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RESEARCH PAPER · Journal of the American Chemical Society · 2005

Highly Porous Uranyl Selenate Nanotubules

Sergey V. Krivovichev, Volker Kahlenberg, Ivan Gundarovich Tananaev, Reinhard Kaindl, Edgar Mersdorf, Boris F. Myasoedov

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Highly Porous Uranyl Selenate NanotubulesOriginalInorganic Nanotube Materials0Nanostructures in Uranium Oxocompounds1Highly Porous Uranyl Selenate Nanotubules.1Self‐Assembly of Protonated 1,12‐Dodecanediamine Molecules and Strongly Undulated Uranyl Selenate Sheets in the Structure of Amine‐Templated Uranyl Selenate: (H3O)2[C12H30N2]3[(UO2)4(SeO4)8](H2O)543Synthesis and Crystal Structure of the First Uranyl Selenite(IV)-Selenate(VI) [C5H14N][(UO2)(SeO4)(SeO2OH)]38Actinide Materials Adopt Curvature: Nanotubules and Nanospheres71Actinoidchemie mit Krümmung: Nanoröhren und Nanokugeln19Amine‐Templated Uranyl Selenates with Layered Structures. I Structural Diversity of Sheets with a U:Se ratio of 1:239Inorganic Nanotubes0Molecular Octa-Uranium Rings with Alternating Nitride and Azide Bridges224Structures and syntheses of four Np5+ sulfate chain structures: Divergence from U6+ crystal chemistry39U6+ MINERALS AND INORGANIC COMPOUNDS: INSIGHTS INTO AN EXPANDED STRUCTURAL HIERARCHY OF CRYSTAL STRUCTURES627References0Synthesis and Stabilization of Nanoparticles6The vitality of uranium molecular chemistry at the dawn of the XXIst century314Extended networks, porous sheets, and chiral frameworks. Thorium materials containing mixed geometry anions: Structures and properties of Th(SeO3)(SeO4), Th(IO3)2(SeO4)(H2O)3·H2O, and Th(CrO4)(IO3)244Expanding the Crystal Chemistry of Actinyl Peroxides: Open Sheets of Uranyl Polyhedra in Na5[(UO2)3(O2)4(OH)3](H2O)1333Topology of inorganic complexes as a function of amine molecular structure in layered uranyl selenates37Na2Li8[(UO2)11O12(WO5)2]: Three Different Uranyl‐Ion Coordination Geometries and Cation–Cation Interactions71Na2Li8[(UO2)11O12(WO5)2]: Three Different Uranyl‐Ion Coordination Geometries and Cation–Cation Interactions17Nanostructured actinide compounds36Geometric isomerism of layered complexes of uranyl selenates: Synthesis and structure of (H3O)[C5H14N]2[(UO2)3(SeO4)4(HSeO4)(H2O)] and (H3O)[C5H14N]2[(UO2)3(SeO4)4(HSeO4)(H2O)](H2O)26Actinyl chemistry at the Centre for Radiochemistry Research7Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates23Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)26Crystal chemistry of uranium oxocompounds: an overview21Nanostructured actinide compounds: an introduction3Risk factors for anastomotic leakage after resection for rectal cancer.29New Organically Templated Gallium and Indium Selenites or Selenates with One-, Two-, and Three-Dimensional Structures18Selenium Oxoanion Compounds of Palladium(II)25Syntheses, crystal structures and photoluminescence properties of three novel organically bonded indium selenates or selenites27An Ordered Assembly of Filled Nanoscale Tubules of Europium Seleno-silicate in the Crystal Structure of a Quaternary Compound17Charge-density matching in organic–inorganic uranyl compounds25Structure Determination and Infrared Spectroscopy of K(UO2)(SO4)(OH)(H2O) and K(UO2)(SO4)(OH)20One-Dimensional Array of Two- and Three-Center Cation−Cation Bonds in the Structure of Li4[(UO2)10O10(Mo2O8)]63Luminescent Organically Templated Lanthanide Oxalate–Selenate Hybrids6One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands32A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds90A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds11Crystal Chemistry of Selenates with Mineral-Like Structures: V. Crystal Structures of (H 3 O) 2 ((UO 2 )(SeO 4 ) 2 (H 2 O))(H 2 O) 2 and (H 3 O) 2 ((UO 2 )(SeO 4 ) 2 (H 2 O))(H 2 O), New Compounds0The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies26Two uranyl-organic frameworks with formic acid. A novel example of a uranyl-based nanotubular assemblage41Preparation, Structures, and Photocatalytic Properties of Three New Uranyl−Organic Assembly Compounds218Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif31Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif9Synthesis, crystal structure and photoelectric property of Mn(II/IV) coordination complexes21An Open-Framework Thorium Sulfate Hydrate with 11.5 Å Voids42Crystal structure of [CH3NH3][(UO2)(H2AsO4)3]17Synthesis, structure determination, and infrared spectroscopy of (NpO2)2(SO4)(H2O)4: Prevalence of cation–cation interactions and cationic nets in neptunyl sulfate compounds21Syntheses, structures, characterizations and charge-density matching of novel amino-templated uranyl selenates45Crystal chemistry of selenates with mineral-like structures: V. Crystal structures of (H3O)2[(UO2)(SeO4)2(H2O)](H2O)2 and (H3O)2[(UO2)(SeO4)2(H2O)](H2O), new compounds with rhomboclase and goldichite topology8NEPTUNYL COMPOUNDS: POLYHEDRON GEOMETRIES, BOND-VALENCE PARAMETERS, AND STRUCTURAL HIERARCHY77Novel layered uranyl arsenates, Ag6[(UO2)2(As2O7)(As4O13)] and AI6[(UO2)2(AsO4)2(As2O7)] (AI–Ag and Na): first observation of a linear As4O136− anion and structure type evolution25Synthesis of Thermally Stable Extra-Large Pore Crystalline Materials: A Uranyl Germanate with 12-Ring Channels41Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Solid-state selenium-77 NMR51Recent Progress in the Study of Inorganic Nanotubes and Fullerene-Like Structures104Amine-templated uranyl selenates with chiral [(UO2)2(SeO4)3(H2O)]2– layers: topology, isomerism, structural relationships31Crystal chemistry of anhydrous Li uranyl phosphates and arsenates. II. Tubular fragments and cation–cation interactions in the 3D framework structures of Li6[(UO2)12(PO4)8(P4O13)], Li5[(UO2)13(AsO4)9(As2O7)], Li[(UO2)4(AsO4)3] and Li3[(UO2)7(AsO4)5O)]38A Nanosized Uranyl Camphorate Cage and its Use as a Building Unit in a Metal−Organic Framework47Crown and Bowl-Shaped Clusters of Uranyl Polyhedra62Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?18A new series of pillared uranyl-vanadates based on uranophane-type sheets in the uranium-vanadium-linear alkyl diamine systems28Uranyl selenates with organic templates: Principles of structure and characteristics of self-organization23Cubic and rhombohedral heterobimetallic networks constructed from uranium, transition metals, and phosphonoacetate: new methods for constructing porous materials113Uranyl peroxide closed clusters containing topological squares52Partially ordered organic-inorganic nanocomposites in the system UO2SeO4-H2O-NH3(CH2)9NH36Supramolecular templates for the synthesis of new nanostructured uranyl compounds: Crystal structure of [NH3(CH2)9NH3][(UO2)(SeO4)(SeO2OH)](NO3)10Syntheses, structures, and IR spectroscopic characterization of new uranyl sulfate/selenate 1D-chain, 2D-sheet and 3D-framework49Actinyl Compounds with Hexavalent Elements (S, Cr, Se, Mo) – Structural Diversity, Nanoscale Chemistry, and Cellular Automata Modeling69Receptor properties of nanoporous structures based on β-cyclodextrin2Crystal Chemistry of the Potassium and Rubidium Uranyl Borate Families Derived from Boric Acid Fluxes49New three-dimensional inorganic frameworks based on the uranophane-type sheet in monoamine templated uranyl-vanadates28Uranium Pyrophosphate/Methylenediphosphonate Polyoxometalate Cage Clusters114Differential Ion Exchange in Elliptical Uranyl Diphosphonate Nanotubules106Differential Ion Exchange in Elliptical Uranyl Diphosphonate Nanotubules9Advances in actinide solid-state and coordination chemistry37Inorganic Nanotubes beyond Cylindrical Matter5Uranyl−Organic Assemblies with Acetate-Bearing Phenyl- and Cyclohexyl-Based Ligands45Inorganic Nanotubes5Inorganic Nanotubes beyond Cylindrical Matter2Nanoscale Chemistry of Uranyl Selenates1Revisiting the Uranyl-phthalate System: Isolation and Crystal Structures of Two Types of Uranyl−Organic Frameworks (UOF)78Exploring the Uranyl Organometallic Chemistry: From Single to Double Uranium−Carbon Bonds135Cation–Cation Interactions: Crystal Structures of Neptunyl(V) Selenate Hydrates, (NpO2)2(SeO4)(H2O)n (n = 1, 2, and 4)36Structural Complexity of Barium Uranyl Arsenates: Synthesis, Structure, and Topology of Ba4[(UO2)2(As2O7)3], Ba3[(UO2)2(AsO4)2(As2O7)], and Ba5Ca[(UO2)8(AsO4)4O8]11Inorganic Nanotubes0Tubular chains in the structures of natural and synthetic silicates17Metal-Controlled Assembly of Uranyl Diphosphonates toward the Design of Functional Uranyl Nanotubules77Synthesis and characterization of uranyl chromate sheet compounds containing edge-sharing dimers of uranyl pentagonal bipyramids19Unprecedented Bidentate Coordination of the Uranyl Cation by the Chromate Anion in the Structure of [(CH3)2CHNH3]2[UO2(CrO4)2]21Inorganic Nanotubes0Complex clover cross-sectioned nanotubules exist in the structure of the first uranium borate phosphate28Polytypism and oxo-tungstate polyhedra polymerization in novel complex uranyl tungstates13Synthesis and structure of a new uranyl selenate complex with 1-butylamine [CH3(CH2)3NH3](H5O2)[(UO2)2(SeO4)3(H2O)]6Unprecedented layer topology in the crystal structure of a new organically templated uranyl selenite-selenate19Synthesis, characterization, and crystal structures of uranyl compounds containing mixed chromium oxidation states7Structural topology and dimensional reduction in uranyl oxysalts: eight novel phases in the methylamine–(UO2)(NO3)2–H2SeO4–H2O system24A novel organic–inorganic hybrid 3D framework based on neodymium oxalate–selenites [Nd2(SeO3)2(C2O4)(H2O)2]·2H2O6Nanoscale Hemispheres in Novel Mixed-Valent Uranyl Chromate(V,VI), (C3NH10)10[(UO2)13(Cr125+O42)(Cr6+O4)6(H2O)6](H2O)618Amine templating effect absent in uranyl sulfates synthesized with 1,4-n-butyldiamine14A calorimetric and thermodynamic investigation of potassium uranyl tungstate K2[(UO2)(W2O8)]7Na1.515EuGeS4, A Three-Dimensional Crystalline Assembly of Empty Nanotubules Constructed with Europium(II/III) Mixed Valence Ions18Environmental Speciation of Actinides423New Reactivity of the Uranyl(VI) Ion116Cellular automata as models of inorganic structures self-assembly (Illustrated by uranyl selenate)4Crystal Chemistry of Uranium Oxides and Minerals27Synthesis and Stabilization of Nanoparticles2Voltammetric Study of Uranyl–Selenium Interactions. Part 2. Uranyl(V) Selenate Complex2Actinide Colloids and Particles of Environmental Concern179Reactivity of U3+ Metallocene Allyl Complexes Leads to a Nanometer-Sized Uranium Carbonate, [(C5Me5)2U]6(μ-κ1:κ2-CO3)623The crystal chemistry of uranium carboxylates394Growth of Uranyl Hydroxide Nanowires and Nanotubes by the Electrodeposition Method and Their Transformation to One‐Dimensional U3O8 Nanostructures16Symmetry reduction in uranyl compounds with [(UO2)2(TO4)3]2- (T = Se, S, Mo) layers: crystal structures of the new guanidinium uranyl selenate and methylammonium uranyl sulfate17A Highly Adjustable Coordination System: Nanotubular and Molecular Cage Species in Uranyl Ion Complexes with Kemp’s Triacid46Increasing Complexity in the Uranyl Ion–Kemp’s Triacid System: From One- and Two-Dimensional Polymers to Uranyl–Copper(II) Dodeca- and Hexadecanuclear Species47Uranyl Ion Complexes with all-cis-1,3,5-Cyclohexanetricarboxylate: Unexpected Framework and Nanotubular Assemblies55Template‐Free Synthesis and Mechanistic Study of Porous Three‐Dimensional Hierarchical Uranium‐Containing and Uranium Oxide Microspheres26The First Family of Actinide Carboxyphosphinates: Two‐ and Three‐Dimensional Uranyl Coordination Polymers27A family of uranyl-aromatic dicarboxylate (pht-, ipa-, tpa-) framework hybrid materials: photoluminescence, surface photovoltage and dye adsorption31Further Insight into Uranium and Thorium Metaphosphate Chemistry and the Effect of Nd3+ Incorporation into Uranium(IV) Metaphosphate12Topologically and geometrically flexible structural units in seven new organically templated uranyl selenates and selenite–selenates22Structural Features in Metal–Organic Nanotube Crystals That Influence Stability and Solvent Uptake33Semiconductive Nanotube Array Constructed from Giant [PbII18I54(I2)9] Wheel Clusters104Semiconductive Nanotube Array Constructed from Giant [PbII18I54(I2)9] Wheel Clusters20Uranyl Complexes with (Meth)acrylate Anions10Inorganic Nanotube Materials1A Revised and Expanded Structure Hierarchy of Natural and Synthetic Hexavalent Uranium Compounds172Nanomaterials in nuclear engineering and radioecology3Pathways for synthesis of new selenium-containing oxo-compounds: Chemical vapor transport reactions, hydrothermal techniques and evaporation method19Synthesis and crystal structure analysis of uranyl triple acetates12Inorganic Synthesis of Actinides3Recent advances in structural studies of heterometallic uranyl-containing coordination polymers and polynuclear closed species93Coordination Polymers and Cage-Containing Frameworks in Uranyl Ion Complexes with rac- and (1R,2R)-trans-1,2-Cyclohexanedicarboxylates: Consequences of Chirality38Variations on the Honeycomb Topology: From Triangular- and Square-Grooved Networks to Tubular Assemblies in Uranyl Tricarballylate Complexes34Tetrahedral and Cuboidal Clusters in Complexes of Uranyl and Alkali or Alkaline-Earth Metal Ions with rac- and (1R,2R)-trans-1,2-Cyclohexanedicarboxylate29Morphotropy in alkaline uranyl methacrylate complexes9Probing the Influence of Acidity and Temperature to Th(IV) on Hydrolysis, Nucleation, and Structural Topology16A Large Family of Centrosymmetric and Chiral f-Element-Bearing Iodate Selenates Exhibiting Coordination Number and Dimensional Reductions26Uranyl Sulfate Nanotubules Templated by N-phenylglycine16Closed Uranyl–Dicarboxylate Oligomers: A Tetranuclear Metallatricycle with Uranyl Bridgeheads and 1,3-Adamantanediacetate Linkers22

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  2. Nanostructures in Uranium Oxocompounds

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  4. Self‐Assembly of Protonated 1,12‐Dodecanediamine Molecules and Strongly Undulated Uranyl Selenate Sheets in the Structure of Amine‐Templated Uranyl Selenate: (H3O)2[C12H30N2]3[(UO2)4(SeO4)8](H2O)5

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  5. Synthesis and Crystal Structure of the First Uranyl Selenite(IV)-Selenate(VI) [C5H14N][(UO2)(SeO4)(SeO2OH)]

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  6. Actinide Materials Adopt Curvature: Nanotubules and Nanospheres

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  7. Actinoidchemie mit Krümmung: Nanoröhren und Nanokugeln

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  8. Amine‐Templated Uranyl Selenates with Layered Structures. I Structural Diversity of Sheets with a U:Se ratio of 1:2

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  9. Inorganic Nanotubes

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  10. Molecular Octa-Uranium Rings with Alternating Nitride and Azide Bridges

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  11. Structures and syntheses of four Np5+ sulfate chain structures: Divergence from U6+ crystal chemistry

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  12. U6+ MINERALS AND INORGANIC COMPOUNDS: INSIGHTS INTO AN EXPANDED STRUCTURAL HIERARCHY OF CRYSTAL STRUCTURES

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  13. References

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  14. Synthesis and Stabilization of Nanoparticles

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  15. The vitality of uranium molecular chemistry at the dawn of the XXIst century

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  16. Extended networks, porous sheets, and chiral frameworks. Thorium materials containing mixed geometry anions: Structures and properties of Th(SeO3)(SeO4), Th(IO3)2(SeO4)(H2O)3·H2O, and Th(CrO4)(IO3)2

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  17. Expanding the Crystal Chemistry of Actinyl Peroxides: Open Sheets of Uranyl Polyhedra in Na5[(UO2)3(O2)4(OH)3](H2O)13

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  18. Topology of inorganic complexes as a function of amine molecular structure in layered uranyl selenates

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  19. Na2Li8[(UO2)11O12(WO5)2]: Three Different Uranyl‐Ion Coordination Geometries and Cation–Cation Interactions

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  20. Na2Li8[(UO2)11O12(WO5)2]: Three Different Uranyl‐Ion Coordination Geometries and Cation–Cation Interactions

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  21. Nanostructured actinide compounds

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  22. Geometric isomerism of layered complexes of uranyl selenates: Synthesis and structure of (H3O)[C5H14N]2[(UO2)3(SeO4)4(HSeO4)(H2O)] and (H3O)[C5H14N]2[(UO2)3(SeO4)4(HSeO4)(H2O)](H2O)

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  24. Hydrothermal synthesis, structure and thermal stability of diamine templated layered uranyl-vanadates

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  25. Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)

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  26. Crystal chemistry of uranium oxocompounds: an overview

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  27. Nanostructured actinide compounds: an introduction

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  32. An Ordered Assembly of Filled Nanoscale Tubules of Europium Seleno-silicate in the Crystal Structure of a Quaternary Compound

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  33. Charge-density matching in organic–inorganic uranyl compounds

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  34. Structure Determination and Infrared Spectroscopy of K(UO2)(SO4)(OH)(H2O) and K(UO2)(SO4)(OH)

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  35. One-Dimensional Array of Two- and Three-Center Cation−Cation Bonds in the Structure of Li4[(UO2)10O10(Mo2O8)]

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  36. Luminescent Organically Templated Lanthanide Oxalate–Selenate Hybrids

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  37. One- and Two-Dimensional Silver and Zinc Uranyl Phosphates Containing Bipyridyl Ligands

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  38. A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds

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  39. A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds

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  40. Crystal Chemistry of Selenates with Mineral-Like Structures: V. Crystal Structures of (H 3 O) 2 ((UO 2 )(SeO 4 ) 2 (H 2 O))(H 2 O) 2 and (H 3 O) 2 ((UO 2 )(SeO 4 ) 2 (H 2 O))(H 2 O), New Compounds

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  41. The First Organically Templated Tetravalent Uranium Phosphates with Dimer-Structured Topologies

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  42. Two uranyl-organic frameworks with formic acid. A novel example of a uranyl-based nanotubular assemblage

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  43. Preparation, Structures, and Photocatalytic Properties of Three New Uranyl−Organic Assembly Compounds

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  44. Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif

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  45. Polyimido Uranium(IV) Clusters: Imidometalates with an M7(μ3‐N)6(μ2‐N)6 Core Analogous to the Anderson‐Type Polyoxometalate Motif

    Angewandte Chemie · 2008-06-23

    J.‐C. Berthet, P. Thuéry, M. Ephritikhine

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  46. Synthesis, crystal structure and photoelectric property of Mn(II/IV) coordination complexes

    Inorganica Chimica Acta · 2008-07-16

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  47. An Open-Framework Thorium Sulfate Hydrate with 11.5 Å Voids

    Inorganic Chemistry · 2008-09-24

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  48. Crystal structure of [CH3NH3][(UO2)(H2AsO4)3]

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  49. Synthesis, structure determination, and infrared spectroscopy of (NpO2)2(SO4)(H2O)4: Prevalence of cation–cation interactions and cationic nets in neptunyl sulfate compounds

    Journal of Solid State Chemistry · 2008-10-10

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  50. Syntheses, structures, characterizations and charge-density matching of novel amino-templated uranyl selenates

    Journal of Solid State Chemistry · 2008-11-21

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