01-01

    Gareth R. Williams, John Crowder, J. Burley, Andrew M. Fogg

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  43. A new method for fast intercalation of bulk crown ether guest into LDH

    Journal of Colloid and Interface Science · 2012-10-23

    Shulan Ma, Juan Wang, Li Du, Yahong Sun, Qingyang Gu, Genban Sun, Xiaojing Yang

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  44. Co‐Assembly of LDH Nanosheets with Crown Ethers: Structural Transformation and Water‐Adsorption Behavior

    European Journal of Inorganic Chemistry · 2013-01-17

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  45. Solvothermal synthesis of Li–Al layered double hydroxides and their electrochemical performance

    Materials Chemistry and Physics · 2013-03-21

    Jinbo Wei, Zan Jun Gao, Yanchao Song, Wanlu Yang, Jun Wang, Zhanshuang Li, Tom Mann, Milin Zhang, Lianhe Liu

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  46. Dispersion-Enhanced Supported Pd Catalysts for Efficient Growth of Carbon Nanotubes through Chemical Vapor Deposition

    Industrial & Engineering Chemistry Research · 2013-03-25

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  47. An effect of alginate on the stability of LDH nanosheets in aqueous solution and preparation of alginate/LDH nanocomposites

    Carbohydrate Polymers · 2013-07-25

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  48. Kinetic and Mechanistic Study of COF-1 Phase Change from a Staggered to Eclipsed Model upon Partial Removal of Mesitylene

    The Journal of Physical Chemistry C · 2013-12-09

    Yi Ping Du, David C. Calabro, Bradley Wooler, Quanchang Li, Stephen Cundy, Preeti Kamakoti, Doug Colmyer, Kanmi Mao, Peter I. Ravikovitch

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  49. Ion exchange and intercalation properties of layered double hydroxides towards halide anions

    Dalton Transactions · 2014-01-01

    Umberto Costantino, Riccardo Vivani, Maria Bastianini, Ferdinando Costantino, Morena Nocchetti

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  50. Combined In Situ and In Silico Studies of Guest Intercalation into the Layered Double Hydroxide [LiAl2(OH)6]X·yH2O

    The Journal of Physical Chemistry C · 2015-07-06

    Abdessamad Y. A. Kaassis, Simin Xu, David G. Evans, Gareth R. Williams, Min Wei, Xue Duan

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