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RESEARCH PAPER · Inorganic Chemistry · 2004

Syntheses, Structures, and Ion-Exchange Properties of the Three-Dimensional Framework Uranyl Gallium Phosphates, Cs4[(UO2)2(GaOH)2(PO4)4]·H2O and Cs[UO2Ga(PO4)2]

Tatiana Y. Shvareva, Tyler A. Sullens, Thomas C. Shehee, Thomas E. Albrecht‐Schmitt

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Syntheses, Structures, and Ion-Exchange Properties of the Three-Dimensional Framework Uranyl Gallium Phosphates, Cs4[(UO2)2(GaOH)2(PO4)4]·H2O and Cs[UO2Ga(PO4)2]OriginalSyntheses, Structures, and Ion‐Exchange Properties of the Three‐Dimensional Framework Uranyl Gallium Phosphates, Cs4 [(UO2)2(GaOH)2(PO4)4] ×H2O and Cs[UO2Ga(PO4)2].0Polar Open-Framework Structure, Optical Properties, and Electron Paramagnetic Resonance of the Mixed-Metal Uranyl Phosphate Cs2[UO2(VO2)2(PO4)2]·0.59H2O22Aluminium, gallium, indium and thallium10General Route to Three-Dimensional Framework Uranyl Transition Metal Phosphates with Atypical Structural Motifs: The Case Examples of Cs2{(UO2)4[Co(H2O)2]2(HPO4)(PO4)4} and Cs3+x[(UO2)3CuH4-x(PO4)5]·H2O40Product evolution in the Np(IV) fluorophosphate system15New Layered Uranium Phosphate Fluorides: Syntheses, Structures, Characterizations, and Ion-Exchange Properties of A(UO2)F(HPO4)·xH2O (A = Cs+, Rb+, K+; x = 0−1)88Uranium and Uranium Compounds18Cs+-Selective Ion Exchange and Magnetic Ordering in a Three-Dimensional Framework Uranyl Vanadium(IV) Phosphate75Actinide compounds with heavy oxoanions containing a stereochemically active lone-pair of electrons2Rational Construction of Porous Polymeric Cadmium Ferrocene-1,1′-disulfonates for Transition Metal Ion Exchange and Sorption113A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds90A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds11Incorporation of tetrahedral Co(II) into a mixed-metal uranyl phosphate framework: Synthesis and structure of K2[UO2Co(PO4)2]·H2O2Synthesis and structure of [C6H14N2][(UO2)4(HPO4)2(PO4)2(H2O)]·H2O: An expanded open-framework amine-bearing uranyl phosphate12Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications370[H2bipy]2[(UO2)6Zn2(PO3OH)4(PO4)4]·H2O: An Open-Framework Uranyl Zinc Phosphate Templated by Diprotonated 4,4′-Bipyridyl17Mixed tetrahedral anionic framework in the K3Ga2(PO4)3 crystal structure3[Hg5O2(OH)4][(UO2)2(AsO4)2]: A complex mercury(II) uranyl arsenate6Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?18Phosphonoacetate as a Ligand for Constructing Layered and Framework Alkali Metal Uranyl Compounds45Binuclear Uranium(VI) Complexes with a “Pacman” Expanded Porphyrin: Computational Evidence for Highly Unusual Bis‐Actinyl Structures45Comparison of Thorium(IV) and Uranium(VI) Carboxyphosphonates80Binuclear Hexa- and Pentavalent Uranium Complexes with a Polypyrrolic Ligand: A Density Functional Study of Water- and Hydronium-Induced Reactions44Crystal Chemistry of the Potassium and Rubidium Uranyl Borate Families Derived from Boric Acid Fluxes49Synthesis, structural and emission studies of a bis (carbamoyl methyl) sulfone complex of uranyl nitrate11Cs-Exchanged Cuprosklodowskite4From Layered Structures to Cubic Frameworks: Expanding the Structural Diversity of Uranyl Carboxyphosphonates via the Incorporation of Cobalt55Hydrothermal Synthesis and Structural Characterization of Organically Templated Uranyl Diphosphonate Compounds72Uranyl carboxyphosphonates that incorporate Cd(II)20Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates38Layered and Three-Dimensional Framework Cesium and Barium Uranyl Carboxyphenylphosphonates69Pillared and open-framework uranyl diphosphonates32Syntheses of Uranyl Diphosphonate Compounds Using Encapsulated Cations as Structure Directing Agents59Heterobimetallic Copper(II) Uranyl Carboxyphenylphosphonates67Metal-Controlled Assembly of Uranyl Diphosphonates toward the Design of Functional Uranyl Nanotubules77Unprecedented Bidentate Coordination of the Uranyl Cation by the Chromate Anion in the Structure of [(CH3)2CHNH3]2[UO2(CrO4)2]21Steric Effects on Uranyl Complexation: Synthetic, Structural, and Theoretical Studies of Carbamoyl Pyrazole Compounds of the Uranyl(VI) Ion25Barium uranyl diphosphonates16Thorium and uranium diphosphonates: Syntheses, structures, and spectroscopic properties32Synthesis, structure, and spectroscopic characterization of three uranyl phosphates with unique structural units10Layered Uranyl Coordination Polymers Rigidly Pillared by Diphosphonates36From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange82Crystal Chemistry of Uranium Oxides and Minerals27Synthetic, structural, extraction and theoretical studies of uranyl nitrate dithio-diglycolamide compounds11Incorporation of Cu2+ Ions into Nanotubular Uranyl Diphosphonates28Use of 2,2-Bipyrimidine for the Preparation of UO22+-3d Diphosphonates18Uranyl–Organic Hybrids Designed from Hydroxyphosphonate14Steric effects in complexes of diphenyl(2-pyridyl)phosphine oxide with the uranyl ion. Synthetic, structural and theoretical studies10Highly Valence-Diversified Binuclear Uranium Complexes of a Schiff-Base Polypyrrolic Macrocycle: Prediction of Unusual Structures, Electronic Properties, and Formation Reactions19Multifunctional Uranyl Hybrid Materials: Structural Diversities as a Function of pH, Luminescence with Potential Nitrobenzene Sensing, and Photoelectric Behavior as p-type Semiconductors56A Revised and Expanded Structure Hierarchy of Natural and Synthetic Hexavalent Uranium Compounds172Diverse Lanthanide Coordination and Selective Ion Exchange in the Microporous Selenites Na4Ln4(SeO3)7O·nH2O (Ln = Gd, Tb, Dy, Ho, Er, Tm, and Yb)5Exploring Crystal Engineering for Porous Uranyl–Organic Frameworks: Insight into Hydrolysis and In Situ Reaction, Structural Variation‐Dependent Physical Properties6Two uranyl heterocyclic carboxyl compounds with fluorescent properties as high sensitivity and selectivity optical detectors for nitroaromatics13Influence of Pyrazine/Piperazine Based Guest Molecules in the Crystal Structures of Uranyl Thiophene Dicarboxylate Coordination Polymers: Structural Diversities and Photocatalytic Activities for the Degradation of Organic Dye47Electron-Transfer-Enhanced Cation–Cation Interactions in Homo- and Heterobimetallic Actinide Complexes: A Relativistic Density Functional Theory Study7In Situ Reduction from Uranyl Ion into a Tetravalent Uranium Trimer and Hexamer Featuring Ion-Exchange Properties and the Alexandrite Effect16Understanding the Polymorphism of A4[(UO2)3(PO4)2O2] (A = Alkali Metals) Uranyl Phosphate Framework Structures10Accessibility of Uranyl–Plutonium Complex Supported by a Polypyrrolic Macrocycle: An Implication for Experimental Synthesis5Crystal Growth and Structure Characterization of Three Layered Uranyl Phosphates and Their Relation to the Phosphuranylite Family13Targeted crystal growth of uranium gallophosphates via the systematic exploration of the UF 4 –GaPO 4 –ACl (A = Cs, Rb) phase space7Uranyl oxide hydrate frameworks with lanthanide ions25Multifunctional Inorganic‐Organic U‐MOF Materials with Nitrogen Heterocyclic Carboxylate: Synthesis, Structure and Properties11Three-dimensional metal-halide open frameworks56Successive Crystallization of Organically Templated Uranyl Sulfates: Synthesis and Crystal Structures of [pyH](H3O)[(UO2)3(SO4)4(H2O)2], [pyH]2[(UO2)6(SO4)7(H2O)], and [pyH]2[(UO2)2(SO4)3]3Mild hydrothermal synthesis of potassium uranyl phosphates with layered and framework structures2Results of 25-Year Studies of Uranium Compounds at the Department of Crystallography of St. Petersburg State University3Rich Chemical Behavior and Topological Variation in Uranium Phosphates via Flux Growth under an Inert Atmosphere0

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  1. Syntheses, Structures, and Ion‐Exchange Properties of the Three‐Dimensional Framework Uranyl Gallium Phosphates, Cs4 [(UO2)2(GaOH)2(PO4)4] ×H2O and Cs[UO2Ga(PO4)2].

    ChemInform · 2005-03-02

    Tatiana Y. Shvareva, Tyler A. Sullens, Thomas C. Shehee, Thomas E. Albrecht‐Schmitt

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  2. Polar Open-Framework Structure, Optical Properties, and Electron Paramagnetic Resonance of the Mixed-Metal Uranyl Phosphate Cs2[UO2(VO2)2(PO4)2]·0.59H2O

    Chemistry of Materials · 2005-11-12

    Tatiana Y. Shvareva, James V. Beitz, Evert C. Duin, Thomas E. Albrecht‐Schmitt

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  3. Aluminium, gallium, indium and thallium

    Annual Reports Section A (Inorganic Chemistry) · 2006-01-01

    Roman A. Kresiński

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  4. General Route to Three-Dimensional Framework Uranyl Transition Metal Phosphates with Atypical Structural Motifs: The Case Examples of Cs2{(UO2)4[Co(H2O)2]2(HPO4)(PO4)4} and Cs3+x[(UO2)3CuH4-x(PO4)5]·H2O

    Inorganic Chemistry · 2006-02-03

    Tatiana Y. Shvareva, Thomas E. Albrecht‐Schmitt

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  5. Product evolution in the Np(IV) fluorophosphate system

    Journal of Solid State Chemistry · 2006-09-30

    Travis H. Bray, Tyler A. Sullens, Tatiana Y. Shvareva, Richard E. Sykora, Richard Geoffrey Haire, Thomas E. Albrecht‐Schmitt

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  6. New Layered Uranium Phosphate Fluorides: Syntheses, Structures, Characterizations, and Ion-Exchange Properties of A(UO2)F(HPO4)·xH2O (A = Cs+, Rb+, K+; x = 0−1)

    Inorganic Chemistry · 2006-11-15

    Kang Min Ok, Jaewook Baek, P. Shiv Halasyamani, Dermot M. O'Hare

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  7. Uranium and Uranium Compounds

    Kirk-Othmer Encyclopedia of Chemical Technology · 2006-11-17

    David L. Clark, Mary P. Neu, Wolfgang Runde, D. Webster Keogh

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  8. Cs+-Selective Ion Exchange and Magnetic Ordering in a Three-Dimensional Framework Uranyl Vanadium(IV) Phosphate

    Chemistry of Materials · 2006-12-24

    Tatiana Y. Shvareva, S. Skanthakumar, L. Soderholm, Abraham Clearfield, Thomas E. Albrecht‐Schmitt

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  9. Actinide compounds with heavy oxoanions containing a stereochemically active lone-pair of electrons

    Elsevier eBooks · 2007-01-01

    Richard E. Sykora, Tatiana Y. Shvareva, Thomas E. Albrecht‐Schmitt

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  10. Rational Construction of Porous Polymeric Cadmium Ferrocene-1,1′-disulfonates for Transition Metal Ion Exchange and Sorption

    Crystal Growth & Design · 2007-11-15

    Liwei Mi, Hongwei Hou, Zhiyong Song, Huayun Han, Hong Liang Xu, Yaoting Fan, Seik-Weng Ng

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  11. A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds

    Angewandte Chemie International Edition · 2007-12-03

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

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  12. A Crown Ether as Template for Microporous and Nanostructured Uranium Compounds

    Angewandte Chemie · 2007-12-03

    Evgeny V. Alekseev, Sergey V. Krivovichev, Wulf Depmeier

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  13. Incorporation of tetrahedral Co(II) into a mixed-metal uranyl phosphate framework: Synthesis and structure of K2[UO2Co(PO4)2]·H2O

    Solid State Sciences · 2007-12-04

    Yaqin Yu, Thomas E. Albrecht‐Schmitt

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  14. Synthesis and structure of [C6H14N2][(UO2)4(HPO4)2(PO4)2(H2O)]·H2O: An expanded open-framework amine-bearing uranyl phosphate

    Journal of Solid State Chemistry · 2008-05-17

    Travis H. Bray, John D. Gorden, Thomas E. Albrecht‐Schmitt

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  15. Metal Complexes of Organophosphate Esters and Open-Framework Metal Phosphates: Synthesis, Structure, Transformations, and Applications

    Chemical Reviews · 2008-06-28

    Ramaswamy Murugavel, Amitava Choudhury, Mrinalini Ganapati Walawalkar, Ramasamy Pothiraja, C. N. R. Rao

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  16. [H2bipy]2[(UO2)6Zn2(PO3OH)4(PO4)4]·H2O: An Open-Framework Uranyl Zinc Phosphate Templated by Diprotonated 4,4′-Bipyridyl

    Inorganic Chemistry · 2008-08-23

    Yaqin Yu, Wei Zhan, Thomas E. Albrecht‐Schmitt

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  17. Mixed tetrahedral anionic framework in the K3Ga2(PO4)3 crystal structure

    Crystallography Reports · 2008-11-01

    Olga V. Yakubovich, Ian M. Steele, Vadim V. Kireev

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  18. [Hg5O2(OH)4][(UO2)2(AsO4)2]: A complex mercury(II) uranyl arsenate

    Journal of Solid State Chemistry · 2009-04-09

    Yaqin Yu, Kai Jiang, Thomas E. Albrecht‐Schmitt

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  19. Does Iodate Incorporate into Layered Uranyl Phosphates Under Hydrothermal Conditions?

    Inorganic Chemistry · 2009-10-30

    Jie Ling, Shijun Wu, Fanrong Chen, Antonio Simonetti, J. T. Shafer, Thomas E. Albrecht‐Schmitt

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  20. Phosphonoacetate as a Ligand for Constructing Layered and Framework Alkali Metal Uranyl Compounds

    Inorganic Chemistry · 2009-11-02

    A.N. Alsobrook, Thomas E. Albrecht‐Schmitt

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  21. Binuclear Uranium(VI) Complexes with a “Pacman” Expanded Porphyrin: Computational Evidence for Highly Unusual Bis‐Actinyl Structures

    Chemistry - A European Journal · 2010-01-11

    Qing‐Jiang Pan, Grigory A. Shamov, Georg Schreckenbach

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  22. Comparison of Thorium(IV) and Uranium(VI) Carboxyphosphonates

    Inorganic Chemistry · 2010-05-13

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  23. Binuclear Hexa- and Pentavalent Uranium Complexes with a Polypyrrolic Ligand: A Density Functional Study of Water- and Hydronium-Induced Reactions

    Inorganic Chemistry · 2010-06-17

    Qing‐Jiang Pan, Georg Schreckenbach

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  24. Crystal Chemistry of the Potassium and Rubidium Uranyl Borate Families Derived from Boric Acid Fluxes

    Inorganic Chemistry · 2010-06-18

    Shuao Wang, Evgeny V. Alekseev, Jared T. Stritzinger, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  25. Synthesis, structural and emission studies of a bis (carbamoyl methyl) sulfone complex of uranyl nitrate

    Inorganic Chemistry Communications · 2010-10-31

    Shanmugaperumal Kannan, Sadhan Bijoy Deb, M.G.B. Drew

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  26. Cs-Exchanged Cuprosklodowskite

    Springer eBooks · 2011-01-01

    Andrey A. Zolotarev, Sergey V. Krivovichev, М. С. Авдонцева

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  27. From Layered Structures to Cubic Frameworks: Expanding the Structural Diversity of Uranyl Carboxyphosphonates via the Incorporation of Cobalt

    Crystal Growth & Design · 2011-02-08

    A.N. Alsobrook, Brad G. Hauser, Joseph T. Hupp, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  28. Hydrothermal Synthesis and Structural Characterization of Organically Templated Uranyl Diphosphonate Compounds

    Crystal Growth & Design · 2011-03-09

    Pius O. Adelani, Allen G. Oliver, Thomas E. Albrecht‐Schmitt

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  29. Uranyl carboxyphosphonates that incorporate Cd(II)

    Journal of Solid State Chemistry · 2011-04-14

    A.N. Alsobrook, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  30. Incorporation of Mn(II) and Fe(II) into Uranyl Carboxyphosphonates

    Crystal Growth & Design · 2011-04-18

    A.N. Alsobrook, Evgeny V. Alekseev, Wulf Depmeier, Thomas E. Albrecht‐Schmitt

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  31. Layered and Three-Dimensional Framework Cesium and Barium Uranyl Carboxyphenylphosphonates

    Crystal Growth & Design · 2011-05-18

    Pius O. Adelani, Allen G. Oliver, Thomas E. Albrecht‐Schmitt

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  32. Pillared and open-framework uranyl diphosphonates

    Journal of Solid State Chemistry · 2011-07-06

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  33. Syntheses of Uranyl Diphosphonate Compounds Using Encapsulated Cations as Structure Directing Agents

    Crystal Growth & Design · 2011-08-05

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  34. Heterobimetallic Copper(II) Uranyl Carboxyphenylphosphonates

    Crystal Growth & Design · 2011-08-30

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  35. Metal-Controlled Assembly of Uranyl Diphosphonates toward the Design of Functional Uranyl Nanotubules

    Inorganic Chemistry · 2011-11-03

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  36. Unprecedented Bidentate Coordination of the Uranyl Cation by the Chromate Anion in the Structure of [(CH3)2CHNH3]2[UO2(CrO4)2]

    European Journal of Inorganic Chemistry · 2011-12-08

    Oleg I. Siidra, Еvgeny V. Nazarchuk, Sergey V. Krivovichev

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  37. Steric Effects on Uranyl Complexation: Synthetic, Structural, and Theoretical Studies of Carbamoyl Pyrazole Compounds of the Uranyl(VI) Ion

    Inorganic Chemistry · 2012-04-03

    Debasish Das, Shanmugaperumal Kannan, Dilip Kumar Maity, Michael G. B. Drew

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  38. Barium uranyl diphosphonates

    Journal of Solid State Chemistry · 2012-04-06

    Anna‐Gay D. Nelson, Evgeny V. Alekseev, Rodney Charles Ewing, Thomas E. Albrecht‐Schmitt

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  39. Thorium and uranium diphosphonates: Syntheses, structures, and spectroscopic properties

    Journal of Solid State Chemistry · 2012-05-02

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  40. Synthesis, structure, and spectroscopic characterization of three uranyl phosphates with unique structural units

    Journal of Solid State Chemistry · 2012-07-18

    Ernest M. Wylie, Colleen M. Dawes, Peter Carman Burns

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  41. Layered Uranyl Coordination Polymers Rigidly Pillared by Diphosphonates

    Crystal Growth & Design · 2012-10-12

    Pius O. Adelani, Thomas E. Albrecht‐Schmitt

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  42. From 1D Chain to 3D Framework Uranyl Diphosphonates: Syntheses, Crystal Structures, and Selective Ion Exchange

    Inorganic Chemistry · 2012-10-24

    Weiting Yang, Hongyue Wu, Run-Xue Wang, Qing‐Jiang Pan, Zhong‐Ming Sun, Hongjie Zhang

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  43. Crystal Chemistry of Uranium Oxides and Minerals

    Elsevier eBooks · 2013-01-01

    Sergey V. Krivovichev

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  44. Synthetic, structural, extraction and theoretical studies of uranyl nitrate dithio-diglycolamide compounds

    Polyhedron · 2014-03-21

    Bal Govind Vats, S. Kannan, I. C. Pius, D. M. Noronha, Dilip Kumar Maity, Michael G. B. Drew

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  45. Incorporation of Cu2+ Ions into Nanotubular Uranyl Diphosphonates

    Inorganic Chemistry · 2014-04-04

    Pius O. Adelani, Nathaniel D. Cook, Jean‐Marie Babo, Peter Carman Burns

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  46. Use of 2,2-Bipyrimidine for the Preparation of UO22+-3d Diphosphonates

    Crystal Growth & Design · 2014-10-12

    Pius O. Adelani, Nathaniel D. Cook, Peter Carman Burns

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  47. Uranyl–Organic Hybrids Designed from Hydroxyphosphonate

    European Journal of Inorganic Chemistry · 2014-12-09

    Pius O. Adelani, Nicholas A. Martinez, Nathaniel D. Cook, Peter Carman Burns

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  48. Steric effects in complexes of diphenyl(2-pyridyl)phosphine oxide with the uranyl ion. Synthetic, structural and theoretical studies

    Polyhedron · 2015-01-17

    Bal Govind Vats, S. Kannan, K. Parvathi, Dilip Kumar Maity, Michael G. B. Drew

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  49. Highly Valence-Diversified Binuclear Uranium Complexes of a Schiff-Base Polypyrrolic Macrocycle: Prediction of Unusual Structures, Electronic Properties, and Formation Reactions

    Inorganic Chemistry · 2015-05-08

    Jun Ping Yao, Xiu‐Jun Zheng, Qing‐Jiang Pan, Georg Schreckenbach

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  50. Multifunctional Uranyl Hybrid Materials: Structural Diversities as a Function of pH, Luminescence with Potential Nitrobenzene Sensing, and Photoelectric Behavior as p-type Semiconductors

    Inorganic Chemistry · 2015-09-02

    Jian Song, Xue Ping Gao, Zhi‐Nan Wang, Chengren Li, Qi Xu, Feng‐Ying Bai, Zhongfeng Shi, Yong‐Heng Xing

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