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RESEARCH PAPER · Inorganic Chemistry · 2019

Molten Alkali Halide Flux Growth of an Extensive Family of Noncentrosymmetric Rare Earth Sulfides: Structure and Magnetic and Optical (SHG) Properties

Mohammad Usman, Mark D. Smith, Gregory W. Morrison, Vladislav V. Klepov, Weiguo Zhang, P. Shiv Halasyamani, Hans‐Conrad zur Loye

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Molten Alkali Halide Flux Growth of an Extensive Family of Noncentrosymmetric Rare Earth Sulfides: Structure and Magnetic and Optical (SHG) PropertiesOriginalOne-Dimensional Quaternary and Penternary Alkali Rare Earth Thiophosphates Obtained via Alkali Halide Flux Crystal Growth12Two Rare‐Earth Molecular Ferroelectrics with High Curie Temperatures, Large Spontaneous Polarization, Switchable Second Harmonic Generation Effects, and Strong Photoluminescence28New insights on the structural and optical-vibration properties of noncentrosymmetric lanthanides pyrogermanates8Frustrated Magnetism in Triangular Lattice TlYbS2 Crystals Grown via Molten Flux14Preparation and characterization of a novel erbium(III)-mercury(II) compound with green upconversion photoluminescence0Preparation, photoluminescence and semiconductive band gap of a gadolinium compound3Rb2Co1.85Ge1.15O6: The First Quaternary, Noncentrosymmetric Rubidium Cobalt Germanate3Two Mixed-Anion Units of [GeOSe3] and [GeO3S] Originating from Partial Isovalent Anion Substitution and Inducing Moderate Second Harmonic Generation Response and Large Birefringence55Synthesis and characterization of a novel Europium(III) complex with a one-dimensional chain-like structure3Lanthanide thioborates, an emerging class of nonlinear optical materials, efficiently synthesized using the boron–chalcogen mixture method23Chalcogen dependent metal vacancies and disorder in Ba2Ln1−Mn2−S5 and Ba2−Ln1−Mn2−Se5 (Ln = Pr, Nd, and Gd) structures5Homologous Alkali Metal Copper Rare-Earth Chalcogenides A 2 Cu 2 n Ln 4 Q 7+ n ( n = 1, 2, 3)16Ln2(SeO3)2(SO4)(H2O)2 (Ln=Sm, Dy, Yb): A Mixed‐Ligand Pathway to New Lanthanide(III) Multifunctional Materials Featuring Nonlinear Optical and Magnetic Anisotropy Properties36Ln2(SeO3)2(SO4)(H2O)2 (Ln=Sm, Dy, Yb): A Mixed‐Ligand Pathway to New Lanthanide(III) Multifunctional Materials Featuring Nonlinear Optical and Magnetic Anisotropy Properties2DOUBLE YTTRIUM THIOSILICATES AYSiS4 (A = Rb, Cs): SYNTHESIS, STRUCTURE, OPTICAL PROPERTIES4LaAeAl 3 S 7 (Ae = Ca, Sr): Cairo pentagonal layered thioaluminates achieving a good balance between a strong second harmonic generation response and a wide bandgap23Mg 2 Pb 2 Si 2 O 7 F 2 : a new lead-containing alkali earth metal silicate fluoride with a short cutoff edge2LnLiSiS4 (Ln = La and Ce): Promising infrared nonlinear optical materials designed by aliovalent substitution from SrCdSiS437Crystal Structures and Property Measurements of Rare Earth Magnesium Thiosilicates Synthesized via Flux Crystal Growth Utilizing the Boron Chalcogen Mixture (BCM) Method15Emergence of a Lanthanide Chalcogenide as an Ideal Scintillator for a Flexible X‐ray Detector37Emergence of a Lanthanide Chalcogenide as an Ideal Scintillator for a Flexible X‐ray Detector9Ca2Ln(BS3)(SiS4) (Ln = La, Ce, and Gd): Mixed Metal Thioborate‐Thiosilicates as Well‐Performed Infrared Nonlinear Optical Materials29Impurity, host and defect-related luminescence of CsLaSiS4 thiosilicate crystals doped with Ce3+ ions8Alkali halide flux synthesis, crystal structure, and photoelectric response of quaternary thiosilicates K 3 Ga 3 Si 7 S 20 and K 2 ZnSi 3 S 81Chemical modulation of A I RE III C IV QVI4 family compounds for band gap and optical anisotropy enhancement16Rare-earth-based chalcogenides and their derivatives: an encouraging IR nonlinear optical material candidate70Luminescence of CsLa1-хCeхSiS4 thiosilicate solid solution: From STE to Ce3+ emission4Crystal Growth of Quaternary AkRE 2 Si 2 S 8 (Ak = Ca and Sr; RE = La–Tb) Thiosilicates Using Flux-Assisted Boron Chalcogen Mixture Method: Exploring X-ray Scintillation, Luminescence, and Magnetic Properties11LiLnGeS 4 (Ln=La−Nd): Designing High Performance Infrared Nonlinear Optical Sulfides through “Band Reformation of AGS”37LiLnGeS 4 (Ln=La−Nd): Designing High Performance Infrared Nonlinear Optical Sulfides through “Band Reformation of AGS”5Hydrothermal syntheses, structures and photophysical properties of two lanthanide isonicotinic acid complexes3Luminescence and energy transfer in CsLaSiS4 single crystals doped with Tb3+ and Ce3+ ions8Synthesis of a series of rare-earth-based multi-anion chalcogenide iodides RE 3 Si 2 Se x S 8− x I (RE = La, Ce, Pr, and Nd) using the flux-assisted boron–chalcogen mixture method14KYSiSe 4 : A Rare-Earth Selenide Infrared Nonlinear Optical Crystal with Wide Infrared Transparency and Well-Balanced E g and SHG Response9Preparation, structure and properties of a novel 4 f -5 d complex with green upconversion photoluminescence0Ultrabroadband-Emissive Lanthanide Chalcogenide for X-ray Scintillation0Crystal Growth of Quaternary RE 2 EuSi 2 S 8 ( RE = Ce–Nd, Sm, Gd, Tb) Using Flux-Assisted Boron Chalcogen Mixture (BCM) Method: Investigation of Magnetic and Luminescence Properties4Indirect-to-direct bandgap transition in CsRESiS 4 (RE = Sc, Y, and Lanthanides) through intrinsic charge-transfer transition (CTT) behaviour1Multifunctional Lanthanide Molecular Ferroelectrics [ R / S -H 2 MPPA][Ln(btfa) 4 ] 2 Constructed by Hydrogen Bond Linking Functional Blocks3Flux-Assisted Growth and Characterization of Noncentrosymmetric Quaternary Rare-Earth Selenides CsRESiSe 4 (RE = La, Pr, Nd, Sm, Gd, Tb): Crystal Structure, Magnetism, and Theoretical Studies0Synthesis and Characterization of RE 3 LiSiSe 7 (RE = La–Nd, Sm, Gd, and Tb) Exhibiting Enhanced Nonlinear Optical (NLO) Properties0A Surprising Continuation of the Nonisotypic Rb 3 Ln [AsS 4 ] 2 Series: The Diverse Crystal Structures of the End‐Members with Ln = Gd–Ho0Layered RbLnGeS4 (ln = Ce, Pr, Nd, Sm, Gd): crystal structures, Rb-site disorder–order transition, and structure–property correlations0Coupled Interlayer–Intralayer Interactions for Promising Optoelectronic Response in ACeSiX4 (A = K, Rb, Cs; X = S, Se)0The use of nanotechnology for oil recovery at low temperatures0Synthesis, structure, optical properties, and magnetic behavior of layered heavy rare-earth thiogermanates CsDyGeS4 and CsErGeS403 d Transition Metal Contribution to the Magnetic Behavior of Chiral Y6 M x Si2S14 and Tb6CoSi2S140

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  1. One-Dimensional Quaternary and Penternary Alkali Rare Earth Thiophosphates Obtained via Alkali Halide Flux Crystal Growth

    Crystal Growth & Design · 2019-08-21

    Mohammad Usman, Mark D. Smith, Vladislav V. Klepov, Hans‐Conrad zur Loye

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  2. Two Rare‐Earth Molecular Ferroelectrics with High Curie Temperatures, Large Spontaneous Polarization, Switchable Second Harmonic Generation Effects, and Strong Photoluminescence

    Chemistry - A European Journal · 2020-02-10

    Kang Yang, Chang‐Shan Yang, Xing‐Xian Dong, Yu‐Hui Tan, Yun‐Zhi Tang, Wen‐Juan Wei

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  3. New insights on the structural and optical-vibration properties of noncentrosymmetric lanthanides pyrogermanates

    Ceramics International · 2020-02-14

    Guilherme M. Martins, Cristiano Fantini, Leandro M. Malard, Pâmela O. Coelho, Roberto Luiz Moreira, Anderson Dias

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  4. Frustrated Magnetism in Triangular Lattice TlYbS2 Crystals Grown via Molten Flux

    Frontiers in Chemistry · 2020-02-26

    Timothy Ferreira, Jie Xing, Liurukara D. Sanjeewa, Athena S. Sefat

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  5. Preparation and characterization of a novel erbium(III)-mercury(II) compound with green upconversion photoluminescence

    Inorganic and Nano-Metal Chemistry · 2020-05-25

    Wen‐Tong Chen

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  6. Preparation, photoluminescence and semiconductive band gap of a gadolinium compound

    Inorganic and Nano-Metal Chemistry · 2020-07-17

    Wen‐Tong Chen

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  7. Rb2Co1.85Ge1.15O6: The First Quaternary, Noncentrosymmetric Rubidium Cobalt Germanate

    Journal of Chemical Crystallography · 2020-10-24

    Mohammad Usman, Mark D. Smith, Hans‐Conrad zur Loye

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  8. Two Mixed-Anion Units of [GeOSe3] and [GeO3S] Originating from Partial Isovalent Anion Substitution and Inducing Moderate Second Harmonic Generation Response and Large Birefringence

    Inorganic Chemistry · 2020-10-26

    Wenhao Xing, Pan Fang, Naizheng Wang, Zhuang Li, Zheshuai Lin, Jiyong Yao, Wenlong Yin, Bin Kang

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  9. Synthesis and characterization of a novel Europium(III) complex with a one-dimensional chain-like structure

    Journal of Solid State Chemistry · 2020-11-01

    Wen‐Tong Chen

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  10. Lanthanide thioborates, an emerging class of nonlinear optical materials, efficiently synthesized using the boron–chalcogen mixture method

    Chemical Communications · 2022-01-01

    Logan S. Breton, Gregory W. Morrison, Matthew R. Lacroix, P. Shiv Halasyamani, Hans‐Conrad zur Loye

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  11. Chalcogen dependent metal vacancies and disorder in Ba2Ln1−Mn2−S5 and Ba2−Ln1−Mn2−Se5 (Ln = Pr, Nd, and Gd) structures

    Journal of Alloys and Compounds · 2022-01-05

    Gopabandhu Panigrahi, Subhendu Jana, Mohd Ishtiyak, Bikash Tripathy, Sairam K. Malladi, Manish K. Niranjan, Jai Prakash

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  12. Homologous Alkali Metal Copper Rare-Earth Chalcogenides A 2 Cu 2 n Ln 4 Q 7+ n ( n = 1, 2, 3)

    Chemistry of Materials · 2022-03-21

    Craig C. Laing, Jiahong Shen, Michael A. Quintero, Benjamin E. Weiss, Yi Xia, Zhi Li, Jiangang He, Chris M. Wolverton, Mercouri G. Kanatzidis

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  13. Ln2(SeO3)2(SO4)(H2O)2 (Ln=Sm, Dy, Yb): A Mixed‐Ligand Pathway to New Lanthanide(III) Multifunctional Materials Featuring Nonlinear Optical and Magnetic Anisotropy Properties

    Angewandte Chemie International Edition · 2022-10-04

    Ebube E. Oyeka, Michal Jerzy Winiarski, Hanna Świątek, Wyatt L. Balliew, Colin D. McMillen, Mingli Liang, Maurice Sorolla, T. Thao Tran

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  14. Ln2(SeO3)2(SO4)(H2O)2 (Ln=Sm, Dy, Yb): A Mixed‐Ligand Pathway to New Lanthanide(III) Multifunctional Materials Featuring Nonlinear Optical and Magnetic Anisotropy Properties

    Angewandte Chemie · 2022-10-04

    Ebube E. Oyeka, Michal Jerzy Winiarski, Hanna Świątek, Wyatt L. Balliew, Colin D. McMillen, Mingli Liang, Maurice Sorolla, T. Thao Tran

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  15. DOUBLE YTTRIUM THIOSILICATES AYSiS4 (A = Rb, Cs): SYNTHESIS, STRUCTURE, OPTICAL PROPERTIES

    Journal of Structural Chemistry · 2022-12-01

    М.С. Тарасенко, R. V. Duritsyn, D. A. Potapov, Natalia V. Kuratieva, Alexey A. Ryadun, Н.Г. Наумов

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  16. LaAeAl 3 S 7 (Ae = Ca, Sr): Cairo pentagonal layered thioaluminates achieving a good balance between a strong second harmonic generation response and a wide bandgap

    Inorganic Chemistry Frontiers · 2023-01-01

    Jingjing Xu, Kui Wu, Bingbing Zhang, Haohai Yu, Huaijin Zhang

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  17. Mg 2 Pb 2 Si 2 O 7 F 2 : a new lead-containing alkali earth metal silicate fluoride with a short cutoff edge

    New Journal of Chemistry · 2023-01-01

    Zhiyuan Zhang, Lihan Deng, Die Xu, Mei Ying Hu, Zhencheng Wu, Xin Su, Yineng Huang

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  18. LnLiSiS4 (Ln = La and Ce): Promising infrared nonlinear optical materials designed by aliovalent substitution from SrCdSiS4

    Materials Today Physics · 2023-01-21

    Ya‐Xiang Han, Chun‐Li Hu, Bingxuan Li, Jiang‐Gao Mao

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  19. Crystal Structures and Property Measurements of Rare Earth Magnesium Thiosilicates Synthesized via Flux Crystal Growth Utilizing the Boron Chalcogen Mixture (BCM) Method

    Inorganic Chemistry · 2023-05-03

    Adam A. King, Logan S. Breton, Gregory W. Morrison, Mark D. Smith, Mingli Liang, P. Shiv Halasyamani, Hans‐Conrad zur Loye

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  20. Emergence of a Lanthanide Chalcogenide as an Ideal Scintillator for a Flexible X‐ray Detector

    Angewandte Chemie International Edition · 2023-05-30

    Liangwei Yang, Zhenyu Li, Linwei He, Jiayu Sun, Junren Wang, Yumin Wang, Yumin Wang, Ming Li, Zibin Zhu, Xing Dai, Shu‐Xian Hu, Fuwan Zhai, Qian Yang, Ye Tao, Zhifang Chai, Shuao Wang, Yaxing Wang, Yaxing Wang

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  21. Emergence of a Lanthanide Chalcogenide as an Ideal Scintillator for a Flexible X‐ray Detector

    Angewandte Chemie · 2023-05-30

    Liangwei Yang, Zhenyu Li, Linwei He, Jiayu Sun, Junren Wang, Yumin Wang, Yumin Wang, Ming Li, Zibin Zhu, Xing Dai, Shu‐Xian Hu, Fuwan Zhai, Qian Yang, Ye Tao, Zhifang Chai, Shuao Wang, Yaxing Wang, Yaxing Wang

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  22. Ca2Ln(BS3)(SiS4) (Ln = La, Ce, and Gd): Mixed Metal Thioborate‐Thiosilicates as Well‐Performed Infrared Nonlinear Optical Materials

    Small · 2023-09-19

    Ya‐Xiang Han, Chun‐Li Hu, Jiang‐Gao Mao

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  23. Impurity, host and defect-related luminescence of CsLaSiS4 thiosilicate crystals doped with Ce3+ ions

    Journal of Luminescence · 2023-09-25

    Vladimir A. Pustovarov, М.С. Тарасенко, Dmitry Tavrunov, Н.Г. Наумов

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  24. Alkali halide flux synthesis, crystal structure, and photoelectric response of quaternary thiosilicates K 3 Ga 3 Si 7 S 20 and K 2 ZnSi 3 S 8

    CrystEngComm · 2024-01-01

    Jia-Ting Liu, Abdusalam Ablez, Qianqian Hu, Jun-Hao Tang, Chuan Lv, Lu Yang, Mei‐Ling Feng, Xiao‐Ying Huang

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  25. Chemical modulation of A I RE III C IV QVI4 family compounds for band gap and optical anisotropy enhancement

    Inorganic Chemistry Frontiers · 2024-01-01

    Hongshan Wang, Xueting Pan, Shilie Pan, Junjie Li

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  26. Rare-earth-based chalcogenides and their derivatives: an encouraging IR nonlinear optical material candidate

    Chemical Science · 2024-01-01

    Ping Feng, Jiaxiang Zhang, Mao‐Yin Ran, Xin‐Tao Wu, Hua Lin, Qi‐Long Zhu

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  27. Luminescence of CsLa1-хCeхSiS4 thiosilicate solid solution: From STE to Ce3+ emission

    Journal of Luminescence · 2024-05-13

    Vladimir A. Pustovarov, Dmitry Tavrunov, Maxim R. Ryzhikov, М.С. Тарасенко, Н.Г. Наумов

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  28. Crystal Growth of Quaternary AkRE 2 Si 2 S 8 (Ak = Ca and Sr; RE = La–Tb) Thiosilicates Using Flux-Assisted Boron Chalcogen Mixture Method: Exploring X-ray Scintillation, Luminescence, and Magnetic Properties

    Inorganic Chemistry · 2024-06-29

    Gopabandhu Panigrahi, Anna A. Berseneva, Gregory W. Morrison, Adam A. King, Robin L. Conner, Luiz Gustavo Jacobsohn, Hans‐Conrad zur Loye

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  29. LiLnGeS 4 (Ln=La−Nd): Designing High Performance Infrared Nonlinear Optical Sulfides through “Band Reformation of AGS”

    Angewandte Chemie International Edition · 2024-09-21

    Qianqian Liu, Xin Liu, Mei-Ze Li, Rui‐Xi Wang, Bingxuan Li, Li‐Ming Wu, Ling Chen

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  30. LiLnGeS 4 (Ln=La−Nd): Designing High Performance Infrared Nonlinear Optical Sulfides through “Band Reformation of AGS”

    Angewandte Chemie · 2024-09-21

    Qianqian Liu, Xin Liu, Mei-Ze Li, Rui‐Xi Wang, Bingxuan Li, Li‐Ming Wu, Ling Chen

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  31. Hydrothermal syntheses, structures and photophysical properties of two lanthanide isonicotinic acid complexes

    Molecular Crystals and Liquid Crystals · 2024-09-23

    Qiuyan Luo, Hao-Dong Liu, Xi-Yu Shao, Yu-Yue Xu, Cheng Liu, Sheng-Ping Dai, Changwang Pan, Wen‐Tong Chen

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  32. Luminescence and energy transfer in CsLaSiS4 single crystals doped with Tb3+ and Ce3+ ions

    Optical Materials · 2024-11-22

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  33. Synthesis of a series of rare-earth-based multi-anion chalcogenide iodides RE 3 Si 2 Se x S 8− x I (RE = La, Ce, Pr, and Nd) using the flux-assisted boron–chalcogen mixture method

    Dalton Transactions · 2025-01-01

    Gopabandhu Panigrahi, Habiba Binte Kashem, Gregory W. Morrison, Hans‐Conrad zur Loye

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  34. KYSiSe 4 : A Rare-Earth Selenide Infrared Nonlinear Optical Crystal with Wide Infrared Transparency and Well-Balanced E g and SHG Response

    Inorganic Chemistry · 2025-06-16

    Haixia Wang, Wangfei Che, Hongbo Zhang, Xinfeng Guo, Limei Xiao, Yakun Tang, Guangmao Li

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  35. Preparation, structure and properties of a novel 4 f -5 d complex with green upconversion photoluminescence

    Molecular Crystals and Liquid Crystals · 2025-07-23

    Xi-Yu Shao, Hao-Dong Liu, Wei Wang, Cheng Liu, Changwang Pan, Wen‐Tong Chen

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  36. Ultrabroadband-Emissive Lanthanide Chalcogenide for X-ray Scintillation

    Inorganic Chemistry · 2025-12-04

    Liangwei Yang, Siyan Huang, Yumin Wang, Yumin Wang, Ming Li, Zhidong Wu, Tao Tang, Mengmeng Zhao, Yunpu Zhang, Zhengjun Liu, Hailong Zhang, Junren Wang, Zhifang Chai, Shuao Wang, Yaxing Wang, Yaxing Wang

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  37. Crystal Growth of Quaternary RE 2 EuSi 2 S 8 ( RE = Ce–Nd, Sm, Gd, Tb) Using Flux-Assisted Boron Chalcogen Mixture (BCM) Method: Investigation of Magnetic and Luminescence Properties

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    Habiba Binte Kashem, Hope Eden Smith, Abdullah Al Muhit, Hans‐Conrad zur Loye

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  38. Indirect-to-direct bandgap transition in CsRESiS 4 (RE = Sc, Y, and Lanthanides) through intrinsic charge-transfer transition (CTT) behaviour

    Journal of Materials Chemistry C · 2026-01-01

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  39. Multifunctional Lanthanide Molecular Ferroelectrics [ R / S -H 2 MPPA][Ln(btfa) 4 ] 2 Constructed by Hydrogen Bond Linking Functional Blocks

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  40. Flux-Assisted Growth and Characterization of Noncentrosymmetric Quaternary Rare-Earth Selenides CsRESiSe 4 (RE = La, Pr, Nd, Sm, Gd, Tb): Crystal Structure, Magnetism, and Theoretical Studies

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  41. Synthesis and Characterization of RE 3 LiSiSe 7 (RE = La–Nd, Sm, Gd, and Tb) Exhibiting Enhanced Nonlinear Optical (NLO) Properties

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  42. A Surprising Continuation of the Nonisotypic Rb 3 Ln [AsS 4 ] 2 Series: The Diverse Crystal Structures of the End‐Members with Ln = Gd–Ho

    Zeitschrift für anorganische und allgemeine Chemie · 2026-07-15

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  43. Layered RbLnGeS4 (ln = Ce, Pr, Nd, Sm, Gd): crystal structures, Rb-site disorder–order transition, and structure–property correlations

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    Alexander A. Sapov, М.С. Тарасенко, Natalia V. Kuratieva, Mikhail M. Syrokvashin, Alexey A. Ryadun, Dmitry Yu. Troitskii, Irina V. Yushina, Н.Г. Наумов

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  44. Coupled Interlayer–Intralayer Interactions for Promising Optoelectronic Response in ACeSiX4 (A = K, Rb, Cs; X = S, Se)

    The Journal of Physical Chemistry C · 2026-08-06

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  45. The use of nanotechnology for oil recovery at low temperatures

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  46. Synthesis, structure, optical properties, and magnetic behavior of layered heavy rare-earth thiogermanates CsDyGeS4 and CsErGeS4

    Journal of Solid State Chemistry · 2026-08-25

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  47. 3 d Transition Metal Contribution to the Magnetic Behavior of Chiral Y6 M x Si2S14 and Tb6CoSi2S14

    Chemistry of Materials · 2026-10-06

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