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RESEARCH PAPER · Inorganic Chemistry · 2019

Mild Hydrothermal Synthesis of the Complex Hafnium-Containing Fluorides Cs2[M(H2O)6][Hf2F12] (M = Ni, Co, Zn), CuHfF6(H2O)4, and Cs2Hf3Mn3F20 Based on HfF7 and HfF6 Coordination Polyhedra

Gyanendra B. Ayer, Vladislav V. Klepov, Mark D. Smith, Hans‐Conrad zur Loye

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Mild Hydrothermal Synthesis of the Complex Hafnium-Containing Fluorides Cs2[M(H2O)6][Hf2F12] (M = Ni, Co, Zn), CuHfF6(H2O)4, and Cs2Hf3Mn3F20 Based on HfF7 and HfF6 Coordination PolyhedraOriginalBaWO 2 F 4 : a mixed anion X-ray scintillator with excellent photoluminescence quantum efficiency18Quaternary cerium( iv ) containing fluorides exhibiting Ce 3 F 16 sheets and Ce 6 F 30 frameworks16Hydrothermal synthesis and properties of MMF5(H2O)7 (M = Co2+ and Ni2+, M = Mn3+, Ga3+, and In3+)8Flux crystal growth of cesium bismuth silicates Cs3BiSi8O19 and Cs4Bi2Si8O21: Structure modification via Eu doping to yield Cs4Bi1.72Eu0.28Si8O21 and alkali metal ion exchange to yield Cs0.79K2.21BiSi8O190Chloride Reduction of Mn3+ in Mild Hydrothermal Synthesis of a Charge Ordered Defect Pyrochlore, CsMn2+Mn3+F6, a Canted Antiferromagnet with a Hard Ferromagnetic Component22A Geometrically Frustrated Family of MIIMIIIF5(H2O)2 Mixed–Metal Fluorides with Complex Magnetic Interactions14Synthesis of Hydrated Ternary Lanthanide-Containing Chlorides Exhibiting X-ray Scintillation and Luminescence7Luminescence and Scintillation of [Nb2O2F9]3–-Dimer-Containing Oxide–Fluorides: Cs10(Nb2O2F9)3F, Cs9.4K0.6(Nb2O2F9)3F, and Cs10(Nb2O2F9)3Cl5Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides7Crystal Growth and Magnetism of Transition Metal Pyrochlore Fluorides7Crystal Growth and Characterization of the Rare Earth Fluoride Carbonates NaLnCO3F2 (Ln = Eu–Lu)5Sensitivity of Mild Hydrothermal Synthesis to the Reaction Conditions: Targeting Mixed-Metal Hexagonal Tungsten Bronze Fluorides AxM2+xM3+(1–x)F3 to Investigate Their Magnetic Behavior3From Magnetic Chains to Sheets: The Impact of Hydrofluoric Acid Quantities in Mild Hydrothermal Synthesis on Mixed-Metal Fluoride Formation2Mild Hydrothermal Synthesis of Zirconium-Containing Fluorides: K 2 [ M (H 2 O) 6 ][Zr 2 F 12 ] ( M = Fe, Co), Rb 2 [ M (H 2 O) 6 ][Zr 2 F 12 ] ( M = Fe, Co, Ni, Cu, Zn), Cs 2 [ M (H 2 O) 6 ][Zr 2 F 12 ] ( M = Fe, Co, Ni), and Cs 2 Zr 3 Mn 3 F 200

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  1. BaWO 2 F 4 : a mixed anion X-ray scintillator with excellent photoluminescence quantum efficiency

    Dalton Transactions · 2020-01-01

    Gyanendra B. Ayer, Vladislav V. Klepov, Mark D. Smith, Ming Hu, Zhonghua Yang, Corey R. Martin, Gregory W. Morrison, Hans‐Conrad zur Loye

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  2. Quaternary cerium( iv ) containing fluorides exhibiting Ce 3 F 16 sheets and Ce 6 F 30 frameworks

    Dalton Transactions · 2020-01-01

    Gyanendra B. Ayer, Vladislav V. Klepov, Kristen A. Pace, Hans‐Conrad zur Loye

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  3. Hydrothermal synthesis and properties of MMF5(H2O)7 (M = Co2+ and Ni2+, M = Mn3+, Ga3+, and In3+)

    Solid State Sciences · 2020-08-07

    Navindra Keerthisinghe, Vladislav V. Klepov, Eric Zhang, Mark D. Smith, Shani Egodawatte, Stephen H. Foulger, Hans‐Conrad zur Loye

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  4. Flux crystal growth of cesium bismuth silicates Cs3BiSi8O19 and Cs4Bi2Si8O21: Structure modification via Eu doping to yield Cs4Bi1.72Eu0.28Si8O21 and alkali metal ion exchange to yield Cs0.79K2.21BiSi8O19

    Solid State Sciences · 2021-05-10

    Adrian T. Hines, Gregory W. Morrison, Mark D. Smith, Hans‐Conrad zur Loye

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  5. Chloride Reduction of Mn3+ in Mild Hydrothermal Synthesis of a Charge Ordered Defect Pyrochlore, CsMn2+Mn3+F6, a Canted Antiferromagnet with a Hard Ferromagnetic Component

    Journal of the American Chemical Society · 2021-07-26

    Vladislav V. Klepov, Kristen A. Pace, Anna A. Berseneva, Justin B. Felder, Stuart Calder, Gregory W. Morrison, Qiang Zhang, Melanie Kirkham, David Parker, Hans‐Conrad zur Loye

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  6. A Geometrically Frustrated Family of MIIMIIIF5(H2O)2 Mixed–Metal Fluorides with Complex Magnetic Interactions

    Inorganic Chemistry · 2021-09-01

    Navindra Keerthisinghe, Anna A. Berseneva, Vladislav V. Klepov, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  7. Synthesis of Hydrated Ternary Lanthanide-Containing Chlorides Exhibiting X-ray Scintillation and Luminescence

    Inorganic Chemistry · 2021-10-07

    Gyanendra B. Ayer, Mark D. Smith, Luiz Gustavo Jacobsohn, Gregory W. Morrison, Hunter B. Tisdale, Logan S. Breton, Weiguo Zhang, P. Shiv Halasyamani, Hans‐Conrad zur Loye

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  8. Luminescence and Scintillation of [Nb2O2F9]3–-Dimer-Containing Oxide–Fluorides: Cs10(Nb2O2F9)3F, Cs9.4K0.6(Nb2O2F9)3F, and Cs10(Nb2O2F9)3Cl

    Inorganic Chemistry · 2022-02-09

    Gyanendra B. Ayer, Gregory W. Morrison, Mark D. Smith, Luiz Gustavo Jacobsohn, Hans‐Conrad zur Loye

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  9. Comparative Study on Crystal Structures and Synthetic Techniques of Ternary Hafnium/Zirconium Fluorides

    Inorganic Chemistry · 2023-07-18

    Navindra Keerthisinghe, Gyanendra B. Ayer, Mark D. Smith, Hans‐Conrad zur Loye

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  10. Crystal Growth and Magnetism of Transition Metal Pyrochlore Fluorides

    Inorganic Chemistry · 2023-08-15

    Lakshani W. Masachchi, Navindra Keerthisinghe, Gregory W. Morrison, Anna A. Berseneva, Mark D. Smith, Hans‐Conrad zur Loye

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  11. Crystal Growth and Characterization of the Rare Earth Fluoride Carbonates NaLnCO3F2 (Ln = Eu–Lu)

    Crystal Growth & Design · 2024-08-06

    Navindra Keerthisinghe, Gregory W. Morrison, Hans‐Conrad zur Loye

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  12. Sensitivity of Mild Hydrothermal Synthesis to the Reaction Conditions: Targeting Mixed-Metal Hexagonal Tungsten Bronze Fluorides AxM2+xM3+(1–x)F3 to Investigate Their Magnetic Behavior

    Inorganic Chemistry · 2024-09-04

    Lakshani W. Masachchi, Navindra Keerthisinghe, Anna A. Berseneva, Gregory W. Morrison, Mark D. Smith, Logan S. Breton, Juliano Schorne Pinto, Mina Aziziha, Hans‐Conrad zur Loye

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  13. From Magnetic Chains to Sheets: The Impact of Hydrofluoric Acid Quantities in Mild Hydrothermal Synthesis on Mixed-Metal Fluoride Formation

    Chemistry of Materials · 2025-02-18

    Navindra Keerthisinghe, Gregory W. Morrison, Logan S. Breton, Mark D. Smith, Qiang Zhang, Melanie Kirkham, Vladislav V. Klepov, Hans‐Conrad zur Loye

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  14. Mild Hydrothermal Synthesis of Zirconium-Containing Fluorides: K 2 [ M (H 2 O) 6 ][Zr 2 F 12 ] ( M = Fe, Co), Rb 2 [ M (H 2 O) 6 ][Zr 2 F 12 ] ( M = Fe, Co, Ni, Cu, Zn), Cs 2 [ M (H 2 O) 6 ][Zr 2 F 12 ] ( M = Fe, Co, Ni), and Cs 2 Zr 3 Mn 3 F 20

    Inorganic Chemistry · 2026-06-30

    Timothy E. Whitesell, Hope Eden Catalano, Mark D. Smith, Hans‐Conrad zur Loye

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