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RESEARCH PAPER · Crystal Growth & Design · 2016

Flux Growth of [NaK6F][(UO2)3(Si2O7)2] and [KK6Cl][(UO2)3(Si2O7)2]: The Effect of Surface Area to Volume Ratios on Reaction Products

Gregory W. Morrison, Hans‐Conrad zur Loye

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Flux Growth of [NaK6F][(UO2)3(Si2O7)2] and [KK6Cl][(UO2)3(Si2O7)2]: The Effect of Surface Area to Volume Ratios on Reaction ProductsOriginalK8(K5F)U6Si8O40: An Intergrowth Uranyl Silicate24A5RE4X[TO4]4 crystal growth: Fluoride flux synthesis of Na5Ln4F[GeO4]4 (Ln=Pr, Nd), the first quaternary germanate oxyfluorides11Understanding the Formation of Salt-Inclusion Phases: An Enhanced Flux Growth Method for the Targeted Synthesis of Salt-Inclusion Cesium Halide Uranyl Silicates61Supercritical synthesis and topological analysis of K 5 U 5 O 17 (OH)3Where Do New Materials Come From? Neither the Stork nor the Birds and the Bees! In Search of the Next “First Material”1Flux versus Hydrothermal Growth: Polymorphism of A2(UO2)Si2O6 (A = Rb, Cs)19Observation of Intense X-ray Scintillation in a Family of Mixed Anion Silicates, Cs3RESi4O10F2 (RE = Y, Eu–Lu), Obtained via an Enhanced Flux Crystal Growth Technique59Hydrothermal Synthesis, Study, and Classification of Microporous Uranium Silicates and Germanates18Comparison of Uranium(VI) and Thorium(IV) Silicates Synthesized via Mixed Fluxes Techniques14Hierarchical Materials as Tailored Nuclear Waste Forms: A Perspective123Formation of Open Framework Uranium Germanates: The Influence of Mixed Molten Flux and Charge Density Dependence in U-Silicate and U-Germanate Families19Versatile Uranyl Germanate Framework Hosting 12 Different Alkali Halide 1D Salt Inclusions32Understanding the Stability of Salt-Inclusion Phases for Nuclear Waste-forms through Volume-based Thermodynamics11Flux crystal growth, structure, magnetic and optical properties of a family of alkali uranium(IV) phosphates10Mineralogy, Crystallography and Structural Complexity of Natural Uranyl Silicates31Flux crystal growth of uranium( v ) containing oxyfluoride perovskites13Flux crystal growth: a versatile technique to reveal the crystal chemistry of complex uranium oxides49Synthesis and crystal structure of [(Cs6F)(Cs3AgF)][Ge14O32] through alkali halide flux growth13Crystal growth of novel 3D skeleton uranyl germanium complexes: influence of synthetic conditions on crystal structures10New germanate and mixed cobalt germanate salt inclusion materials: [(Rb 6 F)(Rb 4 F)][Ge 14 O 32 ] and [(Rb 6 F)(Rb 3.1 Co 0.9 F 0.96 )][Co 3.8 Ge 10.2 O 30 F 2 ]10Crystal Growth of Alkali Uranyl Borates from Molten Salt Fluxes: Characterization and Ion Exchange Behavior of A2(UO2)B2O5 (A = Cs, Rb, K)13Flux Growth of Uranyl Titanates: Rare Examples of TiO4 Tetrahedra and TiO5 Square Bipyramids10Expanding the Chemistry of Salt-Inclusion Materials: Utilizing the Titanyl Ion as a Structure Directing Agent for the Targeted Synthesis of Salt-Inclusion Titanium Silicates14Pentanary cesium titanyl/titanate silicate oxyfluorides: Syntheses and structures2Uranyl Titanate Silicates: Syntheses, Structures, and Family Relations5Two tetravalent uranium silicate and germanate crystals with three membered single-ring by molten salt method: K2USi3O9 and Cs2UGe3O930Luminescence and Scintillation in the Niobium Doped Oxyfluoride Rb4Ge5O9F6:Nb8Effect of charge and anisotropic diffusivity on ion exchange kinetics in nuclear waste form materials6U(VI) Coordination Modes in Complex Uranium Silicates: Cs[(UO6)2(UO2)9(Si2O7)F] and Rb2[(PtO4)(UO2)5(Si2O7)]6Binding of Radionuclides and Surrogate to 18-Crown-6 Ether by Density Functional Theory1Framework Uranyl Silicates: Crystal Chemistry and a New Route for the Synthesis10Flux Synthesis, UV–vis Absorbance, and Magnetism of Cesium Copper Silicates with an Isolated Super-Super Exchange Spin Dimer in Cs6Cu2Si9O230Uranyl silicate nanotubules in Rb2[(UO2)2O(Si3O8)]: synthesis and crystal structure6Exploring the Valence Diversity of Uranium by Flux Growth of Uranium Silicate under Inert Atmosphere6Three uranyl silicate framework structures, Cs1.8K0.2[(UO2)(Si2O6)], K4Sr[(UO2)(Si4O12)], and [Cs2KF][(UO2)(Si4O10)], and theoretical calculation of density functional theory for salt-inclusion material2Potential immobilization of Cs and Sr within perovskite-type CsSr2Ta3O10 ceramic waste forms1New Microporous Framework in the Structure of (K0.67Rb0.33)2[(UO2)2(Si5O13)](H2O)0Growth Dynamics and Morphological Evolution of Salt-Inclusion Material Crystals in Molten Salts: A Phase-Field Study0

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  1. K8(K5F)U6Si8O40: An Intergrowth Uranyl Silicate

    Inorganic Chemistry · 2016-03-14

    Gregory W. Morrison, T. Thao Tran, P. Shiv Halasyamani, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  2. A5RE4X[TO4]4 crystal growth: Fluoride flux synthesis of Na5Ln4F[GeO4]4 (Ln=Pr, Nd), the first quaternary germanate oxyfluorides

    Journal of Solid State Chemistry · 2016-04-29

    Allison M. Latshaw, Branford O. Wilkins, Gregory W. Morrison, Mark D. Smith, Hans‐Conrad zur Loye

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  3. Understanding the Formation of Salt-Inclusion Phases: An Enhanced Flux Growth Method for the Targeted Synthesis of Salt-Inclusion Cesium Halide Uranyl Silicates

    Journal of the American Chemical Society · 2016-05-24

    Gregory W. Morrison, Mark D. Smith, Hans‐Conrad zur Loye

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  4. Supercritical synthesis and topological analysis of K 5 U 5 O 17 (OH)

    CrystEngComm · 2017-01-01

    Justin B. Felder, Mark D. Smith, Hans‐Conrad zur Loye

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  5. Where Do New Materials Come From? Neither the Stork nor the Birds and the Bees! In Search of the Next “First Material”

    Scholar Commons (University of South Carolina) · 2017-01-01

    Gregory W. Morrison, Dileka Abeysinghe, Justin B. Felder, Shani Egodawatte, Timothy Ferreira, Hans‐Conrad zur Loye

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  6. Flux versus Hydrothermal Growth: Polymorphism of A2(UO2)Si2O6 (A = Rb, Cs)

    Inorganic Chemistry · 2017-01-20

    Gregory W. Morrison, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  7. Observation of Intense X-ray Scintillation in a Family of Mixed Anion Silicates, Cs3RESi4O10F2 (RE = Y, Eu–Lu), Obtained via an Enhanced Flux Crystal Growth Technique

    Journal of the American Chemical Society · 2017-09-19

    Gregory W. Morrison, Allison M. Latshaw, Nicholas R. Spagnuolo, Hans‐Conrad zur Loye

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  8. Hydrothermal Synthesis, Study, and Classification of Microporous Uranium Silicates and Germanates

    Inorganic Chemistry · 2018-04-02

    Haijian Li, Philip Kegler, Dirk Bosbach, Evgeny V. Alekseev

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  9. Comparison of Uranium(VI) and Thorium(IV) Silicates Synthesized via Mixed Fluxes Techniques

    Inorganic Chemistry · 2018-05-16

    Haijian Li, Philip Kegler, Vladislav V. Klepov, Martina Klinkenberg, Dirk Bosbach, Evgeny V. Alekseev

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  10. Hierarchical Materials as Tailored Nuclear Waste Forms: A Perspective

    Chemistry of Materials · 2018-06-22

    Hans‐Conrad zur Loye, Theodore M. Besmann, Jake Amoroso, Kyle S. Brinkman, Agnès Grandjean, Charles H. Henager, Shenyang Hu, Scott T. Misture, Simon Robert Phillpot, Natalia B. Shustova, Hui Wang, Robert J. Koch, Gregory W. Morrison, Ekaterina A. Dolgopolova

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  11. Formation of Open Framework Uranium Germanates: The Influence of Mixed Molten Flux and Charge Density Dependence in U-Silicate and U-Germanate Families

    Inorganic Chemistry · 2018-08-20

    Haijian Li, Eike M. Langer, Philip Kegler, Giuseppe Modolo, Evgeny V. Alekseev

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  12. Versatile Uranyl Germanate Framework Hosting 12 Different Alkali Halide 1D Salt Inclusions

    Inorganic Chemistry · 2018-09-05

    Christian A. Juillerat, Emily E. Moore, Gregory W. Morrison, Mark D. Smith, Theodore M. Besmann, Hans‐Conrad zur Loye

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  13. Understanding the Stability of Salt-Inclusion Phases for Nuclear Waste-forms through Volume-based Thermodynamics

    Scientific Reports · 2018-10-11

    Emily E. Moore, Vancho Kocevski, Christian A. Juillerat, Gregory W. Morrison, Mingyang Zhao, Kyle S. Brinkman, Hans‐Conrad zur Loye, Theodore M. Besmann

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  14. Flux crystal growth, structure, magnetic and optical properties of a family of alkali uranium(IV) phosphates

    Journal of Solid State Chemistry · 2018-10-26

    Mohammad Usman, Gregory W. Morrison, Vladislav V. Klepov, Mark D. Smith, Hans‐Conrad zur Loye

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  15. Mineralogy, Crystallography and Structural Complexity of Natural Uranyl Silicates

    Minerals · 2018-11-27

    Jakub Plášil

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  16. Flux crystal growth of uranium( v ) containing oxyfluoride perovskites

    Inorganic Chemistry Frontiers · 2019-01-01

    Christian A. Juillerat, Vancho Kocevski, Gregory W. Morrison, S. Karakalos, Deepak Patil, Scott T. Misture, Theodore M. Besmann, Hans‐Conrad zur Loye

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  17. Flux crystal growth: a versatile technique to reveal the crystal chemistry of complex uranium oxides

    Dalton Transactions · 2019-01-01

    Christian A. Juillerat, Vladislav V. Klepov, Gregory W. Morrison, Kristen A. Pace, Hans‐Conrad zur Loye

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  18. Synthesis and crystal structure of [(Cs6F)(Cs3AgF)][Ge14O32] through alkali halide flux growth

    Solid State Sciences · 2019-08-16

    Nicholas R. Spagnuolo, Gregory W. Morrison, Hans‐Conrad zur Loye

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  19. Crystal growth of novel 3D skeleton uranyl germanium complexes: influence of synthetic conditions on crystal structures

    Dalton Transactions · 2020-01-01

    Haijian Li, Philip Kegler, Evgeny V. Alekseev

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  20. New germanate and mixed cobalt germanate salt inclusion materials: [(Rb 6 F)(Rb 4 F)][Ge 14 O 32 ] and [(Rb 6 F)(Rb 3.1 Co 0.9 F 0.96 )][Co 3.8 Ge 10.2 O 30 F 2 ]

    CrystEngComm · 2020-01-01

    Darren Carone, Mohammad Usman, Vladislav V. Klepov, Mark D. Smith, Vancho Kocevski, Theodore M. Besmann, Hans‐Conrad zur Loye

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  21. Crystal Growth of Alkali Uranyl Borates from Molten Salt Fluxes: Characterization and Ion Exchange Behavior of A2(UO2)B2O5 (A = Cs, Rb, K)

    Inorganic Chemistry · 2020-04-10

    Kristen A. Pace, Robert J. Koch, Mark D. Smith, Gregory W. Morrison, Vladislav V. Klepov, Theodore M. Besmann, Scott T. Misture, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  22. Flux Growth of Uranyl Titanates: Rare Examples of TiO4 Tetrahedra and TiO5 Square Bipyramids

    The Journal of Physical Chemistry A · 2020-11-03

    Gregory W. Morrison, Matthew S. Christian, Theodore M. Besmann, Hans‐Conrad zur Loye

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  23. Expanding the Chemistry of Salt-Inclusion Materials: Utilizing the Titanyl Ion as a Structure Directing Agent for the Targeted Synthesis of Salt-Inclusion Titanium Silicates

    Crystal Growth & Design · 2020-11-12

    Gregory W. Morrison, Hans‐Conrad zur Loye

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  24. Pentanary cesium titanyl/titanate silicate oxyfluorides: Syntheses and structures

    Solid State Sciences · 2021-06-05

    Gregory W. Morrison, Vladislav V. Klepov, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  25. Uranyl Titanate Silicates: Syntheses, Structures, and Family Relations

    Crystal Growth & Design · 2022-01-14

    Gregory W. Morrison, Hans‐Conrad zur Loye

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  26. Two tetravalent uranium silicate and germanate crystals with three membered single-ring by molten salt method: K2USi3O9 and Cs2UGe3O9

    Chinese Chemical Letters · 2022-03-08

    Xu Zhang, Lei Zhang, Tao Bo, Shanen Huang, Zhi‐wei Huang, Wei‐Qun Shi

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  27. Luminescence and Scintillation in the Niobium Doped Oxyfluoride Rb4Ge5O9F6:Nb

    Inorganics · 2022-06-16

    Darren Carone, Vladislav V. Klepov, Scott T. Misture, Joseph C. Schaeperkoetter, Luiz Gustavo Jacobsohn, Mina Aziziha, Juliano Schorne Pinto, Stuart A. J. Thomson, Adrian T. Hines, Theodore M. Besmann, Hans‐Conrad zur Loye

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  28. Effect of charge and anisotropic diffusivity on ion exchange kinetics in nuclear waste form materials

    Journal of Nuclear Materials · 2022-10-10

    Yulan Li, Shenyang Hu, Robert O. Montgomery, Agnès Grandjean, Theodore M. Besmann, Hans‐Conrad zur Loye

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  29. U(VI) Coordination Modes in Complex Uranium Silicates: Cs[(UO6)2(UO2)9(Si2O7)F] and Rb2[(PtO4)(UO2)5(Si2O7)]

    Chemistry · 2022-11-10

    Еvgeny V. Nazarchuk, Oleg I. Siidra, Dmitri O. Charkin, Yana G. Tagirova

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  30. Binding of Radionuclides and Surrogate to 18-Crown-6 Ether by Density Functional Theory

    Microporous and Mesoporous Materials · 2023-01-01

    Yuan Liu, An T. Ta, Kyoung Chul Park, Shenyang Hu, Natalia B. Shustova, Simon Robert Phillpot

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  31. Framework Uranyl Silicates: Crystal Chemistry and a New Route for the Synthesis

    Materials · 2023-06-02

    Еvgeny V. Nazarchuk, Oleg I. Siidra, Dmitri O. Charkin, Yana G. Tagirova

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  32. Flux Synthesis, UV–vis Absorbance, and Magnetism of Cesium Copper Silicates with an Isolated Super-Super Exchange Spin Dimer in Cs6Cu2Si9O23

    Inorganic Chemistry · 2023-07-12

    Gregory W. Morrison, Virginia G. Jones, K. Pilar Zamorano, John E. Greedan, Hans‐Conrad zur Loye

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  33. Uranyl silicate nanotubules in Rb2[(UO2)2O(Si3O8)]: synthesis and crystal structure

    Zeitschrift für Kristallographie - Crystalline Materials · 2023-08-29

    Еvgeny V. Nazarchuk, Oleg I. Siidra, Dmitri O. Charkin, Yana G. Tagirova

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  34. Exploring the Valence Diversity of Uranium by Flux Growth of Uranium Silicate under Inert Atmosphere

    Inorganic Chemistry · 2024-03-02

    Xu Zhang, Tao Bo, Zhi‐wei Huang, Zhiheng Zhou, Kong‐Qiu Hu, Wei‐Qun Shi, Lei Mei

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  35. Three uranyl silicate framework structures, Cs1.8K0.2[(UO2)(Si2O6)], K4Sr[(UO2)(Si4O12)], and [Cs2KF][(UO2)(Si4O10)], and theoretical calculation of density functional theory for salt-inclusion material

    Journal of Solid State Chemistry · 2024-12-25

    Xiaochen Zhang, Yu Wang, Tao Bo, Lei Zhang

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  36. Potential immobilization of Cs and Sr within perovskite-type CsSr2Ta3O10 ceramic waste forms

    Journal of Radioanalytical and Nuclear Chemistry · 2025-01-06

    Yifan Li, Shuang Cao, Qingming Yang, Yuannuo Wang, Jingyang Wang, Caishan Jiao, Meng Zhang, Lei Zhang

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  37. New Microporous Framework in the Structure of (K0.67Rb0.33)2[(UO2)2(Si5O13)](H2O)

    Journal of Structural Chemistry · 2025-04-01

    Еvgeny V. Nazarchuk, Oleg I. Siidra

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  38. Growth Dynamics and Morphological Evolution of Salt-Inclusion Material Crystals in Molten Salts: A Phase-Field Study

    Journal of Nuclear Materials · 2026-10-01

    Yi Li, Jingyang Wang, Hemu Zhao, Bo Liang, Debang Liu, Mingyu Liu, Youyou Wang, Lun-xiu Cao, Chunhui Li, Zhenyu Han, Meng Zhang, Lei Zhang, Yitung Chen

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