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RESEARCH PAPER · Inorganic Chemistry · 2016

K8(K5F)U6Si8O40: An Intergrowth Uranyl Silicate

Gregory W. Morrison, T. Thao Tran, P. Shiv Halasyamani, Hans‐Conrad zur Loye

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K8(K5F)U6Si8O40: An Intergrowth Uranyl SilicateOriginalUnderstanding the Formation of Salt-Inclusion Phases: An Enhanced Flux Growth Method for the Targeted Synthesis of Salt-Inclusion Cesium Halide Uranyl Silicates61Where Do New Materials Come From? Neither the Stork nor the Birds and the Bees! In Search of the Next “First Material”1Flux versus Hydrothermal Growth: Polymorphism of A2(UO2)Si2O6 (A = Rb, Cs)19Observation of Intense X-ray Scintillation in a Family of Mixed Anion Silicates, Cs3RESi4O10F2 (RE = Y, Eu–Lu), Obtained via an Enhanced Flux Crystal Growth Technique59Hydrothermal Synthesis, Study, and Classification of Microporous Uranium Silicates and Germanates18Comparison of Uranium(VI) and Thorium(IV) Silicates Synthesized via Mixed Fluxes Techniques14Formation of Open Framework Uranium Germanates: The Influence of Mixed Molten Flux and Charge Density Dependence in U-Silicate and U-Germanate Families19Mineralogy, Crystallography and Structural Complexity of Natural Uranyl Silicates31Flux crystal growth: a versatile technique to reveal the crystal chemistry of complex uranium oxides49Crystal growth of novel 3D skeleton uranyl germanium complexes: influence of synthetic conditions on crystal structures10New germanate and mixed cobalt germanate salt inclusion materials: [(Rb 6 F)(Rb 4 F)][Ge 14 O 32 ] and [(Rb 6 F)(Rb 3.1 Co 0.9 F 0.96 )][Co 3.8 Ge 10.2 O 30 F 2 ]10Targeted crystal growth of uranium gallophosphates via the systematic exploration of the UF 4 –GaPO 4 –ACl (A = Cs, Rb) phase space7Crystal Growth of Alkali Uranyl Borates from Molten Salt Fluxes: Characterization and Ion Exchange Behavior of A2(UO2)B2O5 (A = Cs, Rb, K)13“Soft” Alkali Bromide and Iodide Fluxes for Crystal Growth36Flux Growth of Uranyl Titanates: Rare Examples of TiO4 Tetrahedra and TiO5 Square Bipyramids10Expanding the Chemistry of Salt-Inclusion Materials: Utilizing the Titanyl Ion as a Structure Directing Agent for the Targeted Synthesis of Salt-Inclusion Titanium Silicates13Hydrothermal Synthesis and Structural Investigation of a Crystalline Uranyl Borosilicate3Pentanary cesium titanyl/titanate silicate oxyfluorides: Syntheses and structures2Uranyl Titanate Silicates: Syntheses, Structures, and Family Relations5Two tetravalent uranium silicate and germanate crystals with three membered single-ring by molten salt method: K2USi3O9 and Cs2UGe3O930Luminescence and Scintillation in the Niobium Doped Oxyfluoride Rb4Ge5O9F6:Nb8Framework Uranyl Silicates: Crystal Chemistry and a New Route for the Synthesis10Structural diversity and complexity of antiperovskites38Synthesis and stability study of strontium-containing Apatites: Sr5(AO4)3X (A = P, V; X = F, Cl, Br)0

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24 direct citing papers saved.

  1. Understanding the Formation of Salt-Inclusion Phases: An Enhanced Flux Growth Method for the Targeted Synthesis of Salt-Inclusion Cesium Halide Uranyl Silicates

    Journal of the American Chemical Society · 2016-05-24

    Gregory W. Morrison, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  2. Where Do New Materials Come From? Neither the Stork nor the Birds and the Bees! In Search of the Next “First Material”

    Scholar Commons (University of South Carolina) · 2017-01-01

    Gregory W. Morrison, Dileka Abeysinghe, Justin B. Felder, Shani Egodawatte, Timothy Ferreira, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  3. Flux versus Hydrothermal Growth: Polymorphism of A2(UO2)Si2O6 (A = Rb, Cs)

    Inorganic Chemistry · 2017-01-20

    Gregory W. Morrison, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  4. Observation of Intense X-ray Scintillation in a Family of Mixed Anion Silicates, Cs3RESi4O10F2 (RE = Y, Eu–Lu), Obtained via an Enhanced Flux Crystal Growth Technique

    Journal of the American Chemical Society · 2017-09-19

    Gregory W. Morrison, Allison M. Latshaw, Nicholas R. Spagnuolo, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  5. Hydrothermal Synthesis, Study, and Classification of Microporous Uranium Silicates and Germanates

    Inorganic Chemistry · 2018-04-02

    Haijian Li, Philip Kegler, Dirk Bosbach, Evgeny V. Alekseev

    Read original paper ↗ ·

  6. Comparison of Uranium(VI) and Thorium(IV) Silicates Synthesized via Mixed Fluxes Techniques

    Inorganic Chemistry · 2018-05-16

    Haijian Li, Philip Kegler, Vladislav V. Klepov, Martina Klinkenberg, Dirk Bosbach, Evgeny V. Alekseev

    Read original paper ↗ ·

  7. Formation of Open Framework Uranium Germanates: The Influence of Mixed Molten Flux and Charge Density Dependence in U-Silicate and U-Germanate Families

    Inorganic Chemistry · 2018-08-20

    Haijian Li, Eike M. Langer, Philip Kegler, Giuseppe Modolo, Evgeny V. Alekseev

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  8. Mineralogy, Crystallography and Structural Complexity of Natural Uranyl Silicates

    Minerals · 2018-11-27

    Jakub Plášil

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  9. Flux crystal growth: a versatile technique to reveal the crystal chemistry of complex uranium oxides

    Dalton Transactions · 2019-01-01

    Christian A. Juillerat, Vladislav V. Klepov, Gregory W. Morrison, Kristen A. Pace, Hans‐Conrad zur Loye

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  10. Crystal growth of novel 3D skeleton uranyl germanium complexes: influence of synthetic conditions on crystal structures

    Dalton Transactions · 2020-01-01

    Haijian Li, Philip Kegler, Evgeny V. Alekseev

    Read original paper ↗ ·

  11. New germanate and mixed cobalt germanate salt inclusion materials: [(Rb 6 F)(Rb 4 F)][Ge 14 O 32 ] and [(Rb 6 F)(Rb 3.1 Co 0.9 F 0.96 )][Co 3.8 Ge 10.2 O 30 F 2 ]

    CrystEngComm · 2020-01-01

    Darren Carone, Mohammad Usman, Vladislav V. Klepov, Mark D. Smith, Vancho Kocevski, Theodore M. Besmann, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  12. Targeted crystal growth of uranium gallophosphates via the systematic exploration of the UF 4 –GaPO 4 –ACl (A = Cs, Rb) phase space

    CrystEngComm · 2020-01-01

    Christian A. Juillerat, Vladislav V. Klepov, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  13. Crystal Growth of Alkali Uranyl Borates from Molten Salt Fluxes: Characterization and Ion Exchange Behavior of A2(UO2)B2O5 (A = Cs, Rb, K)

    Inorganic Chemistry · 2020-04-10

    Kristen A. Pace, Robert J. Koch, Mark D. Smith, Gregory W. Morrison, Vladislav V. Klepov, Theodore M. Besmann, Scott T. Misture, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  14. “Soft” Alkali Bromide and Iodide Fluxes for Crystal Growth

    Frontiers in Chemistry · 2020-06-26

    Vladislav V. Klepov, Christian A. Juillerat, Kristen A. Pace, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  15. Flux Growth of Uranyl Titanates: Rare Examples of TiO4 Tetrahedra and TiO5 Square Bipyramids

    The Journal of Physical Chemistry A · 2020-11-03

    Gregory W. Morrison, Matthew S. Christian, Theodore M. Besmann, Hans‐Conrad zur Loye

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  16. Expanding the Chemistry of Salt-Inclusion Materials: Utilizing the Titanyl Ion as a Structure Directing Agent for the Targeted Synthesis of Salt-Inclusion Titanium Silicates

    Crystal Growth & Design · 2020-11-12

    Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  17. Hydrothermal Synthesis and Structural Investigation of a Crystalline Uranyl Borosilicate

    Inorganics · 2021-04-06

    Kristen A. Pace, Vladislav V. Klepov, Mark D. Smith, Travis Williams, Gregory W. Morrison, Jochen A. Lauterbach, Scott T. Misture, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  18. Pentanary cesium titanyl/titanate silicate oxyfluorides: Syntheses and structures

    Solid State Sciences · 2021-06-05

    Gregory W. Morrison, Vladislav V. Klepov, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  19. Uranyl Titanate Silicates: Syntheses, Structures, and Family Relations

    Crystal Growth & Design · 2022-01-14

    Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  20. Two tetravalent uranium silicate and germanate crystals with three membered single-ring by molten salt method: K2USi3O9 and Cs2UGe3O9

    Chinese Chemical Letters · 2022-03-08

    Xu Zhang, Lei Zhang, Tao Bo, Shanen Huang, Zhi‐wei Huang, Wei‐Qun Shi

    Read original paper ↗ ·

  21. Luminescence and Scintillation in the Niobium Doped Oxyfluoride Rb4Ge5O9F6:Nb

    Inorganics · 2022-06-16

    Darren Carone, Vladislav V. Klepov, Scott T. Misture, Joseph C. Schaeperkoetter, Luiz Gustavo Jacobsohn, Mina Aziziha, Juliano Schorne Pinto, Stuart A. J. Thomson, Adrian T. Hines, Theodore M. Besmann, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  22. Framework Uranyl Silicates: Crystal Chemistry and a New Route for the Synthesis

    Materials · 2023-06-02

    Еvgeny V. Nazarchuk, Oleg I. Siidra, Dmitri O. Charkin, Yana G. Tagirova

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  23. Structural diversity and complexity of antiperovskites

    Coordination Chemistry Reviews · 2023-10-11

    Sergey V. Krivovichev

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  24. Synthesis and stability study of strontium-containing Apatites: Sr5(AO4)3X (A = P, V; X = F, Cl, Br)

    Ceramics International · 2025-06-25

    Lanxin Li, Yu Wang, Zhenyu Han, Jinsheng Liao, Lei Zhang

    Read original paper ↗ ·
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