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RESEARCH PAPER · Review of Scientific Instruments · 2012

The Oxford-Diamond In Situ Cell for studying chemical reactions using time-resolved X-ray diffraction

Saul J. Moorhouse, Nenad Vranješ, Andrew C. Jupe, Michael Drakopoulos, Dermot M. O'Hare

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The Oxford-Diamond In Situ Cell for studying chemical reactions using time-resolved X-ray diffractionOriginalA kinetic and mechanistic study into the formation of the Cu–Cr layered double hydroxide14Pulsed supercritical synthesis of anatase TiO2 nanoparticles in a water–isopropanol mixture studied by in situ powder X-ray diffraction43In Situ Measurements on Solid Oxide Fuel Cell Cathodes – Simultaneous X‐Ray Absorption and AC Impedance Spectroscopy on Symmetrical Cells15In Situ Studies of Solvothermal Synthesis of Energy Materials159In situ powder X-ray diffraction study of the hydro-thermal formation of LiMn 2 O 4 nanocrystallites10Synchrotron radiation techniques in materials and environmental science8In situ analysis of electrocrystallization process of metal electrodeposition with confocal energy dispersive X-ray diffraction based on polycapillary X-ray optics9I12: the Joint Engineering, Environment and Processing (JEEP) beamline at Diamond Light Source293Thermal Behavior of Benzoic Acid/Isonicotinamide Binary Cocrystals10Combined In Situ and In Silico Studies of Guest Intercalation into the Layered Double Hydroxide [LiAl2(OH)6]X·yH2O4An in situ study of resin-assisted solvothermal metal-organic framework synthesis8Time-Resolved in Situ Diffraction Reveals a Solid-State Rearrangement During Solvothermal MOF Synthesis28In situ Powder Diffraction for the Study of Hydrogen Storage Materials: A General Introduction0The chemistry of nucleation119Time-resolved in situ powder X-ray diffraction reveals the mechanisms of molten salt synthesis28Unraveling structural and magnetic information during growth of nanocrystalline SrFe 12 O 1936Focal construct geometry for high intensity energy dispersive x-ray diffraction based on x-ray capillary optics10Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction53Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction14Hydroxy double salts loaded with bioactive ions: Synthesis, intercalation mechanisms, and functional performance15In SituStudies of the Crystallization of Metal-Organic Frameworks10Chapter 6 In situ Powder Diffraction for the Study of Hydrogen Storage Materials: A General Introduction0Compact low power infrared tube furnace for in situ X-ray powder diffraction59Structural variety in ytterbium dicarboxylate frameworks and in situ study diffraction of their solvothermal crystallisation14Metal–Organic Nanosheets Formed via Defect-Mediated Transformation of a Hafnium Metal–Organic Framework295High energy X-rays for following metal-organic framework formation: Identifying intermediates in interpenetrated MOF-5 crystallisation26Time-Resolved Powder X-ray Diffraction of the Solvothermal Crystallization of Cobalt Gallate Spinel Photocatalyst Reveals Transient Layered Double Hydroxides20A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions33Formation Mechanisms of Nanocrystalline MnO 2 Polymorphs under Hydrothermal Conditions78Transmission in situ and operando high temperature X-ray powder diffraction in variable gaseous environments44Pitfalls and reproducibility ofin situsynchrotron powder X-ray diffraction studies of solvothermal nanoparticle formation31An in situ thermo-mechanical rig for lattice strain measurement during creep using neutron diffraction4Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity20In Situ Diffraction Studies of Selected Metal–Organic Framework Materials for Guest Capture/Exchange Applications2A prototype handheld X-ray diffraction instrument5Hydrothermal reactor for in-situ synchrotron radiation powder diffraction at SPring-8 BL02B2 for quantitative design for nanoparticle10High-Energy Adventures at Diamond Light Source7In situ scattering studies of material formation during wet-chemical syntheses1Panoramic (in beam) studies of materials synthesis1Molten salts for rechargeable batteries89LiquidReactionCell – a versatile setup for in situ synchrotron studies of compounds in liquid suspension and solution2Molten Salt‐Assisted Synthesis of Catalysts for Energy Conversion66Recently progress in molten salt-assisted synthesis catalysts for photo−/electrocatalytic carbon dioxide reduction9Effect of cyclic loading on the magnetic properties of FeCo-2V alloy1Inhomogeneous strain associated with Lüders band propagation in an FeCo-2V alloy0

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  1. A kinetic and mechanistic study into the formation of the Cu–Cr layered double hydroxide

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  2. Pulsed supercritical synthesis of anatase TiO2 nanoparticles in a water–isopropanol mixture studied by in situ powder X-ray diffraction

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    Jakob Rostgaard Eltzholtz, Christoffer Tyrsted, Kirsten M. Ø. Jensen, Martin Bremholm, Mogens Christensen, Jacob Becker, Bo B. Iversen

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  3. In Situ Measurements on Solid Oxide Fuel Cell Cathodes – Simultaneous X‐Ray Absorption and AC Impedance Spectroscopy on Symmetrical Cells

    Fuel Cells · 2013-11-08

    Russell J. Woolley, Mary P. Ryan, Stephen J. Skinner

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  4. In Situ Studies of Solvothermal Synthesis of Energy Materials

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    Kirsten M. Ø. Jensen, Christoffer Tyrsted, Martin Bremholm, Bo B. Iversen

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  5. In situ powder X-ray diffraction study of the hydro-thermal formation of LiMn 2 O 4 nanocrystallites

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    Steinar Birgisson, Kirsten M. Ø. Jensen, Troels Lindahl Christiansen, Jon Fold von Bülow, Bo B. Iversen

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  6. Synchrotron radiation techniques in materials and environmental science

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  7. In situ analysis of electrocrystallization process of metal electrodeposition with confocal energy dispersive X-ray diffraction based on polycapillary X-ray optics

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    Fangzuo Li, Zhiguo Liu, Tianxi Sun, Chaolin Yang, Weiyuan Sun, Xuepeng Sun, Yongzhong Ma, Xunliang Ding

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  8. I12: the Joint Engineering, Environment and Processing (JEEP) beamline at Diamond Light Source

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    Michael Drakopoulos, Thomas Connolley, Christina Reinhard, Robert Atwood, Oxana V. Magdysyuk, Nghia Trong Vo, Michael Hart, Leigh D. Connor, Bob Humphreys, George Howell, S. Davies, T. P. Hill, G.R. Wilkin, U. Pedersen, Andrew Foster, Nicoletta De Maio, Mark Basham, Fajin Yuan, Kaz Wanelik

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  9. Thermal Behavior of Benzoic Acid/Isonicotinamide Binary Cocrystals

    Crystal Growth & Design · 2015-05-26

    Asma B. M. Buanz, Timothy J. Prior, J. Burley, Bahijja Tolulope Raimi‐Abraham, Richard Telford, Michael Hart, Colin C. Seaton, Philip J. Davies, Ian J. Scowen, Simon Gaisford, Gareth R. Williams

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  10. Combined In Situ and In Silico Studies of Guest Intercalation into the Layered Double Hydroxide [LiAl2(OH)6]X·yH2O

    The Journal of Physical Chemistry C · 2015-07-06

    Abdessamad Y. A. Kaassis, Simin Xu, David G. Evans, Gareth R. Williams, Min Wei, Xue Duan

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  11. An in situ study of resin-assisted solvothermal metal-organic framework synthesis

    Journal of Solid State Chemistry · 2015-07-26

    Saul J. Moorhouse, Yue Wu, Dermot M. O'Hare

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  12. Time-Resolved in Situ Diffraction Reveals a Solid-State Rearrangement During Solvothermal MOF Synthesis

    Chemistry of Materials · 2015-10-13

    Yue Wu, Saul J. Moorhouse, Dermot M. O'Hare

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  13. In situ Powder Diffraction for the Study of Hydrogen Storage Materials: A General Introduction

    Joint Research Centre (European Commission) · 2016-01-01

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  14. The chemistry of nucleation

    CrystEngComm · 2016-01-01

    Espen Drath Bøjesen, Bo B. Iversen

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  15. Time-resolved in situ powder X-ray diffraction reveals the mechanisms of molten salt synthesis

    Chemical Communications · 2016-01-01

    Saul J. Moorhouse, Yue Wu, Hannah C. Buckley, Dermot M. O'Hare

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  16. Unraveling structural and magnetic information during growth of nanocrystalline SrFe 12 O 19

    Journal of Materials Chemistry C · 2016-01-01

    Cecilia Granados‐Miralles, Matilde Saura Muzquiz, Espen Drath Bøjesen, Kirsten M. Ø. Jensen, H.L. Andersen, Mogens Christensen

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  17. Focal construct geometry for high intensity energy dispersive x-ray diffraction based on x-ray capillary optics

    The Journal of Chemical Physics · 2016-03-08

    Fangzuo Li, Zhiguo Liu, Tianxi Sun, Bowen Jiang, Yu Zhu

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  18. Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction

    Angewandte Chemie International Edition · 2016-03-09

    Yue Wu, Matthew I. Breeze, Guy J. Clarkson, Franck Millange, Dermot M. O'Hare, Richard I. Walton

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  19. Exchange of Coordinated Solvent During Crystallization of a Metal–Organic Framework Observed by In Situ High‐Energy X‐ray Diffraction

    Angewandte Chemie · 2016-03-09

    Yue Wu, Matthew I. Breeze, Guy J. Clarkson, Franck Millange, Dermot M. O'Hare, Richard I. Walton

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  20. Hydroxy double salts loaded with bioactive ions: Synthesis, intercalation mechanisms, and functional performance

    Journal of Solid State Chemistry · 2016-03-10

    Abdessamad Y. A. Kaassis, Simin Xu, Shanyue Guan, David G. Evans, Min Wei, Gareth R. Williams

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  21. In SituStudies of the Crystallization of Metal-Organic Frameworks

    Wiley-VCH eBooks · 2016-06-16

    Richard I. Walton, Franck Millange

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  22. Chapter 6 In situ Powder Diffraction for the Study of Hydrogen Storage Materials: A General Introduction

    Pan Stanford Publishing Pte. Ltd. eBooks · 2016-08-08

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  23. Compact low power infrared tube furnace for in situ X-ray powder diffraction

    Review of Scientific Instruments · 2017-01-01

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  24. Structural variety in ytterbium dicarboxylate frameworks and in situ study diffraction of their solvothermal crystallisation

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  25. Metal–Organic Nanosheets Formed via Defect-Mediated Transformation of a Hafnium Metal–Organic Framework

    Journal of the American Chemical Society · 2017-03-27

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  26. High energy X-rays for following metal-organic framework formation: Identifying intermediates in interpenetrated MOF-5 crystallisation

    Microporous and Mesoporous Materials · 2017-04-22

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  27. Time-Resolved Powder X-ray Diffraction of the Solvothermal Crystallization of Cobalt Gallate Spinel Photocatalyst Reveals Transient Layered Double Hydroxides

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  28. A multi-purpose reaction cell for the investigation of reactions under solvothermal conditions

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  29. Formation Mechanisms of Nanocrystalline MnO 2 Polymorphs under Hydrothermal Conditions

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  30. Transmission in situ and operando high temperature X-ray powder diffraction in variable gaseous environments

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  31. Pitfalls and reproducibility ofin situsynchrotron powder X-ray diffraction studies of solvothermal nanoparticle formation

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  32. An in situ thermo-mechanical rig for lattice strain measurement during creep using neutron diffraction

    Review of Scientific Instruments · 2018-05-01

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  33. Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity

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  34. In Situ Diffraction Studies of Selected Metal–Organic Framework Materials for Guest Capture/Exchange Applications

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  35. A prototype handheld X-ray diffraction instrument

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  36. Hydrothermal reactor for in-situ synchrotron radiation powder diffraction at SPring-8 BL02B2 for quantitative design for nanoparticle

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