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RESEARCH PAPER · Chemical Communications · 2001

Intercalation and controlled release of pharmaceutically active compounds from a layered double hydroxide.

Aamir I. Khan, Lixu Lei, Alexander J. Norquist, Dermot O’Hare

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Intercalation and controlled release of pharmaceutically active compounds from a layered double hydroxide.OriginalIntercalation chemistry of layered double hydroxides: recent developments and applications1196Intercalation compounds of hydrotalcite-like anionic clays with anti-inflammatory agents, II: Uptake of diclofenac for a controlled release formulation142Controlled Chemical and Drug Delivery via the Internal and External Surfaces of Layered Compounds26Layered double hydroxide as an efficient drug reservoir for folate derivatives435A time resolved, in-situ X-ray diffraction study of the de-intercalation of anions and lithium cations from [LiAl 2 (OH) 6 ] n X·qH 2 O (X = Cl − , Br − , NO 3 − , SO 4 2− )73Cationic and Anionic Clays for Biological Applications16LDH-DNA Nanohybrids: a complete biophysical characterization1Nanobiohybrids as delivery vehicles for camptothecin262Inorganic delivery vector for intravenous injection143Synthesis of layered double hydroxide anionic clays intercalated by carboxylate anions124Layered Double Hydroxides (Ldhs)894-Benzoylbenzoate intercalated in layered double hydroxides: a new catalyst for photo-oxidation of sulfides in solution and in the gas phase17Studies on the intercalation of naproxen into layered double hydroxide and its thermal decomposition by in situ FT-IR and in situ HT-XRD117Novel biomaterials for bisphosphonate delivery155Inorganic layered double hydroxides as a drug delivery system?intercalation and in vitro release of fenbufen239Flow cytometry: Interesting tool for studying binding behavior of DNA on inorganic layered double hydroxide (LDH)24Enteric-coated layered double hydroxides as a controlled release drug delivery system145Synthesis of layered double hydroxides in an emulsion solution40Intercalation, delivery, and expression of the gene encoding green fluorescence protein utilizing nanobiohybrids87Structural and thermal properties of Co–Cu–Fe hydrotalcite-like compounds63Functional biopolymer nanocomposites based on layered solids244Layered solids as a “molecular container” for pharmaceutical agents: l -tyrosine-intercalated layered double hydroxides93Novel layered pesticide slow/controlled release materials -- supramolecular structure and slow release property of glyphosate intercalated layered double hydroxides24Study on the supramolecular structure of sorbic acid inter-calated Zn-Al layered double hydroxides and its thermal decomposition13Synthesis and characteriza-tion of nanoscale magnetic drug-inorganic composites4Synthesis and properties of Mg2Al layered double hydroxides containing 5-fluorouracil121Hydroxy Double Salt Anion Exchange Kinetics: Effects of Precursor Structure and Anion Size51Exfoliation of layered double hydroxide in polystyrene by in-situ atom transfer radical polymerization using initiator-modified precursor62Immobilization of Ibuprofen and Copper-Ibuprofen Drugs on Layered Double Hydroxides106Preparation and Characterization of Hybrid Organic-Inorganic Composite Material: Polymerization of m-Aminobenzoic Acid-Intercalated Into Zn/Al-Layered Double Hydroxides10Phenoxymethylpenicillin–intercalated hydrotalcite as a bacteria inhibitor22Applications of Layered Double Hydroxides430Preparation of Layered Double Hydroxides362A magnetic organic–inorganic composite: Synthesis and characterization of magnetic 5-aminosalicylic acid intercalated layered double hydroxides93Selective anion-exchange intercalation of isomeric benzoate anions into the layered double hydroxide [LiAl2(OH)6]Cl·H2O13Preparation of layered double hydroxides and their applications as additives in polymers, as precursors to magnetic materials and in biology and medicine712Isomer selective ion-exchange intercalation of nitrophenolates into the layered double hydroxide [LiAl 2 (OH) 6 ]Cl·xH 2 O30One-step synthesis and AFM imaging of hydrophobic LDH monolayers118Bio-active molecule immobilisation on layered double hydroxides6Chapter 13.1 Layered Double Hydroxides226Intercalation chemistry of the novel layered double hydroxides [MAl4(OH)12](NO3)2·yH2O (M = Zn, Cu, Ni and Co). 1: New organic intercalates and reaction mechanisms68Systematic studies on the formation of DNA-LDHnanocomplexes and their application as gene carriers0Towards understanding, control and application of layered double hydroxide chemistry582Ultrasound-mediated release of [Ru(bpy) 3 ] 2+ from a layered titanate film—a model for controlled drug release from layered metal oxide films3Hydration, Swelling, Interlayer Structure, and Hydrogen Bonding in Organolayered Double Hydroxides: Insights from Molecular Dynamics Simulation of Citrate-Intercalated Hydrotalcite105Preparation and thermal decomposition studies of l-tyrosine intercalated MgAl, NiAl and ZnAl layered double hydroxides49Experimental Investigations of Amino Acid-Layered Double Hydroxide Complexes: Glutamate−Hydrotalcite57Structure and Energetics of Biocompatible Polymer Nanocomposite Systems: A Molecular Dynamics Study42Intercalation and Photophysical Properties of the Tetra-(8-hydroxyquinolinato) Boron Complex and 3,3‘,4,4‘-Benzophenone Tetracarboxylic Anion into Mg−Al Layered Double Hydroxides39Study on the Photochromism of Ni–Al Layered Double Hydroxides Containing Nitrate Anions75Applications of Layered Double Hydroxides205Biocompatible protoporphyrin IX-containing nanohybrids with potential applications in photodynamic therapy19Synthesis and properties of cordycepin intercalates of Mg–Al–nitrate layered double hydroxides33Preparation and thermal decomposition study of pyridinedicarboxylate intercalated layered double hydroxides11Intercalation of hydrophilic and hydrophobic antibiotics in layered double hydroxides118Layered Rare‐Earth Hydroxides: A Class of Pillared Crystalline Compounds for Intercalation Chemistry227Layered Rare‐Earth Hydroxides: A Class of Pillared Crystalline Compounds for Intercalation Chemistry29Potential perspectives of bio-nanocomposites for food packaging applications1106Preparation and characterization of l-cystine and l-cysteine intercalated layered double hydroxides41Nanohybrids for controlled antibiotic release in topical applications79Clay minerals and layered double hydroxides for novel biological applications623Layered double hydroxides and human health: An overview✠400Anionic clays as hosts for anchored synthesis: Interlayer bromination of maleate and fumarate ions in nickel–zinc layered hydroxy double salt14Synthesis and characterization of Naproxen intercalated Zn–Al layered double hydroxides43Molecular Dynamics Simulation of the Energetics and Structure of Layered Double Hydroxides Intercalated with Carboxylic Acids84Hydrothermal synthesis of microscale boehmite and gamma nanoleaves alumina150Toxicity and Biomedical Imaging of Layered Nanohybrids in the Mouse29A Novel Composite: Layered Double Hydroxides Encapsulated in Vesicles23Heterogeneous ultrathin films fabricated by alternate assembly of exfoliated layered double hydroxides and polyanion111Synthesis of unusual coral-like layered double hydroxide microspheres in a nonaqueous polar solvent/surfactant system72Hantzsch pyridine synthesis using hydrotalcites or hydrotalcite-like materials as solid base catalysts65水溶性铑膦配合物插层水滑石的制备及主、客体组成对其催化性能的影响0Direct Control of Drug Release Behavior from Layered Double Hydroxides through Particle Interactions81Hybrid magnetic materials formed by ferritin intercalated into a layered double hydroxide9Nanoceramics Intercalated with Gd-DTPA for Potential Imaging of Systems In Vivo0Synthesis and characterization of 5-fluorocytosine intercalated Zn–Al layered double hydroxide56Preparation of Rh-TPPTS complex intercalated layered double hydroxide and influences of host and guest compositions on its catalytic performances in hydroformylation reaction10Release studies of different NSAIDs encapsulated in Mg,Al,Fe-hydrotalcites90In Situ Polymerization of the 4-Vinylbenzenesulfonic Anion in Ni−Al−Layered Double Hydroxide and Its Molecular Dynamic Simulation36Intercalation of l -Dopa into Layered Double Hydroxides: Enhancement of Both Chemical and Stereochemical Stabilities of a Drug through Host−Guest Interactions120Poly( L ‐lactide)/layered double hydroxides nanocomposites: Preparation and crystallization behavior45Nanocomposites coated with xyloglucan for drug delivery: In vitro studies54Carboxylate-intercalated layered double hydroxides aged under microwave–hydrothermal treatment39Polymere Nanokomposite mit anorganischen Funktionsfüllstoffen14Synthesis and Crystal Structures of New Lanthanide Hydroxyhalide Anion Exchange Materials, Ln2(OH)5X·1.5H2O (X = Cl, Br; Ln = Y, Dy, Er, Yb)138A novel core-shell structured magnetic organic-inorganic nanohybrid involving drug-intercalated layered double hydroxides coated on a magnesium ferrite core for magnetically controlled drug release152A thermodynamically stable layered double hydroxide heterostructure11Determining materials properties of natural composites using molecular simulation23Layered double hydroxides: A review204Direct Assembly of Anisotropic Layered Double Hydroxide (LDH) Nanocrystals on Spherical Template for Fabrication of Drug-LDH Hollow Nanospheres132pH-Responsive composite based on prednisone-block copolymer micelle intercalated inorganic layered matrix: Structure and in vitro drug release51Poly( L ‐lactic acid) nanocomposites with layered double hydroxides functionalized with ibuprofen56Immobilisation and encapsulation of functional protein–inorganic constructs11Synthesis of crystalline layered double hydroxides: Precipitation by using urea hydrolysis and subsequent hydrothermal reactions in aqueous solutions168Intercalation of Hexacyanoferrate(III) Ions in Layered Double Hydroxides: A Novel Precursor To Form Ferri-/Antiferromagnetic Exchange Coupled Oxides and Monodisperse Nanograin Spinel Ferrites26Inorganic layered double hydroxides as ascorbic acid (vitamin C) delivery system—Intercalation and their controlled release properties100Synthesis and Controlled Release Properties of Prednisone Intercalated Mg−Al Layered Double Hydroxide Composite95Synthesis and structural characterization of L-(-)-malic acid pillared layered double hydroxides3Studies on the oxidation reaction of l-cysteine in a confined matrix of layered double hydroxides23Formation of photo- and thermo-stable layered double hydroxide films with photo-responsive wettability by intercalation of functionalized azobenzenes40Layered double hydroxide nanoparticles in gene and drug delivery284Bioinorganic Magnetic Core−Shell Nanocomposites Carrying Antiarthritic Agents: Intercalation of Ibuprofen and Glucuronic Acid into Mg−Al−Layered Double Hydroxides Supported on Magnesium Ferrite106Montmorillonite-Alginate Nanocomposites as a Drug Delivery System: Intercalation and In Vitro Release of Vitamin B 1 and Vitamin B 695Hexacyanoferrate-intercalated nickel zinc hydroxy double salts21Surface Modification of Exfoliated Layered Gadolinium Hydroxide for the Development of Multimodal Contrast Agents for MRI and Fluorescence Imaging129In-Vitro Release Kinetics and Stability of Anticardiovascular Drugs-Intercalated Layered Double Hydroxide Nanohybrids68Selective Adsorption of Adenosine and Guanosine by a β‐Cyclodextrin/Layered Double Hydroxide Intercalation Compound11Hydroformylation of alkenes using heterogeneous catalyst prepared by intercalation of HRh(CO)(TPPTS)3 complex in hydrotalcite40Recent Developments in the Use of Layered Double Hydroxides as Host Materials for the Storage and Triggered Release of Functional Anions144Influence of the inorganic matrix nature on the sustained release of naproxen56Bionanocomposites based on alginate–zein/layered double hydroxide materials as drug delivery systems266Montmorillonite-alginate composites as a drug delivery system: Intercalation and In vitro release of diclofenac sodium52Preparation of Glycy-l-Tyrosine intercalated layered double hydroxide film and its in vitro release behavior47Controlling the Morphology of Nano-Hybrid Materials6Inclusion and Release of Fenbufen in Mesoporous Silica34Synthesis of Mg–Al–carbonate layered double hydroxide by an atom-economic reaction24Layer-by-Layer Ultrathin Films of Azobenzene-Containing Polymer/Layered Double Hydroxides with Reversible Photoresponsive Behavior88Preparation of an anion dye intercalated into layered double hydroxides and its controllable luminescence properties61Layer-by-layer assembly of porphyrin/layered double hydroxide ultrathin film and its electrocatalytic behavior for H2O254Antioxidant drugs intercalated into layered double hydroxide: Structure and in vitro release108Anthraquinone Sulfonate Modified, Layered Double Hydroxide Nanosheets for Dye‐Sensitized Solar Cells38Layered Double Hydroxides Based Ceramic Nanocapsules as Reservoir and Carrier of Functional Anions12Layer-by-layer assembly of bi-protein/layered double hydroxide ultrathin film and its electrocatalytic behavior for catechol56Biomedical Applications of Layered Double Hydroxides5Effect of Process Variations on Anticancerous Drug Intercalation in Ceramic Based Delivery System9Inorganic-polymer nanohybrid carrier for delivery of a poorly-soluble drug, ursodeoxycholic acid41Solubility and release of fenbufen intercalated in Mg, Al and Mg, Al, Fe layered double hydroxides (LDH): The effect of Eudragit® S 100 covering45Assembly Chemistry of Anion-intercalated Layered Materials29Nearly monodispersed core–shell structural Fe3O4@DFUR–LDH submicro particles for magnetically controlled drug delivery and release137Dissolution of nano-size Mg–Al–Cl hydrotalcite in aqueous media127Fabrication of functional bioinorganic nanoconstructs by polymer–silica wrapping of individual myoglobin molecules7Layer-by-layer assembly of layered double hydroxide/cobalt phthalocyanine ultrathin film and its application for sensors92Biomimetic design and assembly of organic–inorganic composite films with simultaneously enhanced strength and toughness76Enhancement of visible light photocatalysis by grafting ZnO nanoplatelets with exposed (0001) facets onto a hierarchical substrate97Fabrication of pyrenetetrasulfonate/layered double hydroxide ultrathin films and their application in fluorescence chemosensors32In-vitro Characterization of Optimized Multi-Unit Dosage Forms of Theophylline and its Solid State Characterisation3In-vitro Characterization of Optimized Multi-Unit Dosage Forms of Theophylline and its Solid State Characterisation *1 UHUMWANGHO, M U; 2 RAMANA, MURTHY K V0Mesoporous synthetic hectorites: A versatile layered host with drug delivery application45The synthesis of hierarchical Zn–Ti layered double hydroxide for efficient visible-light photocatalysis310Preparation of Oriented Layered Double Hydroxide Film Using Electrophoretic Deposition and Its Application in Water Treatment39Magnetic nanocomposites with drug-intercalated layered double hydroxide shell supported on commercial magnetite and laboratory-made magnesium ferrite core materials26Vesicle formation induced by layered double hydroxides in the catanionic surfactant solution composed of sodium dodecyl sulfate and dodecyltrimethylammonium bromide21Preparation of acrylic acid and AMPS cointercalated layered double hydroxide and its application for superabsorbent25Simple and Mixed Metal Oxides and Hydroxides: Solids with Extended Structures of Different Dimensionalities and Porosities2Effect of Metal Ion Concentration on the Property of Methotraexate/Layered Double Hydroxide Compounds2Layered double hydroxide: Inorganic organic conjugate nanocarrier for methotrexate31Layer-by-layer assembly of electroactive dye/inorganic matrix film and its application as sensor for ascorbic acid17Controlled release of nitrate from hydrotalcite modified formulations52Identification and Quantification of Defects in the Cation Ordering in Mg/Al Layered Double Hydroxides134An optical sensor based on H-acid/layered double hydroxide composite film for the selective detection of mercury ion37

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  2. Intercalation compounds of hydrotalcite-like anionic clays with anti-inflammatory agents, II: Uptake of diclofenac for a controlled release formulation

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  4. Layered double hydroxide as an efficient drug reservoir for folate derivatives

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  12. 4-Benzoylbenzoate intercalated in layered double hydroxides: a new catalyst for photo-oxidation of sulfides in solution and in the gas phase

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  13. Studies on the intercalation of naproxen into layered double hydroxide and its thermal decomposition by in situ FT-IR and in situ HT-XRD

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  14. Novel biomaterials for bisphosphonate delivery

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  16. Flow cytometry: Interesting tool for studying binding behavior of DNA on inorganic layered double hydroxide (LDH)

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  18. Synthesis of layered double hydroxides in an emulsion solution

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  19. Intercalation, delivery, and expression of the gene encoding green fluorescence protein utilizing nanobiohybrids

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  22. Layered solids as a “molecular container” for pharmaceutical agents: l -tyrosine-intercalated layered double hydroxides

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  23. Novel layered pesticide slow/controlled release materials -- supramolecular structure and slow release property of glyphosate intercalated layered double hydroxides

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  36. Preparation of layered double hydroxides and their applications as additives in polymers, as precursors to magnetic materials and in biology and medicine

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  37. Isomer selective ion-exchange intercalation of nitrophenolates into the layered double hydroxide [LiAl 2 (OH) 6 ]Cl·xH 2 O

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  39. Bio-active molecule immobilisation on layered double hydroxides

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  40. Chapter 13.1 Layered Double Hydroxides

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  41. Intercalation chemistry of the novel layered double hydroxides [MAl4(OH)12](NO3)2·yH2O (M = Zn, Cu, Ni and Co). 1: New organic intercalates and reaction mechanisms

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  42. Systematic studies on the formation of DNA-LDHnanocomplexes and their application as gene carriers

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  43. Towards understanding, control and application of layered double hydroxide chemistry

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  44. Ultrasound-mediated release of [Ru(bpy) 3 ] 2+ from a layered titanate film—a model for controlled drug release from layered metal oxide films

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  45. Hydration, Swelling, Interlayer Structure, and Hydrogen Bonding in Organolayered Double Hydroxides: Insights from Molecular Dynamics Simulation of Citrate-Intercalated Hydrotalcite

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  46. Preparation and thermal decomposition studies of l-tyrosine intercalated MgAl, NiAl and ZnAl layered double hydroxides

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  47. Experimental Investigations of Amino Acid-Layered Double Hydroxide Complexes: Glutamate−Hydrotalcite

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  48. Structure and Energetics of Biocompatible Polymer Nanocomposite Systems: A Molecular Dynamics Study

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  49. Intercalation and Photophysical Properties of the Tetra-(8-hydroxyquinolinato) Boron Complex and 3,3‘,4,4‘-Benzophenone Tetracarboxylic Anion into Mg−Al Layered Double Hydroxides

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    Zhongliang Wang, Zhenhui Kang, Enbo Wang, Zhong‐Min Su, Lin Xu

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  50. Study on the Photochromism of Ni–Al Layered Double Hydroxides Containing Nitrate Anions

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