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RESEARCH PAPER · Chemistry of Materials · 2010

Observation and Isolation of Layered and Framework Ytterbium Hydroxide Phases Using In Situ Energy-Dispersive X-ray Diffraction

Laura J. McIntyre, Timothy J. Prior, Andrew M. Fogg

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Observation and Isolation of Layered and Framework Ytterbium Hydroxide Phases Using In Situ Energy-Dispersive X-ray DiffractionOriginalLayered Rare-Earth Hydroxides (LRHs) of (Y1−xEux)2(OH)5NO3·nH2O (x = 0−1): Structural Variations by Eu3+ Doping, Phase Conversion to Oxides, and the Correlation of Photoluminescence Behaviors122Yb3O(OH)6Cl·2H2O: An Anion-Exchangeable Hydroxide with a Cationic Inorganic Framework Structure69ChemInform Abstract: Observation and Isolation of Layered and Framework Ytterbium Hydroxide Phases Using in situ Energy‐Dispersive X‐Ray Diffraction.1Ln2(OH)4SO4·nH2O (Ln = Pr to Tb;n∼ 2): A New Family of Layered Rare-Earth Hydroxides Rigidly Pillared by Sulfate Ions119Nanometer-thin layered hydroxide platelets of (Y0.95Eu0.05)2(OH)5NO3·xH2O: exfoliation-free synthesis, self-assembly, and the derivation of dense oriented oxide films of high transparency and greatly enhanced luminescence69Synthesis and characterization of layered double hydroxides intercalated with sugar phosphates7The effects of Gd3+ substitution on the crystal structure, site symmetry, and photoluminescence of Y/Eu layered rare-earth hydroxide (LRH) nanoplates65Well-defined crystallites autoclaved from the nitrate/NH4OH reaction system as the precursor for (Y,Eu)2O3 red phosphor: Crystallization mechanism, phase and morphology control, and luminescent property42Paramagnetic nanoparticles as potential MRI contrast agents: characterization, NMR relaxation, simulations and theory45Intercalation of Amino Acids into Eu3+‐Doped Layered Gadolinium Hydroxide and Quenching of Eu3+ Luminescence40In situ synchrotron powder X-ray diffraction study of formation and growth of yttrium and ytterbium aluminum garnet nanoparticles in sub- and supercritical water16Structure characterization and photoluminescence properties of (Y0.95−xGdxEu0.05)2O3 red phosphors converted from layered rare-earth hydroxide (LRH) nanoflake precursors40Lanthanide-Porphyrin Hybrids: from Layered Structures to Metal–Organic Frameworks with Photophysical Properties81Layered rare-earth hydroxide and oxide nanoplates of the Y/Tb/Eu system: phase-controlled processing, structure characterization and color-tunable photoluminescence via selective excitation and efficient energy transfer56Structural Features and Color Tunable Photoluminescence of the Binary and Ternary Layered Rare-Earth Hydroxides of (Y,Ln)2(OH)5NO3·nH2O (Ln=Tb, Eu)1Cathodic electrodeposition and characterization of nanostructured Y2O3 from chloride solution Part I: Effect of current density7Anion-Centered Tetrahedra in Inorganic Compounds242Cathodic electrodeposition and characterization of nanostructured Y2O3 from nitrate solution. Part I: Effect of current density1Structural transformation and photoluminescence behavior during calcination of the layered europium-doped yttrium hydroxide intercalate with organic-sensitizer17Intercalation of Diverse Organic Guests into Layered Europium Hydroxides – Structural Tuning and Photoluminescence Behavior25Tens of micron-sized unilamellar nanosheets of Y/Eu layered rare-earth hydroxide: efficient exfoliation via fast anion exchange and their self-assembly into oriented oxide film with enhanced photoluminescence47Layered rare earth hydroxides (LREHs): synthesis and structure characterization towards multifunctionality58Synthesis and characterisation of a new anion exchangeable layered hydroxyiodide4New layered double hydroxides by prepared by the intercalation of gibbsite13Powder Diffraction and Synchrotron Radiation2The Effects of Sulfate Anion Exchange on Structural Feature and Thermal Behavior of Y2(OH)5NO3•nH2O Layered Hydroxide Nanosheets0High-yield microwave synthesis of layered Y 2 (OH) 5 NO 3 ·xH 2 O materials34Layered Rare Earth Hydroxides: Structural Aspects and Photoluminescence Properties10One-step freezing temperature crystallization of layered rare-earth hydroxide (Ln 2 (OH) 5 NO 3 ·nH 2 O) nanosheets for a wide spectrum of Ln (Ln = Pr–Er, and Y), anion exchange with fluorine and sulfate, and microscopic coordination probed via photoluminescence58Hydrothermal-assisted exfoliation of Y/Tb/Eu ternary layered rare-earth hydroxides into tens of micron-sized unilamellar nanosheets for highly oriented and color-tunable nano-phosphor films13Boosting Proton Conductivity in Highly Robust 3D Inorganic Cationic Extended Frameworks through Ion Exchange with Dihydrogen Phosphate Anions19Highly Enhanced and Switchable Photoluminescence Properties in Pillared Layered Hydroxides Stabilizing Ce3+16Towards new materials by hierarchical topotactic syntheses1Layered hydroxyl sulfate: Controlled crystallization, structure analysis, and green derivation of multi-color luminescent (La,RE)2O2SO4 and (La,RE)2O2S phosphors (RE = Pr, Sm, Eu, Tb, and Dy)66Sulfate Exchange of the Nitrate-Type Layered Hydroxide Nanosheets of Ln2(OH)5NO3·nH2O for Better Dispersed and Multi-color Luminescent Ln2O3 Nanophosphors (Ln = Y0.98RE0.02, RE = Pr, Sm, Eu, Tb, Dy, Ho, Er, and Tm)17Room-temperature fluorination of layered rare-earth hydroxide nanosheets leading to fluoride nanocrystals and elucidation of down-/up-conversion photoluminescence21Interacting layered hydroxide nanosheets with KF leading to Y/Eu hydroxyfluoride, oxyfluoride, and complex fluoride nanocrystals and investigation of photoluminescence13Two-step crystallization of a phase-pure Ln 2 (OH) 5 NO 3 ·nH 2 O layered compound for the smallest Ln ions of Tm, Yb and Lu, anion exchange, and exfoliation16Analysis of growth kinetics and impact of NH3 on the morphology evolution of hexagonal-prism shaped Y4O(OH)9NO3/Y2O3 single crystals5Recent progress in layered rare-earth hydroxide (LRH) and its application in luminescence46Controlled Hydrothermal Crystallization of Anhydrous Ln2(OH)4SO4 (Ln=Eu–Lu, Y) as a New Family of Layered Rare Earth Metal Hydroxides41Two-step synthetic route towards monodisperse vernier yttrium oxyfluoride with multicolour fluorescence7The Effects of Halogen Exchange on the Structural Features, Thermal Behavior and Photoluminescence of Y/Eu Layered Rare-Earth Hydroxide (LRH) Nanosheets0A novel synthetic route towards monodisperse yttrium hydroxide fluoride by anion exchange and luminescence properties8Synthesis and study of gadolinium-erbium layered hydroxonitrates and hydroxosulfates0Synthesis of (Y0.95Eu0.05)2O3 thin transparent oxide films from layered rare earth hydroxides prepared by coprecipitation at a constant pH value2Ultrathin 2D Rare‐Earth Nanomaterials: Compositions, Syntheses, and Applications162Shape control over microwave hydrothermally grown Y2O3:Eu by europium concentration adjustment15Layered rare-earth hydroxides: a new family of anion-exchangeable layered inorganic materials57Naturally derived pyroxene nanomaterials: an ore for wide applications1Gold Nanoparticles on Nanosheets Derived from Layered Rare-Earth Hydroxides for Catalytic Glycerol-to-Lactic Acid Conversion32“X Factor” in the Structure and Anion Exchange of Layered Yttrium Hydroxides15Garnet transparent ceramic film of Y3Al5O12:Eu3+ fabricated through an interface reaction of layered rare-earth hydroxide nanosheets on amorphous alumina17Layered rare-earth hydroxides: crystal engineering toward functional nanosheets9Exploring the Crystallization of Lanthanum(III) and Neodymium(III) Hydroxides from Solution4Drastic enhancement of photoluminescence properties from anion-pillared layered Y/Eu hydroxides with oxometallate species1

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  1. Layered Rare-Earth Hydroxides (LRHs) of (Y1−xEux)2(OH)5NO3·nH2O (x = 0−1): Structural Variations by Eu3+ Doping, Phase Conversion to Oxides, and the Correlation of Photoluminescence Behaviors

    Chemistry of Materials · 2010-07-02

    Qi Zhu, Ji‐Guang Li, Chunyi Zhi, Xiaodong Li, Xudong Sun, Yoshio Sakka, Dmitri V. Golberg, Yoshio Bando

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  2. Yb3O(OH)6Cl·2H2O: An Anion-Exchangeable Hydroxide with a Cationic Inorganic Framework Structure

    Journal of the American Chemical Society · 2010-07-08

    Helen V. Goulding, Sarah E. Hulse, W. Clegg, Ross W. Harrington, Helen Y. Playford, Richard I. Walton, Andrew M. Fogg

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  3. ChemInform Abstract: Observation and Isolation of Layered and Framework Ytterbium Hydroxide Phases Using in situ Energy‐Dispersive X‐Ray Diffraction.

    ChemInform · 2010-07-24

    Laura J. McIntyre, Timothy J. Prior, Andrew M. Fogg

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  4. Ln2(OH)4SO4·nH2O (Ln = Pr to Tb;n∼ 2): A New Family of Layered Rare-Earth Hydroxides Rigidly Pillared by Sulfate Ions

    Chemistry of Materials · 2010-10-14

    Jianbo Liang, Renzhi Ma, Fengxia Geng, Yasuo Ebina, Takayoshi Sasaki

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  5. Nanometer-thin layered hydroxide platelets of (Y0.95Eu0.05)2(OH)5NO3·xH2O: exfoliation-free synthesis, self-assembly, and the derivation of dense oriented oxide films of high transparency and greatly enhanced luminescence

    Journal of Materials Chemistry · 2011-01-01

    Qi Zhu, J.-G. Li, Chunyi Zhi, Ruqin Ma, Takayoshi Sasaki, J. X. Xu, C. H. Liu, Xin Li, X. D. Sun, Yoshio Sakka

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  6. Synthesis and characterization of layered double hydroxides intercalated with sugar phosphates

    Journal of Physics and Chemistry of Solids · 2011-10-16

    Tom C. Jellicoe, Andrew M. Fogg

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  7. The effects of Gd3+ substitution on the crystal structure, site symmetry, and photoluminescence of Y/Eu layered rare-earth hydroxide (LRH) nanoplates

    Dalton Transactions · 2011-12-14

    Xiaoli Wu, Ji‐Guang Li, Ji-Guang Li, Qi Zhu, Jinkai Li, Jinkai Li, Renzhi Ma, Takayoshi Sasaki, Xiaodong Li, Xudong Sun, Yoshio Sakka

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  8. Well-defined crystallites autoclaved from the nitrate/NH4OH reaction system as the precursor for (Y,Eu)2O3 red phosphor: Crystallization mechanism, phase and morphology control, and luminescent property

    Journal of Solid State Chemistry · 2012-04-21

    Qi Zhu, Ji‐Guang Li, Renzhi Ma, Takayoshi Sasaki, Xiaojing Yang, Xiaodong Li, Xudong Sun, Yoshio Sakka

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  9. Paramagnetic nanoparticles as potential MRI contrast agents: characterization, NMR relaxation, simulations and theory

    Magnetic Resonance Materials in Physics Biology and Medicine · 2012-07-12

    Quoc Lam Vuong, Sabine Van Doorslaer, Jean‐Luc Bridot, Corradina Argante, Gabriela Alejandro, Raphaël P. Hermann, Sabrina Disch, Carlos Mattea, Siegfried Stapf, Yves Gossuin

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  10. Intercalation of Amino Acids into Eu3+‐Doped Layered Gadolinium Hydroxide and Quenching of Eu3+ Luminescence

    European Journal of Inorganic Chemistry · 2012-08-10

    Qingyang Gu, Yahong Sun, Nankai Chu, Shulan Ma, Zhiqian Jia, Xiaojing Yang

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  11. In situ synchrotron powder X-ray diffraction study of formation and growth of yttrium and ytterbium aluminum garnet nanoparticles in sub- and supercritical water

    RSC Advances · 2013-01-01

    Peter Nørby, Kirsten M. Ø. Jensen, Nina Lock, Mogens Christensen, Bo B. Iversen

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  12. Structure characterization and photoluminescence properties of (Y0.95−xGdxEu0.05)2O3 red phosphors converted from layered rare-earth hydroxide (LRH) nanoflake precursors

    Journal of Alloys and Compounds · 2013-02-04

    Xiaoli Wu, Ji‐Guang Li, Ji-Guang Li, Dehai Ping, Jinkai Li, Xiaodong Li, Qi Zhu, Xiaodong Li, Xudong Sun, Yoshio Sakka

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  13. Lanthanide-Porphyrin Hybrids: from Layered Structures to Metal–Organic Frameworks with Photophysical Properties

    Inorganic Chemistry · 2013-02-20

    Jan Demel, Pavel Kubát, Franck Millange, Jérôme Marrot, Ivana Cı́sařová, Kamil Lang

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  14. Layered rare-earth hydroxide and oxide nanoplates of the Y/Tb/Eu system: phase-controlled processing, structure characterization and color-tunable photoluminescence via selective excitation and efficient energy transfer

    Science and Technology of Advanced Materials · 2013-02-21

    Xiaoli Wu, Ji‐Guang Li, Jinkai Li, Jinkai Li, Jinkai Li, Qi Zhu, Xiaodong Li, Xudong Sun, Yoshio Sakka

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  15. Structural Features and Color Tunable Photoluminescence of the Binary and Ternary Layered Rare-Earth Hydroxides of (Y,Ln)2(OH)5NO3·nH2O (Ln=Tb, Eu)

    Key engineering materials · 2013-03-01

    Xiao Li Wu, Ji Guang Li, Jin Kai Li, Shao Hong Liu, Xiao Dong Li, Xu Dong Sun, Yoshio Sakka

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  16. Cathodic electrodeposition and characterization of nanostructured Y2O3 from chloride solution Part I: Effect of current density

    Russian Journal of Electrochemistry · 2013-04-01

    Mustafa Aghazadeh, Abbas-Ali Malek Barmi, Hamid Mohammad Shiri

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  17. Anion-Centered Tetrahedra in Inorganic Compounds

    Chemical Reviews · 2013-04-29

    Sergey V. Krivovichev, Olivier Mentré, Oleg I. Siidra, Marie Colmont, С. К. Филатов

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  18. Cathodic electrodeposition and characterization of nanostructured Y2O3 from nitrate solution. Part I: Effect of current density

    Russian Journal of Electrochemistry · 2013-06-01

    Abbas-Ali Malek Barmi, Mustafa Aghazadeh, Hamid Mohammad Shiri, Farzaneh Ghorab

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  19. Structural transformation and photoluminescence behavior during calcination of the layered europium-doped yttrium hydroxide intercalate with organic-sensitizer

    Materials Research Bulletin · 2013-07-30

    Yahong Sun, Guohua Pan, Qingyang Gu, Xinxin Li, Genban Sun, Shulan Ma, Xiaojing Yang

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  20. Intercalation of Diverse Organic Guests into Layered Europium Hydroxides – Structural Tuning and Photoluminescence Behavior

    European Journal of Inorganic Chemistry · 2013-12-12

    Qingyang Gu, Nankai Chu, Guohua Pan, Genban Sun, Shulan Ma, Xiaojing Yang

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  21. Tens of micron-sized unilamellar nanosheets of Y/Eu layered rare-earth hydroxide: efficient exfoliation via fast anion exchange and their self-assembly into oriented oxide film with enhanced photoluminescence

    Science and Technology of Advanced Materials · 2013-12-20

    Qi Zhu, Ji‐Guang Li, Xiaodong Li, Xudong Sun, Yang Qi, Miaoyong Zhu, Yoshio Sakka

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  22. Layered rare earth hydroxides (LREHs): synthesis and structure characterization towards multifunctionality

    Dalton Transactions · 2014-01-01

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  23. Synthesis and characterisation of a new anion exchangeable layered hydroxyiodide

    Dalton Transactions · 2014-01-01

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  24. New layered double hydroxides by prepared by the intercalation of gibbsite

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  25. Powder Diffraction and Synchrotron Radiation

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  26. The Effects of Sulfate Anion Exchange on Structural Feature and Thermal Behavior of Y2(OH)5NO3•nH2O Layered Hydroxide Nanosheets

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  27. High-yield microwave synthesis of layered Y 2 (OH) 5 NO 3 ·xH 2 O materials

    CrystEngComm · 2015-01-01

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  28. Layered Rare Earth Hydroxides: Structural Aspects and Photoluminescence Properties

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  29. One-step freezing temperature crystallization of layered rare-earth hydroxide (Ln 2 (OH) 5 NO 3 ·nH 2 O) nanosheets for a wide spectrum of Ln (Ln = Pr–Er, and Y), anion exchange with fluorine and sulfate, and microscopic coordination probed via photoluminescence

    Journal of Materials Chemistry C · 2015-01-01

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  30. Hydrothermal-assisted exfoliation of Y/Tb/Eu ternary layered rare-earth hydroxides into tens of micron-sized unilamellar nanosheets for highly oriented and color-tunable nano-phosphor films

    Nanoscale Research Letters · 2015-03-13

    Qi Zhu, Zhixin Xu, Ji‐Guang Li, Xiaodong Li, Yang Qi, Xudong Sun

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  31. Boosting Proton Conductivity in Highly Robust 3D Inorganic Cationic Extended Frameworks through Ion Exchange with Dihydrogen Phosphate Anions

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  32. Highly Enhanced and Switchable Photoluminescence Properties in Pillared Layered Hydroxides Stabilizing Ce3+

    The Journal of Physical Chemistry C · 2015-10-26

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  33. Towards new materials by hierarchical topotactic syntheses

    Unknown journal · 2015-11-13

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  34. Layered hydroxyl sulfate: Controlled crystallization, structure analysis, and green derivation of multi-color luminescent (La,RE)2O2SO4 and (La,RE)2O2S phosphors (RE = Pr, Sm, Eu, Tb, and Dy)

    Chemical Engineering Journal · 2016-05-23

    Xuejiao Wang, Ji‐Guang Li, Мaxim S. Моlokeev, Qi Zhu, Xiaodong Li, Xudong Sun

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  35. Sulfate Exchange of the Nitrate-Type Layered Hydroxide Nanosheets of Ln2(OH)5NO3·nH2O for Better Dispersed and Multi-color Luminescent Ln2O3 Nanophosphors (Ln = Y0.98RE0.02, RE = Pr, Sm, Eu, Tb, Dy, Ho, Er, and Tm)

    Nanoscale Research Letters · 2016-07-12

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  36. Room-temperature fluorination of layered rare-earth hydroxide nanosheets leading to fluoride nanocrystals and elucidation of down-/up-conversion photoluminescence

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  37. Interacting layered hydroxide nanosheets with KF leading to Y/Eu hydroxyfluoride, oxyfluoride, and complex fluoride nanocrystals and investigation of photoluminescence

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  38. Two-step crystallization of a phase-pure Ln 2 (OH) 5 NO 3 ·nH 2 O layered compound for the smallest Ln ions of Tm, Yb and Lu, anion exchange, and exfoliation

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  39. Analysis of growth kinetics and impact of NH3 on the morphology evolution of hexagonal-prism shaped Y4O(OH)9NO3/Y2O3 single crystals

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  40. Recent progress in layered rare-earth hydroxide (LRH) and its application in luminescence

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  41. Controlled Hydrothermal Crystallization of Anhydrous Ln2(OH)4SO4 (Ln=Eu–Lu, Y) as a New Family of Layered Rare Earth Metal Hydroxides

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  42. Two-step synthetic route towards monodisperse vernier yttrium oxyfluoride with multicolour fluorescence

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  43. The Effects of Halogen Exchange on the Structural Features, Thermal Behavior and Photoluminescence of Y/Eu Layered Rare-Earth Hydroxide (LRH) Nanosheets

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  44. A novel synthetic route towards monodisperse yttrium hydroxide fluoride by anion exchange and luminescence properties

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  45. Synthesis and study of gadolinium-erbium layered hydroxonitrates and hydroxosulfates

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  46. Synthesis of (Y0.95Eu0.05)2O3 thin transparent oxide films from layered rare earth hydroxides prepared by coprecipitation at a constant pH value

    AIP conference proceedings · 2019-01-01

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  47. Ultrathin 2D Rare‐Earth Nanomaterials: Compositions, Syntheses, and Applications

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  48. Shape control over microwave hydrothermally grown Y2O3:Eu by europium concentration adjustment

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  49. Layered rare-earth hydroxides: a new family of anion-exchangeable layered inorganic materials

    Russian Chemical Reviews · 2019-11-29

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  50. Naturally derived pyroxene nanomaterials: an ore for wide applications

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