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RESEARCH PAPER · Angewandte Chemie International Edition · 2023

In Situ Chiral Template Approach to Synthesize Homochiral Lead Iodides for Second‐Harmonic Generation

Juan Cheng, Gangji Yi, Zhizhuan Zhang, Ying Long, Hongmei Zeng, Ling Huang, Guohong Zou, Zhien Lin

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In Situ Chiral Template Approach to Synthesize Homochiral Lead Iodides for Second‐Harmonic GenerationOriginal(C 13 N 3 H 14 ) 2 MBr 4 (M = Zn, Cd): two novel hybrid metal halides with balanced integrated nonlinear optical performance31Formation of iminium ions during the processing of metal halide perovskites0RbSb(SO 4 )(H 2 PO 2 )F: a short-wave UV antimony( iii ) oxysalt with mixed-anions demonstrating enhanced birefringence11Solvent-free synthesis and optical properties of two open-framework metal oxalates with zeolitic ABW and diamondoid topologies3Multiple Functions of l -Thioproline in the Synthesis of Chiral Metal Bromides Showing Second-Harmonic-Generation Responses18Optimization of Functional Building Blocks Generates a Substantial Improvement in Birefringence from Sn2OSO4 to Sn3O2(OH)(HSO4)6l -Homoproline-Directed Synthesis of Organic–Inorganic Metal Iodides for Second Harmonic Generation14Chiral Metal Self‐Assemblies of Zirconium‐Tetrahedra and Their Second Harmonic Generation Activity6Chiral Metal Self‐Assemblies of Zirconium‐Tetrahedra and Their Second Harmonic Generation Activity0Chiral 0D hybrid lead-bromide perovskites with strong nonlinear chiroptical properties16Chiral-driven formation of hybrid cyanurates with large birefringence2Template Synthesis of Iodocuprate and Iodoargentate with Photocatalytic Activity and Second Harmonic Generation Efficiency7Two l -Proline Cadmium Thiocyanates with Moderate Second-Harmonic-Generation Responses and Large Birefringences13Novel antimony-based mixed halides exhibiting an excellent SHG response and a broad transmission range20Rational Design and Controlled Synthesis of High-Performance Inorganic Short-Wave UV Nonlinear Optical Materials150Strategically designed anisotropic organic–inorganic metal halides (OIMHs) with superior balance between bandgap and birefringence12Bulk crystal growth and optical properties of a novel organic–inorganic hybrid nonlinear optical thiocyanate: [Mn(CH 3 CONH 2 ) 2 ] [Hg(SCN) 4 ]10Enhanced luminescence in 1D corrugated lead bromides via reduced flexibility of trivalent cations3Enhanced second-harmonic generation response in a chiral lead iodide induced by amino acid coordination8From poor-active to high performance via heteroleptic tetrahedra engineering: rational design of non-π-conjugated hybrids for phase-matchable ultraviolet nonlinear optics12Ligand substitution in organic–inorganic hybrid zinc iodides for second-harmonic generation7Strong second-harmonic generation response in an organic–inorganic hybrid antimony bromide1Extendable Synthesis of Organic Cations for In Situ Construction of Hybrid Metal Halides with Near‐Unity Photoluminescence and Strong Second Harmonic Generation22Extendable Synthesis of Organic Cations for In Situ Construction of Hybrid Metal Halides with Near‐Unity Photoluminescence and Strong Second Harmonic Generation8A Wide Band Gap Germanate with the Largest Second Harmonic Generation Response Created by Hypoxic Strategy22A Wide Band Gap Germanate with the Largest Second Harmonic Generation Response Created by Hypoxic Strategy5Chiral-Unit-Oriented Design of Non-π-Conjugated Noncentrosymmetric Phosphates with Short Absorption Edges4Enhanced Birefringence and Excellent Thermal Stability in Two Tellurium(IV) Vanadates: KTeOVO4 and Ca2TeV2O95Second-Harmonic Generation in Organic–Inorganic Hybrid Cadmium Thiocyanates Containing Terminal Amino Acids22Phase-Matching Second-Harmonic Generation in Zero-Dimensional Zinc Thiocyanates Ligated with Chiral Amino Acids6Halogen-Driven Structural Engineering in Tellurium Oxyhalides: Enhanced SHG Response and Broad Optical Transparency6Chemical Composition Regulation for Tuning the Luminescent Properties of Organic–Inorganic Metal Halides7Chiral Ligand-Induced Second-Harmonic Generation Response in Helical One-Dimensional Hybrid Lead Bromides9Simultaneous Boosting of Second Harmonic Generation and Circularly Polarized Luminescence in Chiral Hybrid Metal Halides Through Enhanced Octahedral Distortion27Simultaneous Boosting of Second Harmonic Generation and Circularly Polarized Luminescence in Chiral Hybrid Metal Halides Through Enhanced Octahedral Distortion8Halide Ion-Directed Symmetry Control in π-Conjugated Molecular Crystals6Structural Evolution of Hybrid Bismuth-Based Halides toward Enhanced Second-Harmonic Generation Response and Birefringence through Multisite Chemical Substitution7Hydrogen Bond-Assisted Structural Regulation Enables Large Birefringence in Two Antimony Oxalofluoride Crystals5Record Second‐Harmonic Generation in a Lead‐Free 2D Hybrid Halide Perovskite13Remarkable Disparity of Second Harmonic Generation Response in Two Inorganic–Organic Hybrid Metal Thiocyanates5From (C12H9N2)2TeBr6·2H2O to (C12H9N2)2TeBr6: Dehydration-Driven Crystal Reorganization for Birefringence Optimization6Na6(SO4)2SiF6: A Stable Sulfate Fluosilicate with Wide Deep-Ultraviolet Transparency Window and Strong Second-Harmonic Generation Response4A 2D Double Perovskite Based on the Chiral Cystaminium Cation Exhibiting Multiple Switches in Quadratic Nonlinear Optical Response7Stepwise Substitution Strategy for Beryllium-Based Selenites with Enhanced SHG Response, Moderate Birefringence, and Short UV Cutoff Edges6Amino Acid Modification in One-Dimensional Cadmium Thiocyanates for Enhancing Second-Harmonic Generation Response2Chiral-Induced Spin Selectivity in Photocatalysis: Fundamentals and Emerging Opportunities14Chiral-Unit-Driven Short-Wave Ultraviolet Nonlinear Optical Acetates with Balanced Overall Optical Properties3A universal synthetic strategy for noncentrosymmetric lead oxyhalide frameworks with strong second-harmonic generation0Internally and externally induced chiral hybrid metal halide materials for advanced chiroptoelectronic applications23Second-harmonic generation in two hybrid organic–inorganic metal chlorides based on l -thioproline ligand1Second-harmonic generation responses in low-dimensional metal bromides functionalized with l -arginine1Supramolecular template modulation in chiral lead bromide hybrids toward enhanced second-harmonic generation0(C 6 H 7 N 2 O)NO 3 : π-Conjugation-Driven Synergistic Enhancement of Second-Harmonic Generation and Birefringence0Unlocking Strong SHG Response and Large Birefringence in Hybrid Antimony Halides via a Three-in-One Strategy7V-Shaped Pseudo-Chains Coupled with Lone-Pair-Distorted [GeX 3 ] − Units Enable Large Birefringence in Ge(II) Hybrid Halides2In-situ organic cation evolution driven sequential crystal transformation in hybrid metal halides1Chiral Nonlinear Optical Response in Achiral Quasi‐2D Perovskite Ferroelectric Featuring Unusually Large A‐Site Cation8Mixed Coordination and Pronounced Distortion Enabling Strong Nonlinear Optics in Chiral Lead Halides0Second-harmonic generation circular dichroism of chiral organic–inorganic hybrid metal halides: Insights and perspectives2Enhanced Birefringence in Organic–Inorganic Hybrid Antimony Halides via Partial Halogen Substitution1Halogen-Substitution-Modulated Lone-Pair Orientation in Sb(H 2 PO 2 ) 2 X (X = Cl, F) for Enhanced UV Birefringence1Crystal Structure of Two Bismuth(III) Bromide Complexes with Protonated L-Phenylalanine and L-Ornithine0Amino Acid-Directed Synthesis of Chiral Manganese Chlorides with One-Dimensional Helical Structures0Lateral‐Site Unblocking Enables Bilateral π ‐Chromophore Organization for Giant Birefringence in One‐Dimensional Lead Hybrids0Steric‐Guided Coordination Engineering Enables Significantly Optimized Optical Anisotropy via Sulfur‐Driven [C 5 H 5 NS] Birefringence‐Active Groups0Low-Dimensional Perovskites and Metal Halides across Structures and Functions: Connectivity, Dimensionality, and Emerging Principles1An Excellent Deep‐Ultraviolet Nonlinear Optical Crystal Realized via a Functional Group Based on a Two‐in‐One Strategy0Strong Second‐Order Nonlinear Optical Activities in Chiral Hybrid Copper(I) Bromide Microplates0

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  1. (C 13 N 3 H 14 ) 2 MBr 4 (M = Zn, Cd): two novel hybrid metal halides with balanced integrated nonlinear optical performance

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  2. Formation of iminium ions during the processing of metal halide perovskites

    Chemical Communications · 2024-01-01

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  3. RbSb(SO 4 )(H 2 PO 2 )F: a short-wave UV antimony( iii ) oxysalt with mixed-anions demonstrating enhanced birefringence

    Journal of Materials Chemistry C · 2024-01-01

    Jinwen Tan, Han Luo, Shiyi Wang, Ling Huang, Liling Cao, Xuehua Dong, Guohong Zou

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  4. Solvent-free synthesis and optical properties of two open-framework metal oxalates with zeolitic ABW and diamondoid topologies

    CrystEngComm · 2024-01-01

    Shuxian Guo, Sihan Liu, Xuemei Wen, Juan Cheng, Xin Wang, Hongmei Zeng, Guohong Zou, Zhien Lin

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  5. Multiple Functions of l -Thioproline in the Synthesis of Chiral Metal Bromides Showing Second-Harmonic-Generation Responses

    Inorganic Chemistry · 2024-04-23

    Peiqi Qian, Ying Li, Juan Cheng, Jing Li, Hongmei Zeng, Ling Huang, Guohong Zou, Zhien Lin

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  6. Optimization of Functional Building Blocks Generates a Substantial Improvement in Birefringence from Sn2OSO4 to Sn3O2(OH)(HSO4)

    Inorganic Chemistry · 2024-07-31

    Yuqi Chen, Han Luo, Zeqiao Yin, Xuehua Dong, Daojiang Gao, Yuqiao Zhou, Ling Huang, Liling Cao, Guohong Zou

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  7. l -Homoproline-Directed Synthesis of Organic–Inorganic Metal Iodides for Second Harmonic Generation

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    Juan Cheng, Gangji Yi, Peiqi Qian, Jing Li, Ling Huang, Hongmei Zeng, Guohong Zou, Zhien Lin

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  8. Chiral Metal Self‐Assemblies of Zirconium‐Tetrahedra and Their Second Harmonic Generation Activity

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  9. Chiral Metal Self‐Assemblies of Zirconium‐Tetrahedra and Their Second Harmonic Generation Activity

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  10. Chiral 0D hybrid lead-bromide perovskites with strong nonlinear chiroptical properties

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  11. Chiral-driven formation of hybrid cyanurates with large birefringence

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  12. Template Synthesis of Iodocuprate and Iodoargentate with Photocatalytic Activity and Second Harmonic Generation Efficiency

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    Meng-Yuan Xie, Tong Liu, Yu-Ying Xia, Qi Wei, Song‐De Han, Zhen‐Zhen Xue, Jie Pan

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  13. Two l -Proline Cadmium Thiocyanates with Moderate Second-Harmonic-Generation Responses and Large Birefringences

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  14. Novel antimony-based mixed halides exhibiting an excellent SHG response and a broad transmission range

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  15. Rational Design and Controlled Synthesis of High-Performance Inorganic Short-Wave UV Nonlinear Optical Materials

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  16. Strategically designed anisotropic organic–inorganic metal halides (OIMHs) with superior balance between bandgap and birefringence

    Inorganic Chemistry Frontiers · 2024-12-16

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  17. Bulk crystal growth and optical properties of a novel organic–inorganic hybrid nonlinear optical thiocyanate: [Mn(CH 3 CONH 2 ) 2 ] [Hg(SCN) 4 ]

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  18. Enhanced luminescence in 1D corrugated lead bromides via reduced flexibility of trivalent cations

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  19. Enhanced second-harmonic generation response in a chiral lead iodide induced by amino acid coordination

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  20. From poor-active to high performance via heteroleptic tetrahedra engineering: rational design of non-π-conjugated hybrids for phase-matchable ultraviolet nonlinear optics

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  21. Ligand substitution in organic–inorganic hybrid zinc iodides for second-harmonic generation

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  22. Strong second-harmonic generation response in an organic–inorganic hybrid antimony bromide

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  23. Extendable Synthesis of Organic Cations for In Situ Construction of Hybrid Metal Halides with Near‐Unity Photoluminescence and Strong Second Harmonic Generation

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  24. Extendable Synthesis of Organic Cations for In Situ Construction of Hybrid Metal Halides with Near‐Unity Photoluminescence and Strong Second Harmonic Generation

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  25. A Wide Band Gap Germanate with the Largest Second Harmonic Generation Response Created by Hypoxic Strategy

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  26. A Wide Band Gap Germanate with the Largest Second Harmonic Generation Response Created by Hypoxic Strategy

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  27. Chiral-Unit-Oriented Design of Non-π-Conjugated Noncentrosymmetric Phosphates with Short Absorption Edges

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  28. Enhanced Birefringence and Excellent Thermal Stability in Two Tellurium(IV) Vanadates: KTeOVO4 and Ca2TeV2O9

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  29. Second-Harmonic Generation in Organic–Inorganic Hybrid Cadmium Thiocyanates Containing Terminal Amino Acids

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  30. Phase-Matching Second-Harmonic Generation in Zero-Dimensional Zinc Thiocyanates Ligated with Chiral Amino Acids

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  31. Halogen-Driven Structural Engineering in Tellurium Oxyhalides: Enhanced SHG Response and Broad Optical Transparency

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  32. Chemical Composition Regulation for Tuning the Luminescent Properties of Organic–Inorganic Metal Halides

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  33. Chiral Ligand-Induced Second-Harmonic Generation Response in Helical One-Dimensional Hybrid Lead Bromides

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  34. Simultaneous Boosting of Second Harmonic Generation and Circularly Polarized Luminescence in Chiral Hybrid Metal Halides Through Enhanced Octahedral Distortion

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  35. Simultaneous Boosting of Second Harmonic Generation and Circularly Polarized Luminescence in Chiral Hybrid Metal Halides Through Enhanced Octahedral Distortion

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  36. Halide Ion-Directed Symmetry Control in π-Conjugated Molecular Crystals

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  37. Structural Evolution of Hybrid Bismuth-Based Halides toward Enhanced Second-Harmonic Generation Response and Birefringence through Multisite Chemical Substitution

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  38. Hydrogen Bond-Assisted Structural Regulation Enables Large Birefringence in Two Antimony Oxalofluoride Crystals

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  39. Record Second‐Harmonic Generation in a Lead‐Free 2D Hybrid Halide Perovskite

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  40. Remarkable Disparity of Second Harmonic Generation Response in Two Inorganic–Organic Hybrid Metal Thiocyanates

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  41. From (C12H9N2)2TeBr6·2H2O to (C12H9N2)2TeBr6: Dehydration-Driven Crystal Reorganization for Birefringence Optimization

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  42. Na6(SO4)2SiF6: A Stable Sulfate Fluosilicate with Wide Deep-Ultraviolet Transparency Window and Strong Second-Harmonic Generation Response

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  43. A 2D Double Perovskite Based on the Chiral Cystaminium Cation Exhibiting Multiple Switches in Quadratic Nonlinear Optical Response

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  44. Stepwise Substitution Strategy for Beryllium-Based Selenites with Enhanced SHG Response, Moderate Birefringence, and Short UV Cutoff Edges

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  45. Amino Acid Modification in One-Dimensional Cadmium Thiocyanates for Enhancing Second-Harmonic Generation Response

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  46. Chiral-Induced Spin Selectivity in Photocatalysis: Fundamentals and Emerging Opportunities

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  47. Chiral-Unit-Driven Short-Wave Ultraviolet Nonlinear Optical Acetates with Balanced Overall Optical Properties

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  48. A universal synthetic strategy for noncentrosymmetric lead oxyhalide frameworks with strong second-harmonic generation

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  49. Internally and externally induced chiral hybrid metal halide materials for advanced chiroptoelectronic applications

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  50. Second-harmonic generation in two hybrid organic–inorganic metal chlorides based on l -thioproline ligand

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