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RESEARCH PAPER · Inorganic Chemistry · 2003

Controlled Structural Variations in Templated Uranium Sulfates

Alexander J. Norquist, M.B. Doran, Paul M. Thomas, Dermot O’Hare

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Controlled Structural Variations in Templated Uranium SulfatesOriginalControlled Structural Variations in Templated Uranium Sulfates.022 New compounds and structures in the solid state2The effects of hydrofluoric acid addition on the hydrothermal synthesis of templated uranium sulfates46[N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride50(C8H26N4)0.5[(UO2)2(SO4)3(H2O)]·2H2O, an organically templated uranyl sulfate with a novel layer type22Combinatorial topology of salts of inorganic oxoacids: zero-, one- and two-dimensional units with corner-sharing between coordination polyhedra103Comparative study of the flexibility of structural complexes in uranyl sulfates, chromates, and molybdates28Synthesis and Crystal Structures of α‐ and β‐Mg2[(UO2)3(SeO4)5](H2O)1639Toward Templated Metal−Organic Frameworks: Synthesis, Structures, Thermal Properties, and Luminescence of Three Novel Lanthanide−Adipate Frameworks227Synthesis and crystal structures of M2[(UO2)3(SeO4)5](H2O)16 (M=Co, Zn)2820 New compounds and structures in the solid state5Structural variation in organically templated uranium sulfate fluorides42Highly Porous Uranyl Selenate Nanotubules170(C7H20N2)[(UO2)2(SO4)3(H2O)]: an organically templated uranium sulfate with a novel layer topology18(C3H12N2)2[UO2(H2O)2(SO4)2]2·2H2O: an organically templated uranium sulfate with a novel dimer type14Self‐Assembly of Protonated 1,12‐Dodecanediamine Molecules and Strongly Undulated Uranyl Selenate Sheets in the Structure of Amine‐Templated Uranyl Selenate: (H3O)2[C12H30N2]3[(UO2)4(SeO4)8](H2O)543[H2en]2{La2M(SO4)6(H2O)2} (M=Co, Ni): First organically templated 3d–4f mixed metal sulfates38Low‐Dimensional Structural Units in Amine‐Templated Uranyl Oxoselenates(VI): Synthesis and Crystal Structures of [C3H12N2][(UO2)(SeO4)2(H2O)2](H2O), [C5H16N2]2[(UO2)(SeO4)2(H2O)](NO3)2, [C4H12N][(UO2)(SeO4)(NO3)], and [C4H14N2][(UO2)(SeO4)2(H2O)]40Organically-templated metal sulfates, selenites and selenates194Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates23Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)26The crystal structure of Li4[(UO2)2(W2O10)] and crystal chemistry of Li uranyl tungstates13An Open-Framework Thorium Sulfate Hydrate with 11.5 Å Voids42Crystal structure of [CH3NH3][(UO2)(H2AsO4)3]17Syntheses, structures, characterizations and charge-density matching of novel amino-templated uranyl selenates45Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Glycine-Templated Manganese Sulfate with New Topology and Canted Antiferromagnetism35A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems28Uranyl selenates with organic templates: Principles of structure and characteristics of self-organization23Amine templated two- and three-dimensional uranyl sulfates24Hydrothermal Synthesis and Crystal Structures of Actinide Compounds2Actinyl Compounds with Hexavalent Elements (S, Cr, Se, Mo) – Structural Diversity, Nanoscale Chemistry, and Cellular Automata Modeling69New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates28Understanding an Order–Disorder Phase Transition in Ionothermally Synthesized Gallium Phosphates9A series of new rare earth sulfates based on lanthanide contraction and dual organic-amine templating effects12Unprecedented layer topology in the crystal structure of a new organically templated uranyl selenite-selenate19Structural topology and dimensional reduction in uranyl oxysalts: eight novel phases in the methylamine–(UO2)(NO3)2–H2SeO4–H2O system24Influence of the Organic Species and Oxoanion in the Synthesis of two Uranyl Sulfate Hydrates, (H3O)2[(UO2)2(SO4)3(H2O)]·7H2O and (H3O)2[(UO2)2(SO4)3(H2O)]·4H2O, and a Uranyl Selenate‐Selenite [C5H6N][(UO2)(SeO4)(HSeO3)]15Amine templating effect absent in uranyl sulfates synthesized with 1,4-n-butyldiamine14Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks26Crystal Chemistry of Uranium Oxides and Minerals27Syntheses, Structures, and Comparisons of Thallium Uranium Phosphites, Mixed Phosphate-Phosphites, and Phosphate22Crystal structures and characterization of two divalent metal selenates templated by dabco, (C6H14N2)[MII(H2O)6](SeO4)2 (MII: NiII, ZnII)11MOFs of Uranium and the Actinides95A Family of UO22+–5-Nitro-1,3-dicarboxylate Hybrid Materials: Structural Variation As a Function of pH and Structure Directing Species20Hybrid Materials of the f-Elements Part I5Hybrid Materials of the f-Elements Part II5Host-guest structural architectures in hydrous alkaline (Li, K) uranyl chromates and dichromates10Pathways for synthesis of new selenium-containing oxo-compounds: Chemical vapor transport reactions, hydrothermal techniques and evaporation method19Mixed Uranyl Sulfate–Selenates: Evolution of Structural Topology and Complexity vs Chemical Composition23Ring opening of azetidine cycle: First examples of 1-azetidinepropanamine molecules as a template in hybrid organic-inorganic compounds14Specific Features of the Crystal Chemistry of Layered Uranyl Compounds with the Ratio UO2: TO4 = 5 : 8 (T = S6+, Cr6+, Se6+, Mo6+)9Structural unit charge density and molecular cation templating effects on orientational geometric isomerism and interlayer spacing in 2-D uranyl sulfates11Ligand Mediated Morphology of the Two‐Dimensional Uranyl Aqua Sulfates [UO2(X)(SO4)(H2O)] [X = Cl– or (CH3)3NCH2COO]6The role of 1-ethyl-3-methylimidazolium diethyl phosphate ionic liquid in uranyl phosphate compounds7Effect of Ionothermal Conditions on the Crystallization of Organically Templated Uranyl Sulfate Compounds6Hydrogen bond network and bond valence analysis on uranyl sulfate compounds with organic-based interstitial cations5Organically Templated Uranyl Sulfates and Selenates: Structural Complexity and Crystal Chemical Restrictions for Isotypic Compounds Formation7Results of 25-Year Studies of Uranium Compounds at the Department of Crystallography of St. Petersburg State University3

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  1. Controlled Structural Variations in Templated Uranium Sulfates.

    ChemInform · 2003-11-26

    Alexander J. Norquist, M.B. Doran, Paul M. Thomas, Dermot O’Hare

    Read original paper ↗ ·

  2. 22 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2004-01-01

    Gary B. Hix

    Read original paper ↗ ·

  3. The effects of hydrofluoric acid addition on the hydrothermal synthesis of templated uranium sulfates

    Dalton Transactions · 2004-01-01

    M.B. Doran, Ben E. Cockbain, Alexander J. Norquist, Dermot O’Hare

    Read original paper ↗ ·

  4. [N2C6H14]2[(UO2)6(H2O)2F2(PO4)2(HPO4)4]·4H2O: A New Microporous Uranium Phosphate Fluoride

    Chemistry of Materials · 2004-01-30

    M.B. Doran, Clair L. Stuart, Alexander J. Norquist, Dermot O’Hare

    Read original paper ↗ ·

  5. (C8H26N4)0.5[(UO2)2(SO4)3(H2O)]·2H2O, an organically templated uranyl sulfate with a novel layer type

    Acta Crystallographica Section E Structure Reports Online · 2004-06-26

    M.B. Doran, Alexander J. Norquist, Clair L. Stuart, Dermot O’Hare

    Read original paper ↗ ·

  6. Combinatorial topology of salts of inorganic oxoacids: zero-, one- and two-dimensional units with corner-sharing between coordination polyhedra

    Crystallography Reviews · 2004-07-01

    Sergey V. Krivovichev

    Read original paper ↗ ·

  7. Comparative study of the flexibility of structural complexes in uranyl sulfates, chromates, and molybdates

    Radiochemistry · 2004-09-01

    Sergey V. Krivovichev

    Read original paper ↗ ·

  8. Synthesis and Crystal Structures of α‐ and β‐Mg2[(UO2)3(SeO4)5](H2O)16

    Zeitschrift für anorganische und allgemeine Chemie · 2004-12-01

    Sergey V. Krivovichev, Volker Kahlenberg

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  9. Toward Templated Metal−Organic Frameworks: Synthesis, Structures, Thermal Properties, and Luminescence of Three Novel Lanthanide−Adipate Frameworks

    Inorganic Chemistry · 2004-12-30

    Daniel T. de Lill, Noel S. Gunning, Christopher L. Cahill

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  10. Synthesis and crystal structures of M2[(UO2)3(SeO4)5](H2O)16 (M=Co, Zn)

    Journal of Alloys and Compounds · 2004-12-31

    Sergey V. Krivovichev, Volker Kahlenberg

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  11. 20 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2005-01-01

    Gary B. Hix

    Read original paper ↗ ·

  12. Structural variation in organically templated uranium sulfate fluorides

    Dalton Transactions · 2005-01-01

    M.B. Doran, Ben E. Cockbain, Dermot O’Hare

    Read original paper ↗ ·

  13. Highly Porous Uranyl Selenate Nanotubules

    Journal of the American Chemical Society · 2005-01-06

    Sergey V. Krivovichev, Volker Kahlenberg, Ivan Gundarovich Tananaev, Reinhard Kaindl, Edgar Mersdorf, Boris F. Myasoedov

    Read original paper ↗ ·

  14. (C7H20N2)[(UO2)2(SO4)3(H2O)]: an organically templated uranium sulfate with a novel layer topology

    Acta Crystallographica Section E Structure Reports Online · 2005-04-09

    Alexander J. Norquist, M.B. Doran, Dermot O’Hare

    Read original paper ↗ ·

  15. (C3H12N2)2[UO2(H2O)2(SO4)2]2·2H2O: an organically templated uranium sulfate with a novel dimer type

    Acta Crystallographica Section E Structure Reports Online · 2005-04-16

    M.B. Doran, Alexander J. Norquist, Dermot O’Hare

    Read original paper ↗ ·

  16. Self‐Assembly of Protonated 1,12‐Dodecanediamine Molecules and Strongly Undulated Uranyl Selenate Sheets in the Structure of Amine‐Templated Uranyl Selenate: (H3O)2[C12H30N2]3[(UO2)4(SeO4)8](H2O)5

    European Journal of Inorganic Chemistry · 2005-04-28

    Sergey V. Krivovichev, Volker Kahlenberg, Evgeniya Y. Avdontseva, Edgar Mersdorf, Reinhard Kaindl

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  17. [H2en]2{La2M(SO4)6(H2O)2} (M=Co, Ni): First organically templated 3d–4f mixed metal sulfates

    Journal of Solid State Chemistry · 2005-05-29

    Yan-Ping Yuan, Rui‐Yao Wang, Deyuan Kong, Jiang‐Gao Mao, Abraham Clearfield

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  18. Low‐Dimensional Structural Units in Amine‐Templated Uranyl Oxoselenates(VI): Synthesis and Crystal Structures of [C3H12N2][(UO2)(SeO4)2(H2O)2](H2O), [C5H16N2]2[(UO2)(SeO4)2(H2O)](NO3)2, [C4H12N][(UO2)(SeO4)(NO3)], and [C4H14N2][(UO2)(SeO4)2(H2O)]

    Zeitschrift für anorganische und allgemeine Chemie · 2005-08-29

    Sergey V. Krivovichev, Volker Kahlenberg

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  19. Organically-templated metal sulfates, selenites and selenates

    Chemical Society Reviews · 2006-01-01

    C. N. R. Rao, J. N. Behera, Meenakshi Dan-Hardi

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  20. Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates

    Journal of Solid State Chemistry · 2006-12-13

    Murielle Rivenet, Nicolas Vigier, Pascal Roussel, F. Abraham

    Read original paper ↗ ·

  21. Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)

    Elsevier eBooks · 2007-01-01

    Sergey V. Krivovichev, Peter Carman Burns

    Read original paper ↗ ·

  22. The crystal structure of Li4[(UO2)2(W2O10)] and crystal chemistry of Li uranyl tungstates

    Zeitschrift für Kristallographie · 2007-07-01

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier, Thomas Malcherek, Evgeny V. Suleimanov, Evgeny V. Chuprunov

    Read original paper ↗ ·

  23. An Open-Framework Thorium Sulfate Hydrate with 11.5 Å Voids

    Inorganic Chemistry · 2008-09-24

    Richard E. Wilson, S. Skanthakumar, Karah E. Knope, Christopher L. Cahill, L. Soderholm

    Read original paper ↗ ·

  24. Crystal structure of [CH3NH3][(UO2)(H2AsO4)3]

    Radiochemistry · 2008-10-01

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

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  25. Syntheses, structures, characterizations and charge-density matching of novel amino-templated uranyl selenates

    Journal of Solid State Chemistry · 2008-11-21

    Jie Ling, Ginger E. Sigmon, Peter Carman Burns

    Read original paper ↗ ·

  26. Alternative approaches to structure description

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  27. Anion-topology approach

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  28. Basic concepts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  29. Copyright Page

    Unknown journal · 2009-01-22

    Read original paper ↗ ·

  30. Dedication

    Unknown journal · 2009-01-22

    Read original paper ↗ ·

  31. Dimensional reduction in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  32. Graph theory applied to low-dimensional structural units in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  33. Preface

    Unknown journal · 2009-01-22

    Read original paper ↗ ·

  34. Structural Crystallography of Inorganic Oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  35. Topology of framework structures in inorganic oxysalts

    Unknown journal · 2009-01-22

    Sergey V. Krivovichev

    Read original paper ↗ ·

  36. Glycine-Templated Manganese Sulfate with New Topology and Canted Antiferromagnetism

    Inorganic Chemistry · 2009-08-21

    Zhehui Weng, Zilu Chen, Fupei Liang

    Read original paper ↗ ·

  37. A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems

    Journal of Solid State Chemistry · 2009-11-01

    Laurent J. Jouffret, Murielle Rivenet, F. Abraham

    Read original paper ↗ ·

  38. Uranyl selenates with organic templates: Principles of structure and characteristics of self-organization

    Russian Journal of General Chemistry · 2009-12-01

    Sergey V. Krivovichev, Vladislav V. Gurzhiy, Ivan Gundarovich Tananaev, Boris F. Myasoedov

    Read original paper ↗ ·

  39. Amine templated two- and three-dimensional uranyl sulfates

    Dalton Transactions · 2010-01-01

    Mohan Singh Bharara, Anne E. V. Gorden

    Read original paper ↗ ·

  40. Hydrothermal Synthesis and Crystal Structures of Actinide Compounds

    Springer eBooks · 2010-01-01

    Wolfgang Runde, Mary P. Neu

    Read original paper ↗ ·

  41. Actinyl Compounds with Hexavalent Elements (S, Cr, Se, Mo) – Structural Diversity, Nanoscale Chemistry, and Cellular Automata Modeling

    European Journal of Inorganic Chemistry · 2010-05-25

    Sergey V. Krivovichev

    Read original paper ↗ ·

  42. New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates

    Journal of Solid State Chemistry · 2010-07-25

    Laurent J. Jouffret, Zhenmian Shao, Murielle Rivenet, F. Abraham

    Read original paper ↗ ·

  43. Understanding an Order–Disorder Phase Transition in Ionothermally Synthesized Gallium Phosphates

    Crystal Growth & Design · 2011-05-04

    Jacob H. Olshansky, Samuel M. Blau, Mat­thias Zeller, Joshua Schrier, Alexander J. Norquist

    Read original paper ↗ ·

  44. A series of new rare earth sulfates based on lanthanide contraction and dual organic-amine templating effects

    CrystEngComm · 2012-01-01

    Deng Zhang, Yun Lu, Lei Chen, Hu Cai, Dunru Zhu, Yan Xu

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  45. Unprecedented layer topology in the crystal structure of a new organically templated uranyl selenite-selenate

    Mendeleev Communications · 2012-01-01

    Vadim M. Kovrugin, Vladislav V. Gurzhiy, Sergey V. Krivovichev, Ivan Gundarovich Tananaev, Boris F. Myasoedov

    Read original paper ↗ ·

  46. Structural topology and dimensional reduction in uranyl oxysalts: eight novel phases in the methylamine–(UO2)(NO3)2–H2SeO4–H2O system

    Structural Chemistry · 2012-05-05

    Vadim M. Kovrugin, Vladislav V. Gurzhiy, Sergey V. Krivovichev

    Read original paper ↗ ·

  47. Influence of the Organic Species and Oxoanion in the Synthesis of two Uranyl Sulfate Hydrates, (H3O)2[(UO2)2(SO4)3(H2O)]·7H2O and (H3O)2[(UO2)2(SO4)3(H2O)]·4H2O, and a Uranyl Selenate‐Selenite [C5H6N][(UO2)(SeO4)(HSeO3)]

    Zeitschrift für anorganische und allgemeine Chemie · 2012-08-08

    Laurent J. Jouffret, Ernest M. Wylie, Peter Carman Burns

    Read original paper ↗ ·

  48. Amine templating effect absent in uranyl sulfates synthesized with 1,4-n-butyldiamine

    Journal of Solid State Chemistry · 2012-09-05

    Laurent J. Jouffret, Ernest M. Wylie, Peter Carman Burns

    Read original paper ↗ ·

  49. Role of Hydrogen-Bonding in the Formation of Polar Achiral and Nonpolar Chiral Vanadium Selenite Frameworks

    Inorganic Chemistry · 2012-09-24

    Jacob H. Olshansky, T. Thao Tran, Kristen J. Hernandez, Mat­thias Zeller, P. Shiv Halasyamani, Joshua Schrier, Alexander J. Norquist

    Read original paper ↗ ·

  50. Crystal Chemistry of Uranium Oxides and Minerals

    Elsevier eBooks · 2013-01-01

    Sergey V. Krivovichev

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