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RESEARCH PAPER · Inorganic Chemistry · 2002

Mixed-Metal Uranium(VI) Iodates: Hydrothermal Syntheses, Structures, and Reactivity of Rb[UO2(CrO4)(IO3)(H2O)], A2[UO2(CrO4)(IO3)2] (A = K, Rb, Cs), and K2[UO2(MoO4)(IO3)2]

Richard E. Sykora, Steven M. McDaniel, Daniel M. Wells, Thomas E. Albrecht‐Schmitt

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Mixed-Metal Uranium(VI) Iodates: Hydrothermal Syntheses, Structures, and Reactivity of Rb[UO2(CrO4)(IO3)(H2O)], A2[UO2(CrO4)(IO3)2] (A = K, Rb, Cs), and K2[UO2(MoO4)(IO3)2]Original22 New compounds and structures in the solid state2ChemInform Abstract: Mixed‐Metal Uranium(VI) Iodates: Hydrothermal Syntheses, Structures, and Reactivity of Rb[UO2(CrO4)(IO3)(H2O)], A2[UO2(CrO4)(IO3)2] (A: K, Rb, Cs), and K2[UO2(MoO4)(IO3)2].321 New compounds and structures in the solid state1Advances in Understanding of the Crystal Chemistry of Hexavalent Uranium2Structure and Bonding in Solution of Dioxouranium(VI) Oxalate Complexes: Isomers and Intramolecular Ligand Exchange68Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies17Cation−Cation Interactions in Neptunyl(V) Compounds: Hydrothermal Preparation and Structural Characterization of NpO2(IO3) and α- and β-AgNpO2(SeO3)87Do Secondary and Tertiary Ammonium Cations Act as Structure-Directing Agents in the Formation of Layered Uranyl Selenites?48DFT Studies of Uranyl Acetate, Carbonate, and Malonate, Complexes in Solution50New one-dimensional uranyl and neptunyl iodates: crystal structures of K3[(UO2)2(IO3)6](IO3)·H2O and K[NpO2(IO3)3]·1.5H2O22Hydrothermal synthesis and structure of K6[(UO2)4(CrO4)7]·6H2O: A layered uranyl chromate with a new uranyl sheet topology30Hydrothermal Synthesis of Rare Earth Iodates from the Corresponding Periodates: II1). Synthesis and Structures of Ln(IO3)3 (Ln = Pr, Nd, Sm, Eu, Gd, Tb, Ho, Er) and Ln(IO3)3 · 2H2O (Ln = Eu, Gd, Dy, Er, Tm, Yb)34Combinatorial topology of salts of inorganic oxoacids: zero-, one- and two-dimensional units with corner-sharing between coordination polyhedra103Hydrothermal synthesis and crystal structure of Cs6[(UO2)4(W5O21)(OH)2(H2O)2]: a new polar uranyl tungstate19Crystal chemistry and ion-exchange properties of the layered uranyl iodate K[UO2(IO3)3]40Synthesis, Structure, and Spectroscopic Properties of Am(IO3)3 and the Photoluminescence Behavior of Cm(IO3)348U6+ MINERALS AND INORGANIC COMPOUNDS: INSIGHTS INTO AN EXPANDED STRUCTURAL HIERARCHY OF CRYSTAL STRUCTURES627Extended networks, porous sheets, and chiral frameworks. Thorium materials containing mixed geometry anions: Structures and properties of Th(SeO3)(SeO4), Th(IO3)2(SeO4)(H2O)3·H2O, and Th(CrO4)(IO3)244Synthesis, structure, and property of a uranium–potassium–organic coordination polymer containing infinite metal oxide sheets16Syntheses, structures, and vibrational spectroscopy of the two-dimensional iodates Ln(IO3)3 and Ln(IO3)3(H2O) (LnYb, Lu)21Structural Polarity Induced by Cooperative Hydrogen Bonding and Lone-Pair Alignment in the Molecular Uranyl Iodate Na2[UO2(IO3)4(H2O)]18Synthesis and structure of In(IO3)3 and vibrational spectroscopy of M(IO3)3 (M=Al, Ga, In)31Intercalation of Iodic Acid into the Layered Uranyl Iodate, UO2(IO3)2(H2O)26Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)26Actinide compounds with heavy oxoanions containing a stereochemically active lone-pair of electrons2An organic–inorganic hybrid uranyl nicotinate molybdate polymer and its fluorescent property16THE STEREOCHEMISTRY AND CHEMICAL COMPOSITION OF INTERSTITIAL COMPLEXES IN URANYL-OXYSALT MINERALS75Hydrothermal synthesis of a chiral rare earth iodate (Gd(IO3)3 · H2O) showing the rare (3, 8)-connected (43)(4 · 62) (49 · 617 · 82) topology3Alternative approaches to structure description1Anion-topology approach0Basic concepts3Copyright Page0Dedication0Dimensional reduction in inorganic oxysalts0Graph theory applied to low-dimensional structural units in inorganic oxysalts2Preface0Structural Crystallography of Inorganic Oxysalts127Topology of framework structures in inorganic oxysalts0Syntheses, crystal structures, and properties of three new lanthanum( iii ) vanadium iodates56Polarity and Chirality in Uranyl Borates: Insights into Understanding the Vitrification of Nuclear Waste and the Development of Nonlinear Optical Materials104Explorations of New Second-Order Nonlinear Optical Materials in the KI-MII -IV-O Systems43Polar or Non-Polar? Syntheses, Crystal Structures, and Optical Properties of Three New Palladium(II) Iodates45Highly efficient iodine species enriching and guest-driven tunable luminescent properties based on a cadmium(ii)-triazole MOF185Structures and properties of functional metal iodates72Facile Routes to ThIV, UIV, and NpIV Phosphites and Phosphates23Syntheses and crystal structures of two novel alkaline uranyl chromates A2(UO2)(CrO4)2 (A=Rb, Cs) with bidentate coordination mode of uranyl ions by chromate anions20Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) Phosphates43Crystal Chemistry of Uranium Oxides and Minerals27K4TM4(V2O7)2(IO3)4(H2O) (TM = Zn, Ni, Co): a series of quinary mixed metal–vanadium(v)–iodates18Structural changes within the alkaline earth uranyl phosphites9From Order to Disorder and Back Again: In Situ Hydrothermal Redox Reactions of Uranium Phosphites and Phosphates28Syntheses, Structures, and Comparisons of Thallium Uranium Phosphites, Mixed Phosphate-Phosphites, and Phosphate22CrVI→CrV Transition in Uranyl Chromium Compounds: Synthesis and High‐temperature X‐ray Diffraction Study of Cs2[(UO2)2(CrO4)3]24Explorations of New Second-Order Nonlinear Optical Materials in the Ternary Rubidium Iodate System: Noncentrosymmetric β-RbIO3(HIO3)2 and Centrosymmetric Rb3(IO3)3(I2O5)(HIO3)4(H2O)59Synthesis, crystal structure and optical properties of two new layered cadmium iodates: Cd(IO3)X (X=Cl, OH)13The structure hierarchy hypothesis44A series of novel mercury( i ) selenites and tellurites containing SOJT Mo 6+ cations18Expanding the Crystal Chemistry of Uranyl Peroxides: Four Hybrid Uranyl-Peroxide Structures Containing EDTA28Bio-relevant cobalt(II) complexes with compartmental polyquinoline ligand: Synthesis, crystal structures and biological activities13Recent advances on second-order NLO materials based on metal iodates328Flux Synthesis, Structure, Properties, and Theoretical Magnetic Study of Uranium(IV)-Containing A2USi6O15 (A = K, Rb) with an Intriguing Green-to-Purple, Crystal-to-Crystal Structural Transition in the K Analogue32Explorations of New SHG Materials in the Alkali-Metal–Nb5+–Selenite System33A Revised and Expanded Structure Hierarchy of Natural and Synthetic Hexavalent Uranium Compounds172Mild Periodic Acid Flux and Hydrothermal Methods for the Synthesis of Crystalline f-Element-Bearing Iodate Compounds20Detection and identification of solids, surfaces, and solutions of uranium using vibrational spectroscopy179Expansion of the structural diversity of f-element bearing molybdate iodates: synthesis, structures, and optical properties19Effect of solution acidity on the crystallization of polychromates in uranyl-bearing systems: synthesis and crystal structures of Rb2[(UO2)(Cr2O7)(NO3)2] and two new polymorphs of Rb2Cr3O105Cd3(IO3)(IO4)F2·0.1CdO: A Nonlinear-Optical Crystal with the Introduction of Fluoride into Iodate Containing Both [IO3]− and [IO4]3– Groups18Structural, Electronic, Mechanical, Linear and Nonlinear Optical, and Piezoelectric Properties of CsIO\(_3\) Materials from Ab Initio Study0Crystal Chemistry and Structural Complexity of the Uranyl Molybdate Minerals and Synthetic Compounds9

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  1. 22 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2002-01-01

    Martin P. Attfield

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  2. ChemInform Abstract: Mixed‐Metal Uranium(VI) Iodates: Hydrothermal Syntheses, Structures, and Reactivity of Rb[UO2(CrO4)(IO3)(H2O)], A2[UO2(CrO4)(IO3)2] (A: K, Rb, Cs), and K2[UO2(MoO4)(IO3)2].

    ChemInform · 2002-12-10

    Richard E. Sykora, Steven M. McDaniel, Daniel M. Wells, Thomas E. Albrecht‐Schmitt

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  3. 21 New compounds and structures in the solid state

    Annual Reports Section A (Inorganic Chemistry) · 2003-01-01

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  4. Advances in Understanding of the Crystal Chemistry of Hexavalent Uranium

    MRS Proceedings · 2003-01-01

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  5. Structure and Bonding in Solution of Dioxouranium(VI) Oxalate Complexes: Isomers and Intramolecular Ligand Exchange

    Inorganic Chemistry · 2003-02-20

    Valérie Vallet, Henry Moll, Ulf Wahlgren, Zoltán Szabó, Ingmar Grenthe

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  6. Hydrothermal Preparation of Nickel(II)/Uranium(IV) Fluorides with One-, Two-, and Three-Dimensional Topologies

    Inorganic Chemistry · 2003-03-25

    Amanda C. Bean, Tyler A. Sullens, Wolfgang Runde, Thomas E. Albrecht‐Schmitt

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  7. Cation−Cation Interactions in Neptunyl(V) Compounds: Hydrothermal Preparation and Structural Characterization of NpO2(IO3) and α- and β-AgNpO2(SeO3)

    Inorganic Chemistry · 2003-05-09

    Thomas E. Albrecht‐Schmitt, Philip M. Almond, Richard E. Sykora

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  8. Do Secondary and Tertiary Ammonium Cations Act as Structure-Directing Agents in the Formation of Layered Uranyl Selenites?

    Inorganic Chemistry · 2003-08-12

    Philip M. Almond, Thomas E. Albrecht‐Schmitt

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  9. DFT Studies of Uranyl Acetate, Carbonate, and Malonate, Complexes in Solution

    Inorganic Chemistry · 2003-08-23

    Jordi Vázquez, Carles Bó, Josep Maria Poblet, Joan de Pablo, Jordi Bruno

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  10. New one-dimensional uranyl and neptunyl iodates: crystal structures of K3[(UO2)2(IO3)6](IO3)·H2O and K[NpO2(IO3)3]·1.5H2O

    Journal of Solid State Chemistry · 2003-10-25

    Richard E. Sykora, Amanda C. Bean, Brian L. Scott, Wolfgang Runde, Thomas E. Albrecht‐Schmitt

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  11. Hydrothermal synthesis and structure of K6[(UO2)4(CrO4)7]·6H2O: A layered uranyl chromate with a new uranyl sheet topology

    Journal of Solid State Chemistry · 2003-12-31

    Richard E. Sykora, Steven M. McDaniel, Thomas E. Albrecht‐Schmitt

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  12. Hydrothermal Synthesis of Rare Earth Iodates from the Corresponding Periodates: II1). Synthesis and Structures of Ln(IO3)3 (Ln = Pr, Nd, Sm, Eu, Gd, Tb, Ho, Er) and Ln(IO3)3 · 2H2O (Ln = Eu, Gd, Dy, Er, Tm, Yb)

    Zeitschrift für anorganische und allgemeine Chemie · 2004-02-16

    Paul Douglas, Andrew L. Hector, William Levason, Mark E. Light, Melissa L. Matthews, Michael Webster

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  13. Combinatorial topology of salts of inorganic oxoacids: zero-, one- and two-dimensional units with corner-sharing between coordination polyhedra

    Crystallography Reviews · 2004-07-01

    Sergey V. Krivovichev

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  14. Hydrothermal synthesis and crystal structure of Cs6[(UO2)4(W5O21)(OH)2(H2O)2]: a new polar uranyl tungstate

    Journal of Solid State Chemistry · 2004-08-31

    Richard E. Sykora, Thomas E. Albrecht‐Schmitt

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  15. Crystal chemistry and ion-exchange properties of the layered uranyl iodate K[UO2(IO3)3]

    Journal of Solid State Chemistry · 2004-12-15

    Tatiana Y. Shvareva, Philip M. Almond, Thomas E. Albrecht‐Schmitt

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  16. Synthesis, Structure, and Spectroscopic Properties of Am(IO3)3 and the Photoluminescence Behavior of Cm(IO3)3

    Inorganic Chemistry · 2005-07-06

    Richard E. Sykora, Zerihun Assefa, Richard Geoffrey Haire, Thomas E. Albrecht‐Schmitt

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  17. U6+ MINERALS AND INORGANIC COMPOUNDS: INSIGHTS INTO AN EXPANDED STRUCTURAL HIERARCHY OF CRYSTAL STRUCTURES

    The Canadian Mineralogist · 2005-12-01

    Peter Carman Burns

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  18. Extended networks, porous sheets, and chiral frameworks. Thorium materials containing mixed geometry anions: Structures and properties of Th(SeO3)(SeO4), Th(IO3)2(SeO4)(H2O)3·H2O, and Th(CrO4)(IO3)2

    Journal of Solid State Chemistry · 2006-02-08

    Tyler A. Sullens, Philip M. Almond, Jessica A. Byrd, James V. Beitz, Travis H. Bray, Thomas E. Albrecht‐Schmitt

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  19. Synthesis, structure, and property of a uranium–potassium–organic coordination polymer containing infinite metal oxide sheets

    Journal of Molecular Structure · 2006-03-01

    Weihai Zhang, Jianshe Zhao

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  20. Syntheses, structures, and vibrational spectroscopy of the two-dimensional iodates Ln(IO3)3 and Ln(IO3)3(H2O) (LnYb, Lu)

    Journal of Solid State Chemistry · 2006-08-07

    Zerihun Assefa, Jie Ling, Richard Geoffrey Haire, Thomas E. Albrecht‐Schmitt, Richard E. Sykora

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  21. Structural Polarity Induced by Cooperative Hydrogen Bonding and Lone-Pair Alignment in the Molecular Uranyl Iodate Na2[UO2(IO3)4(H2O)]

    Inorganic Chemistry · 2006-08-19

    Travis H. Bray, James V. Beitz, Amanda C. Bean, Yaqin Yu, Thomas E. Albrecht‐Schmitt

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  22. Synthesis and structure of In(IO3)3 and vibrational spectroscopy of M(IO3)3 (M=Al, Ga, In)

    Journal of Solid State Chemistry · 2006-08-31

    Nhan Ngo, Katrina Kalachnikova, Zerihun Assefa, Richard Geoffrey Haire, Richard E. Sykora

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  23. Intercalation of Iodic Acid into the Layered Uranyl Iodate, UO2(IO3)2(H2O)

    Inorganic Chemistry · 2006-12-20

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  24. Actinide compounds containing hexavalent cations of the VI group elements (S, Se, Mo, Cr, W)

    Elsevier eBooks · 2007-01-01

    Sergey V. Krivovichev, Peter Carman Burns

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  25. Actinide compounds with heavy oxoanions containing a stereochemically active lone-pair of electrons

    Elsevier eBooks · 2007-01-01

    Richard E. Sykora, Tatiana Y. Shvareva, Thomas E. Albrecht‐Schmitt

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  26. An organic–inorganic hybrid uranyl nicotinate molybdate polymer and its fluorescent property

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  27. THE STEREOCHEMISTRY AND CHEMICAL COMPOSITION OF INTERSTITIAL COMPLEXES IN URANYL-OXYSALT MINERALS

    The Canadian Mineralogist · 2008-04-01

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  28. Hydrothermal synthesis of a chiral rare earth iodate (Gd(IO3)3 · H2O) showing the rare (3, 8)-connected (43)(4 · 62) (49 · 617 · 82) topology

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  29. Alternative approaches to structure description

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  30. Anion-topology approach

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  31. Basic concepts

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  32. Copyright Page

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  33. Dedication

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  34. Dimensional reduction in inorganic oxysalts

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  35. Graph theory applied to low-dimensional structural units in inorganic oxysalts

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  36. Preface

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  37. Structural Crystallography of Inorganic Oxysalts

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  38. Topology of framework structures in inorganic oxysalts

    Unknown journal · 2009-01-22

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  39. Syntheses, crystal structures, and properties of three new lanthanum( iii ) vanadium iodates

    Dalton Transactions · 2010-01-01

    Chuan‐Fu Sun, Ting Hu, Xiang Xu, Jiang‐Gao Mao

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  40. Polarity and Chirality in Uranyl Borates: Insights into Understanding the Vitrification of Nuclear Waste and the Development of Nonlinear Optical Materials

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    Shuao Wang, Evgeny V. Alekseev, Jie Ling, Guokui Liu, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  41. Explorations of New Second-Order Nonlinear Optical Materials in the KI-MII -IV-O Systems

    Inorganic Chemistry · 2010-04-16

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  42. Polar or Non-Polar? Syntheses, Crystal Structures, and Optical Properties of Three New Palladium(II) Iodates

    Inorganic Chemistry · 2010-09-20

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  43. Highly efficient iodine species enriching and guest-driven tunable luminescent properties based on a cadmium(ii)-triazole MOF

    Chemical Communications · 2011-01-01

    Qi‐Kui Liu, Jian‐Ping Ma, Yu‐Bin Dong

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  44. Structures and properties of functional metal iodates

    Science China Chemistry · 2011-05-30

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  45. Facile Routes to ThIV, UIV, and NpIV Phosphites and Phosphates

    European Journal of Inorganic Chemistry · 2011-08-05

    Eric M. Villa, Shuao Wang, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  46. Syntheses and crystal structures of two novel alkaline uranyl chromates A2(UO2)(CrO4)2 (A=Rb, Cs) with bidentate coordination mode of uranyl ions by chromate anions

    Journal of Solid State Chemistry · 2012-01-30

    Oleg I. Siidra, Еvgeny V. Nazarchuk, Sergey V. Krivovichev

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  47. Systematic Evolution from Uranyl(VI) Phosphites to Uranium(IV) Phosphates

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  48. Crystal Chemistry of Uranium Oxides and Minerals

    Elsevier eBooks · 2013-01-01

    Sergey V. Krivovichev

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  49. K4TM4(V2O7)2(IO3)4(H2O) (TM = Zn, Ni, Co): a series of quinary mixed metal–vanadium(v)–iodates

    CrystEngComm · 2013-01-01

    Bing‐Ping Yang, Xiang Xu, Chao Huang, Jiang‐Gao Mao

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  50. Structural changes within the alkaline earth uranyl phosphites

    Dalton Transactions · 2013-01-01

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