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RESEARCH PAPER · Chem · 2018

Reversible Mg-Ion Insertion in a Metastable One-Dimensional Polymorph of V2O5

Justin L. Andrews, Arijita Mukherjee, Hyun Deog Yoo, Abhishek Parija, Peter M. Marley, Sirine C. Fakra, David Prendergast, Jordi Cabana, Robert F. Klie, Sarbajit Banerjee

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Reversible Mg-Ion Insertion in a Metastable One-Dimensional Polymorph of V2O5OriginalStriping modulations and strain gradients within individual particles of a cathode material upon lithiation23Magnifying Opportunities in Mg Batteries through Metastability3Defining Diffusion Pathways in Intercalation Cathode Materials: Some Lessons from V2O5 on Directing Cation Traffic103Traversing Energy Landscapes Away from Equilibrium: Strategies for Accessing and Utilizing Metastable Phase Space94Physical properties of silicene electrodes for Li-, Na-, Mg-, and K-ion batteries35Roadblocks in Cation Diffusion Pathways: Implications of Phase Boundaries for Li-Ion Diffusivity in an Intercalation Cathode Material34Probing spatial coupling of resistive modes in porous intercalation electrodes through impedance spectroscopy31Novel NaTi2(PO4)3 nanowire clusters as high performance cathodes for Mg-Na hybrid-ion batteries53Hole Extraction by Design in Photocatalytic Architectures Interfacing CdSe Quantum Dots with Topochemically Stabilized Tin Vanadium Oxide47It’s Not Over until the Big Ion Dances: Potassium Gets Its Groove On19The Middle Road Less Taken: Electronic-Structure-Inspired Design of Hybrid Photocatalytic Platforms for Solar Fuel Generation37Directing Mg-Storage Chemistry in Organic Polymers toward High-Energy Mg Batteries200Formation of Magnesium Dendrites during Electrodeposition333Chemo-mechanical degradation in V 2 O 5 thin film cathodes of Li-ion batteries during electrochemical cycling38Fast magnesiation kinetics in α-Ag 2 S nanostructures enabled by an in situ generated silver matrix34Magnesium Batteries23Manganese ion pre-intercalated hydrated vanadium oxide as a high-performance cathode for magnesium ion batteries91Mg 2+ storage and mobility in anatase TiO 2 : the role of frustrated coordination22Phase stability of intercalated V 2 O 5 battery cathodes elucidated through the Goldschmidt tolerance factor10In Operando Synchrotron Diffraction and in Operando X-ray Absorption Spectroscopy Investigations of Orthorhombic V2O5 Nanowires as Cathode Materials for Mg-Ion Batteries106Status and Outlook for Magnesium Battery Technologies: A Conversation with Stan Whittingham and Sarbajit Banerjee39Prototype rechargeable magnesium batteries using ionic liquid electrolytes64Vanadium Oxide Pillared by Interlayer Mg2+ Ions and Water as Ultralong-Life Cathodes for Magnesium-Ion Batteries298Intercalation of Magnesium into a Layered Vanadium Oxide with High Capacity100A High‐Rate Rechargeable Mg Battery Based on AgCl Conversion Cathode with Fast Solid‐State Mg2+ Diffusion Kinetics17Surfactant induced formation of flower-like V2O5 microspheres as cathode materials for rechargeable magnesium batteries14Building Brain-Inspired Logic Circuits from Dynamically Switchable Transition-Metal Oxides70Chemical Flexibility of Mg in Pnictide Materials: Structure and Properties Diversity27Atomic-scale observation of phase transition of MgMn2O4 cubic spinel upon the charging in Mg-ion battery36Low-cost MgFexMn2-xO4 cathode materials for high-performance aqueous rechargeable magnesium-ion batteries137The Influence of Surface Stress on the Chemo-Mechanical Behavior of Inverse-Opal-Structured Electrodes for Lithium-Ion Batteries3A robust ionic liquid magnesium electrolyte enabling Mg/S batteries32Crystal regulation towards rechargeable magnesium battery cathode materials102Electro-insertion of Mn 2+ ions into V 2 O 5 · n H 2 O on MWCNTs coated carbon felt for binder-free Na + ion battery electrodes25Enhanced charge storage of nanometric ζ-V 2 O 5 in Mg electrolytes23Interfaces in rechargeable magnesium batteries32Valence-to-core X-ray emission spectroscopy of vanadium oxide and lithiated vanadyl phosphate materials18Metal-Insulator Transitions in β′-CuxV2O5 Mediated by Polaron Oscillation and Cation Shuttling17Designing catalysts for water splitting based on electronic structure considerations69Decreasing the Ion Diffusion Pathways for the Intercalation of Multivalent Cations into One-Dimensional TiS2 Nanobelt Arrays19Recent Advances in Rechargeable Magnesium‐Based Batteries for High‐Efficiency Energy Storage241Alloy Anode Materials for Rechargeable Mg Ion Batteries252Fast and stable Mg2+ intercalation in a high voltage NaV2O2(PO4)2F/rGO cathode material for magnesium-ion batteries60Energy storage emerging: A perspective from the Joint Center for Energy Storage Research344An Atomic View of Cation Diffusion Pathways from Single‐Crystal Topochemical Transformations36An Atomic View of Cation Diffusion Pathways from Single‐Crystal Topochemical Transformations3Intercalation of Mg into a Few-Layer Phyllomanganate in Nonaqueous Electrolytes at Room Temperature4Water‐Pillared Sodium Vanadium Bronze Nanowires for Enhanced Rechargeable Magnesium Ion Storage58Ab initio investigation of α- and ζ-V2O5 for beyond lithium ion battery cathodes21Reversible Room-Temperature Fluoride-Ion Insertion in a Tunnel-Structured Transition Metal Oxide Host29Probing Mg Intercalation in the Tetragonal Tungsten Bronze Framework V4Nb18O559Rationally Designed Vanadium Pentoxide as High Capacity Insertion Material for Mg‐Ion63Current status and future directions of multivalent metal-ion batteries1519High Capacity for Mg2+ Deintercalation in Spinel Vanadium Oxide Nanocrystals67Solution‐Processed All‐V2O5 Battery7Electrochemical synthesis and structural characterization of nanostructured V 2 O 5 .nH 2 O on CNTs coated/uncoated carbon felt composite15Curvature-Induced Modification of Mechano-Electrochemical Coupling and Nucleation Kinetics in a Cathode Material30Pseudocapacitive Ti-Doped Niobium Pentoxide Nanoflake Structure Design for a Fast Kinetics Anode toward a High-Performance Mg-Ion-Based Dual-Ion Battery52Does Water Enhance Mg Intercalation in Oxides? The Case of a Tunnel Framework17Magnesium batteries: Current picture and missing pieces of the puzzle114Hydrated MgxV5O12 Cathode with Improved Mg2+ Storage Performance58Intercalation-Type V2O3 with Fast Mg2+ Diffusion Kinetics for High-Capacity and Long-Life Mg-Ion Storage21Recent Progress and Challenges in the Optimization of Electrode Materials for Rechargeable Magnesium Batteries90Control of crystal size tailors the electrochemical performance of α-V 2 O 5 as a Mg 2+ intercalation host12Fast lithium-ion conductivity in the ‘empty-perovskite’ n = 2 Ruddlesden–Popper-type oxysulphide Y 2 Ti 2 S 2 O 514The Quest for Functional Oxide Cathodes for Magnesium Batteries: A Critical Perspective77Ab initio random structure searching for battery cathode materials41Kinetic 2D Crystals via Topochemical Approach29Advancing Electrolyte Solution Chemistry and Interfacial Electrochemistry of Divalent Metal Batteries32Database of ab initio L-edge X-ray absorption near edge structure51Maximizing Magnesiation Capacity of Nanowire Cluster Oxides by Conductive Macromolecule Pillaring and Multication Intercalation47An Aqueous Mg2+‐Based Dual‐Ion Battery with High Power Density70In Situ and Operando Analyses of Reaction Mechanisms in Vanadium Oxides for Li‐, Na‐, Zn‐, and Mg‐Ions Batteries55Lessons learned from FeSb2O4 on stereoactive lone pairs as a design principle for anion insertion17Assessing the role of vanadium technologies in decarbonizing hard-to-abate sectors and enabling the energy transition34Research on the Effects of Sn Dopants of V2O5 Based on the First Principles7Recent advances in Mg-Li and Mg-Na hybrid batteries83Synthesis and Characterization of Magnesium Vanadates as Potential Magnesium‐Ion Cathode Materials through an Ab Initio Guided Carbothermal Reduction Approach**3Facilitating Mg2+ diffusion in high potential LixV2(PO4)3 cathode material with a co-insertion strategy for rechargeable Mg-ion batteries24Synthesis and Characterization of Magnesium Vanadates as Potential Magnesium‐Ion Cathode Materials through an Ab Initio Guided Carbothermal Reduction Approach**13Cathode Materials for Rechargeable Magnesium-Ion Batteries: A Review17Hydrated eutectic electrolytes for high-performance Mg-ion batteries129In situ crafting of a 3D N-doped carbon/defect-rich V 2 O 5− x · n H 2 O nanosheet composite for high performance fibrous flexible Zn-ion batteries21Topochemical stabilization and single-crystal transformations of a metastable 2D γʹ-V2O5 intercalation cathode19High‐Voltage Aqueous Mg‐Ion Batteries Enabled by Solvation Structure Reorganization124Anionic Te-Substitution Boosting the Reversible Redox in CuS Nanosheet Cathodes for Magnesium Storage113High‐Performance Mg−Li Hybrid Batteries Based on Pseudocapacitive Anatase Ti1‐xCoxO2‐y Nanosheet Cathodes18Cation reordering instead of phase transitions: Origins and implications of contrasting lithiation mechanisms in 1D ζ- and 2D α-V 2 O 524Flexible three-dimensional-networked iron vanadate nanosheet arrays/carbon cloths as high-performance cathodes for magnesium ion batteries30Highly reversible electrochemical magnesium/lithium insertion performance in TiO2(B) nanosheets with Ti cationic vacancies30Stability of Wadsley-type vanadium oxides V2O5 and V6O13 at high pressures14A deep learned nanowire segmentation model using synthetic data augmentation43Switchable and Strain‐Releasable Mg‐Ion Diffusion Nanohighway Enables High‐Capacity and Long‐Life Pyrovanadate Cathode14Crystallographic Design of Intercalation Materials12Recent advances in solid-state beyond lithium batteries34Unconventional Charge Transport in MgCr2O4 and Implications for Battery Intercalation Hosts26Synthesis and Mg2+ deintercalation in manganese spinel nanocrystals1Octylamine‐Supporting Interlayer Expanded Molybdenum Diselenide as a High‐Power Cathode for Rechargeable Mg Batteries18Electrochemical generation of birnessite MnO2 nanoflowers for intercalation of Mg2+ ions32Multifunctional 1D Nanostructures toward Future Batteries: A Comprehensive Review91β-V2O5 as Magnesium Intercalation Cathode28Enhanced Li-ion migration behavior in Li3V2O5 rock-salt anode via stepwise lattice tailoring43V2O5 as a versatile electrode material for postlithium energy storage systems29Interlayer engineering in V 6 O 13 nanobelts toward superior Mg-ion storage13Fundamentals and Scientific Challenges in Structural Design of Cathode Materials for Zinc‐Ion Hybrid Supercapacitors242Chemistry–mechanics–geometry coupling in positive electrode materials: a scale-bridging perspective for mitigating degradation in lithium-ion batteries through materials design51Vanadium-based cathode materials for rechargeable magnesium batteries28Current material design strategies on the copper chalcogenide cathodes for rechargeable magnesium batteries: a review17Ab Initio Study of the Electronic Properties of a Silicene Anode Subjected to Transmutation Doping9Structural, Morphological and Interfacial Investigation of H2V3O8 upon Mg2+ Intercalation3A critical review of vanadium-based electrode materials for rechargeable magnesium batteries45Intercalant-induced V t 2 g orbital occupation in vanadium oxide cathode toward fast-charging aqueous zinc-ion batteries116Solid Batteries Chemistries Beyond Lithium2Thermolysis-Driven Growth of Vanadium Oxide Nanostructures Revealed by In Situ Transmission Electron Microscopy: Implications for Battery Applications14Cathode Materials and Chemistries for Magnesium Batteries: Challenges and Opportunities120Structural Transformations at the Atomic Scale in Spinel Vanadium Oxides upon Mg2+ Extraction5Amorphous Vanadium Oxide Nanosheets with Alterable Polyhedron Configuration for Fast‐Charging Lithium‐Ion Batteries17Structure Evolution of V 2 O 5 as Electrode Materials for Metal‐Ion Batteries33Layered Materials in the Magnesium Ion Batteries: Development History, Materials Structure, and Energy Storage Mechanism24Research advances of the electrolytes for rechargeable magnesium ion batteries26Unraveling the Role of Hydrogen Insertion in Enhancing the Electrochemical Performance of the V2O5 Cathode for Mg-Ion Batteries: A First-Principles Study73D π–d Conjugated Coordination Polymer Enabling Ultralong Life Magnesium‐Ion Storage30Potassium ion pre-intercalated MnO2 for aqueous multivalent ion batteries13Amorphous quantum dots enable V2O5 with superior Mg storage4Nitridation-boosted V e g occupation of a VN@CNT flexible electrode for high-rate Zn-ion hybrid supercapacitors4Review—Advanced Secondary Batteries with Multi-Electron Reaction of Light Elements2Securing cation vacancies to enable reversible Mg insertion/extraction in rocksalt oxides11Strategies to alleviate distortive phase transformations in Li-ion intercalation reactions: an example with vanadium pentoxide15Mitigating Interfacial Capacity Fading in Vanadium Pentoxide by Sacrificial Vanadium Sulfide Encapsulation for Rechargeable Mg‐Ion Batteries11Ca2+ pre-intercalated bilayered vanadium oxide for high-performance aqueous Mg-ion batteries30Effect of pre-intercalation on Li-ion diffusion mapped by topochemical single-crystal transformation and operando investigation40CuS-based composite for high-performance magnesium storage with a clarified charge-discharge mechanism9Research status and prospect of rechargeable magnesium ion batteries cathode materials19Highly cycle-stable VOPO4-based cathodes for magnesium ion batteries: Insight into the role of interlayer engineering in batteries performance17Freestanding Ammonium Vanadate Composite Cathodes with Lattice Self‐Regulation and Ion Exchange for Long‐Lasting Ca‐Ion Batteries36Synergistic tailoring of adsorption and vacancy enrichment in lamellar stacked layers of α-MoO3 nanorods by Mg2+ for NO2 gas sensor15Unlocking zinc storage in silver vanadate structures for high-performance aqueous zinc batteries7Boosting proton intercalation via sulfur anion doping in V2O3 cathode materials towards high capacity and rate performance of aqueous zinc ion batteries45Progress and Challenges of Vanadium Oxide Cathodes for Rechargeable Magnesium Batteries17Monoclinic Silver Vanadate (Ag0.33V2O5) as a High‐Capacity Stable Cathode Material for Aqueous Manganese Batteries29Unraveling the Ionic Storage Mechanism of Flexible Nitrogen‐Doped MXene Films for High‐Performance Aqueous Hybrid Supercapacitors63Na+ Preintercalated Bilayered V2O5 Cathode Materials for Na-Ion Batteries7Study of the Physical Properties of the New Spinel Oxide NaMgMn₂O₄ Material1A Study on Oxygen Vacancy Resistance Mechanism of V2O54Enhanced dynamics of Al3+/H+ ions in aqueous aluminum ion batteries: Construction of metastable structures in vanadium pentoxide upon oxygen vacancies17Constructing Sulfur‐Heterocyclic Aromatic Amine Polymer with Multiple‐Redox Active Sites for Long‐Lifespan and All‐Organic Aqueous Magnesium Ion Batteries46Divalent Metal-Ion Batteries as Alternatives to Li-Ion Based Energy Storage0Engineering Heterointerface to Synergistically Regulate Kinetics and Stress of Copper–Cobalt Selenide toward Reversible Magnesium/Lithium Hybrid Batteries17Carbonyl-rich organic conjugated polymer as an ultra-stable and high-capacity cathode material for Mg-Li dual-ion batteries12Combined Displacement/Intercalation Mechanism of Ag 0.33 V 2 O 5 Cathode for Rechargeable Zinc‐Ion Batteries3

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  1. Striping modulations and strain gradients within individual particles of a cathode material upon lithiation

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  2. Magnifying Opportunities in Mg Batteries through Metastability

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  3. Defining Diffusion Pathways in Intercalation Cathode Materials: Some Lessons from V2O5 on Directing Cation Traffic

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  4. Traversing Energy Landscapes Away from Equilibrium: Strategies for Accessing and Utilizing Metastable Phase Space

    The Journal of Physical Chemistry C · 2018-07-06

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  5. Physical properties of silicene electrodes for Li-, Na-, Mg-, and K-ion batteries

    Journal of Solid State Electrochemistry · 2018-07-20

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  6. Roadblocks in Cation Diffusion Pathways: Implications of Phase Boundaries for Li-Ion Diffusivity in an Intercalation Cathode Material

    ACS Applied Materials & Interfaces · 2018-08-14

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  7. Probing spatial coupling of resistive modes in porous intercalation electrodes through impedance spectroscopy

    Physical Chemistry Chemical Physics · 2018-10-19

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  8. Novel NaTi2(PO4)3 nanowire clusters as high performance cathodes for Mg-Na hybrid-ion batteries

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  9. Hole Extraction by Design in Photocatalytic Architectures Interfacing CdSe Quantum Dots with Topochemically Stabilized Tin Vanadium Oxide

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  10. It’s Not Over until the Big Ion Dances: Potassium Gets Its Groove On

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  11. The Middle Road Less Taken: Electronic-Structure-Inspired Design of Hybrid Photocatalytic Platforms for Solar Fuel Generation

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  12. Directing Mg-Storage Chemistry in Organic Polymers toward High-Energy Mg Batteries

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  13. Formation of Magnesium Dendrites during Electrodeposition

    ACS Energy Letters · 2018-12-26

    Rachel D. Davidson, Ankit Verma, David A. Santos, Feng Hao, Cole D. Fincher, Sisi Xiang, Jonathan S. Van Buskirk, Kelvin Y. Xie, Matt Pharr, Partha P. Mukherjee, Sarbajit Banerjee

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  14. Chemo-mechanical degradation in V 2 O 5 thin film cathodes of Li-ion batteries during electrochemical cycling

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    Yuwei Zhang, Yuting Luo, Cole D. Fincher, Sarbajit Banerjee, Matt Pharr

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  15. Fast magnesiation kinetics in α-Ag 2 S nanostructures enabled by an in situ generated silver matrix

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  16. Magnesium Batteries

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  17. Manganese ion pre-intercalated hydrated vanadium oxide as a high-performance cathode for magnesium ion batteries

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  18. Mg 2+ storage and mobility in anatase TiO 2 : the role of frustrated coordination

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  19. Phase stability of intercalated V 2 O 5 battery cathodes elucidated through the Goldschmidt tolerance factor

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  20. In Operando Synchrotron Diffraction and in Operando X-ray Absorption Spectroscopy Investigations of Orthorhombic V2O5 Nanowires as Cathode Materials for Mg-Ion Batteries

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  21. Status and Outlook for Magnesium Battery Technologies: A Conversation with Stan Whittingham and Sarbajit Banerjee

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  22. Prototype rechargeable magnesium batteries using ionic liquid electrolytes

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  23. Vanadium Oxide Pillared by Interlayer Mg2+ Ions and Water as Ultralong-Life Cathodes for Magnesium-Ion Batteries

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  24. Intercalation of Magnesium into a Layered Vanadium Oxide with High Capacity

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  25. A High‐Rate Rechargeable Mg Battery Based on AgCl Conversion Cathode with Fast Solid‐State Mg2+ Diffusion Kinetics

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  26. Surfactant induced formation of flower-like V2O5 microspheres as cathode materials for rechargeable magnesium batteries

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  27. Building Brain-Inspired Logic Circuits from Dynamically Switchable Transition-Metal Oxides

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  28. Chemical Flexibility of Mg in Pnictide Materials: Structure and Properties Diversity

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  29. Atomic-scale observation of phase transition of MgMn2O4 cubic spinel upon the charging in Mg-ion battery

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  30. Low-cost MgFexMn2-xO4 cathode materials for high-performance aqueous rechargeable magnesium-ion batteries

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  31. The Influence of Surface Stress on the Chemo-Mechanical Behavior of Inverse-Opal-Structured Electrodes for Lithium-Ion Batteries

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  32. A robust ionic liquid magnesium electrolyte enabling Mg/S batteries

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  33. Crystal regulation towards rechargeable magnesium battery cathode materials

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  34. Electro-insertion of Mn 2+ ions into V 2 O 5 · n H 2 O on MWCNTs coated carbon felt for binder-free Na + ion battery electrodes

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  35. Enhanced charge storage of nanometric ζ-V 2 O 5 in Mg electrolytes

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  36. Interfaces in rechargeable magnesium batteries

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  37. Valence-to-core X-ray emission spectroscopy of vanadium oxide and lithiated vanadyl phosphate materials

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  38. Metal-Insulator Transitions in β′-CuxV2O5 Mediated by Polaron Oscillation and Cation Shuttling

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  39. Designing catalysts for water splitting based on electronic structure considerations

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  40. Decreasing the Ion Diffusion Pathways for the Intercalation of Multivalent Cations into One-Dimensional TiS2 Nanobelt Arrays

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  41. Recent Advances in Rechargeable Magnesium‐Based Batteries for High‐Efficiency Energy Storage

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  42. Alloy Anode Materials for Rechargeable Mg Ion Batteries

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  43. Fast and stable Mg2+ intercalation in a high voltage NaV2O2(PO4)2F/rGO cathode material for magnesium-ion batteries

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  44. Energy storage emerging: A perspective from the Joint Center for Energy Storage Research

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    Lynn Trahey, Fikile Richard Brushett, Nitash P. Balsara, Gerbrand Ceder, Lei Cheng, Yet‐Ming Chiang, Nathan T. Hahn, Brian J. Ingram, Shelley D. Minteer, Jeffrey S. Moore, Karl Todd Mueller, Linda F. Nazar, Kristin Aslaug Persson, Donald J. Siegel, Kang Xu, Kevin R. Zavadil, Venkat N. Srinivasan, G. W. Crabtree

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  45. An Atomic View of Cation Diffusion Pathways from Single‐Crystal Topochemical Transformations

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  46. An Atomic View of Cation Diffusion Pathways from Single‐Crystal Topochemical Transformations

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  47. Intercalation of Mg into a Few-Layer Phyllomanganate in Nonaqueous Electrolytes at Room Temperature

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  48. Water‐Pillared Sodium Vanadium Bronze Nanowires for Enhanced Rechargeable Magnesium Ion Storage

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  49. Ab initio investigation of α- and ζ-V2O5 for beyond lithium ion battery cathodes

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  50. Reversible Room-Temperature Fluoride-Ion Insertion in a Tunnel-Structured Transition Metal Oxide Host

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