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RESEARCH PAPER · Frontiers in Chemistry · 2020

“Soft” Alkali Bromide and Iodide Fluxes for Crystal Growth

Vladislav V. Klepov, Christian A. Juillerat, Kristen A. Pace, Gregory W. Morrison, Hans‐Conrad zur Loye

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“Soft” Alkali Bromide and Iodide Fluxes for Crystal GrowthOriginalFacile Oxide to Chalcogenide Conversion for Actinides Using the Boron-Chalcogen Mixture Method38Covalency in Actinide Compounds78Dimensional reduction upon calcium incorporation in Cs 0.3 (Ca 0.3 Ln 0.7 )PS 4 and Cs 0.5 (Ca 0.5 Ln 0.5 )PS 45A novel promising infrared nonlinear optical selenide KAg 3 Ga 8 Se 14 designed from benchmark AgGaQ 2 (Q = S, Se)55A series of Rb 4 Ln 2 (P 2 S 6 )(PS 4 ) 2 (Ln = La, Ce, Pr, Nd, Sm, Gd) rare earth thiophosphates with two distinct thiophosphate units [P V S 4 ] 3− and [P IV 2 S 6 ] 4−16Synthesis-enabled exploration of chiral and polar multivalent quaternary sulfides37Trends in rare earth thiophosphate syntheses: Rb 3 Ln(PS 4 ) 2 (Ln = La, Ce, Pr), Rb 3−x Na x Ln(PS 4 ) 2 (Ln = Ce, Pr; x = 0.50, 0.55), and RbEuPS 4 obtained by molten flux crystal growth5Flux crystal growth of cesium bismuth silicates Cs3BiSi8O19 and Cs4Bi2Si8O21: Structure modification via Eu doping to yield Cs4Bi1.72Eu0.28Si8O21 and alkali metal ion exchange to yield Cs0.79K2.21BiSi8O190Pentanary cesium titanyl/titanate silicate oxyfluorides: Syntheses and structures2Predictive Synthesis54New Compounds and Phase Selection of Nickel Sulfides via Oxidation State Control in Molten Hydroxides20Synthesis, air stability and electrochemical investigation of lithium superionic bromine substituted argyrodite (Li6-xPS5-xCl1.0Brx) for all-solid-state lithium batteries59Li-Free ternary sulphide Cs 5 Ga 9 S 16 with excellent nonlinear optical performance similar to classic LiGaS 213Semiconducting silicon–phosphorus frameworks for caging exotic polycations10Uranyl Titanate Silicates: Syntheses, Structures, and Family Relations5Reactivity of FeMoO4 in CsCl Fluxes and Formation of the Salt-Inclusion Type of Compounds3Flux crystal growth of rubidium–iron silicates and germanates and their ion-exchange using alkali nitrate salts1A review of structures and physical properties of rare earth chalcophosphates78Discovery of chalcogenides structures and compositions using mixed fluxes53Polymorphism in A 3 MF 6 (A = Rb, Cs; M = Al, Ga) grown using mixed halide fluxes13Tunable Salt-Inclusion Chalcogenides for Ion Exchange, Photoluminescence, and Scintillation12Advances in Chalcogenide Crystal Growth: Flux and Solution Syntheses, and Approaches for Postsynthetic Modifications13Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides7Data-Driven Reactivity Predictions between a Solute and Solvent for Inorganic Crystal Growth in Solution0Solution-Growth Liquid-Phase Epitaxy of CsPbBr3 on NaCl by Optimizing the Substrate Dissolution2Cold sintering of nickel manganese oxide for thermistor fabrication9Crystal structure and magnetism of actinide oxides: a review22Molten flux growth of single crystals of quasi-1D hexagonal chalcogenide BaTiS310Bulk Crystal Growth and Single-Crystal-to-Single-Crystal Phase Transitions in the Averievite CsClCu5V2O105Revealing the effect of SrO addition on NH 3 -assisted SrCl 2 flux growth of SrTaO 2 N single crystals2Ionothermal Synthesis of Am 4 B 22 O 42 Cl 12 : A Chiral Cubic Americium Borate Cluster2Simultaneous encapsulation and structural behavior of high-utility CsPbX3 quantum dots in 3D dendritic mesoporous silica nanospheres3Investigation of Americium-Containing Phosphates, Silicates, Borates, Molybdates, and Fluorides Synthesized via High-Temperature Flux Crystal Growth6Centrosymmetric to noncentrosymmetric structure transition of the RbREP 2 Se 6 (RE = La–Nd, Sm, Ho–Yb) series: crystal growth, magnetic and optical properties4Compositional versatility and structural distortions in HfCuSi2-type pnictides0Crystal Growth of Quaternary RE 2 EuSi 2 S 8 ( RE = Ce–Nd, Sm, Gd, Tb) Using Flux-Assisted Boron Chalcogen Mixture (BCM) Method: Investigation of Magnetic and Luminescence Properties4

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  1. Facile Oxide to Chalcogenide Conversion for Actinides Using the Boron-Chalcogen Mixture Method

    Journal of the American Chemical Society · 2020-07-27

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  2. Covalency in Actinide Compounds

    Chemistry - A European Journal · 2020-12-06

    Kristen A. Pace, Vladislav V. Klepov, Anna A. Berseneva, Hans‐Conrad zur Loye

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  3. Dimensional reduction upon calcium incorporation in Cs 0.3 (Ca 0.3 Ln 0.7 )PS 4 and Cs 0.5 (Ca 0.5 Ln 0.5 )PS 4

    CrystEngComm · 2020-12-09

    Vladislav V. Klepov, Vancho Kocevski, Theodore M. Besmann, Hans‐Conrad zur Loye

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  4. A novel promising infrared nonlinear optical selenide KAg 3 Ga 8 Se 14 designed from benchmark AgGaQ 2 (Q = S, Se)

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    Jia-Nuo Li, Wen‐Dong Yao, Xiaohui Li, Wenlong Liu, Huaiguo Xue, Sheng‐Ping Guo

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  5. A series of Rb 4 Ln 2 (P 2 S 6 )(PS 4 ) 2 (Ln = La, Ce, Pr, Nd, Sm, Gd) rare earth thiophosphates with two distinct thiophosphate units [P V S 4 ] 3− and [P IV 2 S 6 ] 4−

    Dalton Transactions · 2021-01-01

    Ceren Kütahyalı Aslani, Logan S. Breton, Vladislav V. Klepov, Hans‐Conrad zur Loye

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  6. Synthesis-enabled exploration of chiral and polar multivalent quaternary sulfides

    Chemical Science · 2021-01-01

    Georgiy Akopov, Nethmi W. Hewage, Philip Yox, Gayatri Viswanathan, Shannon Lee, Liam Hulsebosch, Sarah D. Cady, Alexander L. Paterson, Frédéric A. Perras, Wenqian Xu, Kui Wu, Yaroslav Mudryk, Kirill A. Kovnir

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  7. Trends in rare earth thiophosphate syntheses: Rb 3 Ln(PS 4 ) 2 (Ln = La, Ce, Pr), Rb 3−x Na x Ln(PS 4 ) 2 (Ln = Ce, Pr; x = 0.50, 0.55), and RbEuPS 4 obtained by molten flux crystal growth

    CrystEngComm · 2021-01-01

    Logan S. Breton, Mark D. Smith, Hans‐Conrad zur Loye

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  8. Flux crystal growth of cesium bismuth silicates Cs3BiSi8O19 and Cs4Bi2Si8O21: Structure modification via Eu doping to yield Cs4Bi1.72Eu0.28Si8O21 and alkali metal ion exchange to yield Cs0.79K2.21BiSi8O19

    Solid State Sciences · 2021-05-10

    Adrian T. Hines, Gregory W. Morrison, Mark D. Smith, Hans‐Conrad zur Loye

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  9. Pentanary cesium titanyl/titanate silicate oxyfluorides: Syntheses and structures

    Solid State Sciences · 2021-06-05

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  10. Predictive Synthesis

    Chemistry of Materials · 2021-07-02

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  11. New Compounds and Phase Selection of Nickel Sulfides via Oxidation State Control in Molten Hydroxides

    Journal of the American Chemical Society · 2021-08-19

    Xiuquan Zhou, David J. Mandia, Hyowon Park, Mahalingam Balasubramanian, Lei Yu, Jianguo Wen, Andrey Andreevich Yakovenko, Duck Young Chung, Mercouri G. Kanatzidis

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  12. Synthesis, air stability and electrochemical investigation of lithium superionic bromine substituted argyrodite (Li6-xPS5-xCl1.0Brx) for all-solid-state lithium batteries

    Journal of Power Sources · 2021-12-02

    Yuvaraj Subramanian, Rajesh Rajagopal, Kwang‐Sun Ryu

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  13. Li-Free ternary sulphide Cs 5 Ga 9 S 16 with excellent nonlinear optical performance similar to classic LiGaS 2

    Inorganic Chemistry Frontiers · 2022-01-01

    Jin-Xu Zhao, Xiao‐Ming Jiang, Wen‐Fa Chen, Shao‐Min Pei, Bin‐Wen Liu, Guo‐Cong Guo

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  14. Semiconducting silicon–phosphorus frameworks for caging exotic polycations

    Chemical Communications · 2022-01-01

    Philip Yox, Andrew P. Porter, Rick W. Dorn, Victoria Kyveryga, Aaron J. Rossini, Kirill A. Kovnir

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  15. Uranyl Titanate Silicates: Syntheses, Structures, and Family Relations

    Crystal Growth & Design · 2022-01-14

    Gregory W. Morrison, Hans‐Conrad zur Loye

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  16. Reactivity of FeMoO4 in CsCl Fluxes and Formation of the Salt-Inclusion Type of Compounds

    Inorganic Chemistry · 2022-06-16

    Anna K. Weber, Martin Panthöfer, Angela Möller

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  17. Flux crystal growth of rubidium–iron silicates and germanates and their ion-exchange using alkali nitrate salts

    Solid State Sciences · 2022-08-27

    Mohammad Usman, Matthew S. Christian, Gregory W. Morrison, Mark D. Smith, Weiguo Zhang, Theodore M. Besmann, P. Shiv Halasyamani, Hans‐Conrad zur Loye

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  18. A review of structures and physical properties of rare earth chalcophosphates

    Coordination Chemistry Reviews · 2022-10-11

    Zi‐Xia Chen, Wenlong Liu, Sheng‐Ping Guo

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  19. Discovery of chalcogenides structures and compositions using mixed fluxes

    Nature · 2022-11-09

    Xiuquan Zhou, Venkata Surya Chaitanya Kolluru, Wenqian Xu, Luqing Wang, Tieyan Chang, Yu‐Sheng Chen, Lei Yu, Jianguo Wen, Maria K. Y. Chan, Duck Young Chung, Mercouri G. Kanatzidis

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  20. Polymorphism in A 3 MF 6 (A = Rb, Cs; M = Al, Ga) grown using mixed halide fluxes

    Dalton Transactions · 2023-01-01

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  21. Tunable Salt-Inclusion Chalcogenides for Ion Exchange, Photoluminescence, and Scintillation

    Chemistry of Materials · 2023-01-23

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  22. Advances in Chalcogenide Crystal Growth: Flux and Solution Syntheses, and Approaches for Postsynthetic Modifications

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  23. Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides

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  24. Data-Driven Reactivity Predictions between a Solute and Solvent for Inorganic Crystal Growth in Solution

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  25. Solution-Growth Liquid-Phase Epitaxy of CsPbBr3 on NaCl by Optimizing the Substrate Dissolution

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  27. Crystal structure and magnetism of actinide oxides: a review

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  28. Molten flux growth of single crystals of quasi-1D hexagonal chalcogenide BaTiS3

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  29. Bulk Crystal Growth and Single-Crystal-to-Single-Crystal Phase Transitions in the Averievite CsClCu5V2O10

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  30. Revealing the effect of SrO addition on NH 3 -assisted SrCl 2 flux growth of SrTaO 2 N single crystals

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  31. Ionothermal Synthesis of Am 4 B 22 O 42 Cl 12 : A Chiral Cubic Americium Borate Cluster

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  32. Simultaneous encapsulation and structural behavior of high-utility CsPbX3 quantum dots in 3D dendritic mesoporous silica nanospheres

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  33. Investigation of Americium-Containing Phosphates, Silicates, Borates, Molybdates, and Fluorides Synthesized via High-Temperature Flux Crystal Growth

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  36. Crystal Growth of Quaternary RE 2 EuSi 2 S 8 ( RE = Ce–Nd, Sm, Gd, Tb) Using Flux-Assisted Boron Chalcogen Mixture (BCM) Method: Investigation of Magnetic and Luminescence Properties

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