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RESEARCH PAPER · Chemical Reviews · 2022

In Situ Kinetic Observations on Crystal Nucleation and Growth

Junjie Li, Francis Leonard Deepak

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In Situ Kinetic Observations on Crystal Nucleation and GrowthOriginalAIB3IIC3IIIQ8VI: A New Family for the Design of Infrared Nonlinear Optical Materials by Coupling Octahedra and Tetrahedra Units152Heteroepitaxy Growth and Characterization of High-Quality AlN Films for Far-Ultraviolet Photodetection6Rb 2 CdSi 4 S 10 : novel [Si 4 S 10 ] T2-supertetrahedra-contained infrared nonlinear optical material with large band gap79Carbon quantum dots with high quantum yield prepared by heterogeneous nucleation processes16Noncentrosymmetric versus Centrosymmetric: Halogen Induced Variable Coordination Modes of Sn2+ and Structural Transition in Sn3B3O7X (X = Cl and Br)17A new infrared nonlinear optical material BaZnGeS 4 with a wide band gap and large nonlinear optical response34Ba 3 (BS 3 )(PS 4 ): the first alkaline-earth metal thioborate–thiophosphate with strong optical anisotropy originating from planar [BS 3 ] units8Cs[B 3 O 3 F 2 (OH) 2 ]: discovery of a hydroxyfluorooxoborate guided by selective organic–inorganic transformation13Discovery of SrZn 2 B 6 O 12 with an unprecedented quadruple-layered configuration0From Cs8Sb4Nb5O5F35 to Cs6Sb4Mo3O5F26: The first noncentrosymmetric fluoroantimonite with d0 transition metal30Hydroxyfluorooxoborate (NH 4 )[C(NH 2 ) 3 ][B 3 O 3 F 4 (OH)] for exploring the effects of cation substitution on structure and optical properties26In situ TEM investigation of nucleation and crystallization of hybrid bismuth nanodiamonds5KRb 2 (NO 3 ) 2 Cl: a new birefringent crystal exhibiting a perovskite-related framework and a short cutoff edge6LiCs 3 AlB 7 O 14 : achieving enhanced optical anisotropy via [AlO 4 ] tetrahedron introduction to rearrange the anionic framework5MB 3 P 2 S 10 (M = Rb, Cs): two new alkali metal thioboratephosphates with [B 6 P 4 S 20 ] T3-supertetrahedra2Multi-scale Crystallization Materials: Advances in in-situ Characterization Techniques and Computational Simulations2Nanoparticle exsolution via electrochemical switching in perovskite fibers for solid oxide fuel cell electrodes34Recent progress on sulfide infrared nonlinear optical materials with large SHG response and wide band gap26Structure Evolution of Porous Alumina During Aging Process and its Support Effect on Ptsn/Al2o3 Catalyzed Propane Dehydrogenation16Synthesis, structure and characterization of Cd 2 TeO 3 Cl 2 with unprecedented [Cd 2 O 6 Cl 4 ] octahedral dimers5Optical Super‐Localisation of Single Nanoparticle Nucleation and Growth in Nanodroplets34Recent advances of inorganic phosphates with UV/DUV cutoff edge and large second harmonic response7In Situ Observations Reveal the Five-fold Twin-Involved Growth of Gold Nanorods by Particle Attachment3Semicrystalline IrOx with Abundant Boundaries for Overall Water Splitting7Direct Imaging of the Kinetic Crystallization Pathway: Simulation and Liquid-Phase Transmission Electron Microscopy Observations11Clamping effect driven design and fabrication of new infrared birefringent materials with large optical anisotropy45Na2BaB12O18F4: A Mixed Alkali/Alkaline-Earth Metal Fluorooxoborate with Two Unprecedented Interpenetrating Three-Dimensional B–O/F Anionic Networks and a Short Ultraviolet Cutoff Edge9The Synergy of the Buried Interface Surface Energy and Temperature for Thermal Evaporated Perovskite Light-Emitting Diodes14Four New Sb‐based Orthophosphates: Cation Regulation to Investigate Diversified Structural Architecture1Na3SiS3F: A Wide Bandgap Fluorothiosilicate with Unique [SiS3F] Unit and High Laser‐Induced Damage Threshold39Design Rules for Obtaining Narrow Luminescence from Semiconductors Made in Solution87Efficient inhibition of mild steel corrosion in acidic medium by novel pyrimidine derivatives: Inhibitive effect evaluation and interface adsorption mechanism31BaMo3O10 Polymorphs with Tunable Symmetries and Properties3Crystallization inhibitory effects of konjac glucomannan, sodium alginate and xanthan gum on curcumin in supersaturated solution12Recent Advances in Magnetite Crystallization: Pathway, Modulation, and Characterization17Zn 2 HgP 2 S 8 : A Wide Bandgap Hg‐Based Infrared Nonlinear Optical Material with Large Second‐Harmonic Generation Response75Gas-phase materials synthesis in environmental transmission electron microscopy5Realization of flexible in-memory computing in a van der Waals ferroelectric heterostructure tri-gate transistor34Structural Self-Destruction of Deep Eutectic Solvents Induced the Formation of Unusual Diamond-Shaped Crystals of Honokiol and Its Mechanistic Study5Enhanced electrical and mechanical properties of Bi2Te3-based thermoelectric thick films enabled by a practical dynamic regulation strategy10MXenes are materials, not chemicals: Synthesis factors that influence MXene properties27Nucleation and Growth of Nanocrystals Investigated by In Situ Transmission Electron Microscopy42Observing the Evolution of Metal Oxides in Liquids6Heterologous Isomorphic Substitution Induces Optical Property Enhancement for Deep-UV Crystals: a Case in Rb[B3O3F2(OH)2]10Mixed Anionic Tetrahedra Guided Design of New Infrared Nonlinear Optical Material Cs 3 Ga 8 S 13 Cl with High Laser‐Induced Damage Threshold26The Strain Effects and Interfacial Defects of Large ZnSe/ZnS Core/Shell Nanocrystals20Double alkaline earth metals sulfide SrMgGeS4 with high laser-induced damage threshold and strong second-harmonic generation29Theoretical investigations on ternary defective diamond-like infrared nonlinear optical materials in Be-Ga-Se system18Ion Irradiation‐Induced Sinking of Ag Nanocubes into Substrates1Breaking the Inherent Interarrangement of [B3O6] Clusters for Nonlinear Optics with Orbital Hybridization Enhancement142Mineral scaling induced membrane wetting in membrane distillation for water treatment: Fundamental mechanism and mitigation strategies90Atomic imaging reveals in-situ growth behavior of bi nanoparticles by high-energy electron irradiation2Parallel Nanosheet Arrays for Industrial Oxygen Production130Kinetically Controlled Nucleation Enabled by Tunable Microfluidic Mixing for the Synthesis of Dendritic Au@Pt Core/Shell Nanomaterials16A I B 3 II C 2 III Q 6 VI X VII : A Thioborate Halide Family for Developing Wide Bandgap Infrared Nonlinear Materials by Coupling Planar [BS 3 ] and Polycations25Fluorination Strategy Towards Symmetry Breaking of Boron‐centered Tetrahedron for Poly‐fluorinated Optical Crystals15Fluorination Strategy Towards Symmetry Breaking of Boron‐centered Tetrahedron for Poly‐fluorinated Optical Crystals70In situ observation of a stepwise [2 + 2] photocycloaddition process using fluorescence spectroscopy31Nanocomposite Hydrogel‐Based Optical Fiber Probe for Continuous Glucose Sensing16In-situ study of hybrid nanomaterial formation : a multiscale approach combining electron microscopy and spectroscopic techniques0Asymmetric Sandwich Janus Structure for High‐Performance Textile‐Based Thermo–Hydroelectric Generators Toward Human Health Monitoring17Fluorination strategy toward chemical and functional modification65Scalable In‐Plane Directional Crystallization for The Printable Hole‐Conductor‐Free Perovskite Solar Cell Based on The Carbon Electrode30Comparing brute force to transition path sampling for gas hydrate nucleation with a flat interface: comments on time reversal symmetry0“Three‐in‐One”: A New Hg‐Based Selenide Hg 7 P 2 Se 12 Exhibiting Wide Infrared Transparency Range and Strong Nonlinear Optical Effect80Ca1-Xsrxmno3-Δ Granules, Pellets, Foams: Influence of Fabrication Conditions and Microstructure on Oxidation Kinetics0Chemical modulation of A I RE III C IV QVI4 family compounds for band gap and optical anisotropy enhancement16Discovery of a new bimetallic borate with strong optical anisotropy activated by π-conjugated [B 2 O 5 ] units3Exposing the (002) active facet by reducing surface energy for a high-performance Na 3 V 2 (PO 4 ) 2 F 3 cathode23Intramolecular CH⋯π attraction mediated conformational polymorphism of constrained helical peptides11Pb 3.5 GeS 4 Br 3 : the first phase-matching thiogermanate halide infrared nonlinear optical material12Pb 6 Ba 3 Si 2 S 8 I 10 : a new thiohalide with a quasi-two-dimensional structure and wide band gap2Review of in Situ TEM Study on Evolution Mechanism of Semiconductor Materials in Gas Environment0Shearing-induced formation of Au nanowires2Theoretical prediction on the stability, elastic, electronic and optical properties of MAB-phase M 4 AlB 4 compounds (M = Cr, Mo, W)7Transient intermediate in the formation of an amorphous metal–organic framework13Understanding the nanoscale phenomena of nucleation and crystal growth in electrodeposition87Wide band gap selenide infrared nonlinear optical materials A II Mg 6 Ga 6 Se 16 with strong SHG responses and high laser-induced damage thresholds31β -CsHg 2 I 5 , a compound with rare [Hg 2 I 5 ] dimers and large optical anisotropy2Design of Deep-Ultraviolet Zero-Order Waveplate Materials by Rational Assembly of [AlO2F4] and [SO4] Groups9Insight into the Role of Hydroxypropyl Cellulose in Tuning Crystallization Behaviors of dl -Methionine8Platinum–Ruthenium Dual‐Atomic Sites Dispersed in Nanoporous Ni 0.85 Se Enabling Ampere‐Level Current Density Hydrogen Production31Polysulfide Anions [S x ] 2− ( x = 2, 3, 4, 5): Promising Functional Building Units for Infrared Nonlinear Optical Materials22A toolbox for investigating liquid metal systems15A novel reinforced concrete-like composite solid-state electrolyte with enhanced performance for all-solid-state lithium batteries5Agglomeration inhibition engineering of nickel–cobalt alloys by a sacrificial template for efficient urea electrolysis34Understanding the bio-crystallization: An insight to therapeutic relevance2Microelectrode‐enabled Electrocrystallization of Cobalt TCNQ Complex for Gas Sensing7Enhanced electrochemical performance of MoSe2 nanosheets on CoAl- layered double hydroxide for oxygen evolution reaction13Weakening the silicate network through six-coordinated magnesium to achieve a high degree of crystallization of β-CaSiO3 in calcium borosilicate glass ceramics for 5G application8Catalytic Activity and Electrochemical Stability of Ru1–xMxO2 (M = Zr, Nb, Ta): Computational and Experimental Study of the Oxygen Evolution Reaction18Direct Synthesis of CuPd Icosahedra Supercrystals Studied by In Situ X‐Ray Scattering7Crystal nucleation in an AlNiZr metallic liquid: Within and beyond classical nucleation theory13Homogeneous Organic Crystal Nucleation Rates in Solution from the Perspective of Chemical Reaction Kinetics10Regioselective super-assembly of Prussian blue analogue11Time-Dependent Effect of Additives on Crystallization of Amorphous Calcium Phosphate: Faster Nucleation after Dilution6A DSC study of undercooling thermodynamics and crystallization kinetics for liquid Ag-Si alloys2Seeding Atomic Silver into Internal Lattice Sites of Transition Metal Oxide for Advanced Electrocatalysis20A microscopic view on the electrochemical deposition and dissolution of Au with scanning electrochemical cell microscopy – Part II: Potentiostatic dissolution and correlation with in-situ EC-TEM15Tunable Optical Anisotropy in Rare‐Earth Borates with Flexible [BO3] Clusters7Formation and growth of nanophase iron particles on the surface of Mercury revealed by experimental study6The synergy of pre-frozen substrates and post-annealing for high-efficiency co-evaporated blue perovskite LEDs13Acceleration of radiative recombination for efficient perovskite LEDs394Directed self-assembly of mesoporous starch-based microparticle: Characterization, antimicrobial activities, and digestibility9Interrogation of 3d Transition Bimetallic Nanocrystal Nucleation and Growth Using In Situ Electron Microscope and Synchrotron X-ray Techniques7Improving spectral linewidth performance of InP quantum dots by promoting size-focused growth and decreasing exciton-phonon coupling7Prussian Blue Analogue Glasses for Photoinduced CO2 Conversion20Regioselective epitaxial growth of metallic heterostructures54Coexisting hematite induces and accelerates the transformation of ferrihydrite: Pathway and underlying mechanisms2Synergy in use of mixed nickel cobalt oxide over a novel interfacial carbon film on current collector for electrochemical energy storage1Tailored Design of Mesoporous Nanospheres with High Entropic Alloy Sites for Efficient Redox Electrocatalysis44A uniform understanding of polymer crystallization models: Diffusion and conformational transition model10Temperature Dependent Growth Kinetics of Pd Nanocrystals: Insights from Liquid Cell Transmission Electron Microscopy9Unveiling the Factors Influencing Different Nucleation Pathways and Liquid–Liquid Phase Separation1Epitaxial Growth of Two-Dimensional Organic Crystals with In-Plane Heterostructured Domain Regulation23Netting Crystal Nuclei in Metal–Organic Framework Cavities2Solvent Dependence of Ionic Liquid-Based Pt Nanoparticle Synthesis: Machine Learning-Aided In-Line Monitoring in a Flow Reactor11Dynamic Metal Exchange in Nanoclusters: Isotope Labeling Sheds Light on Cellular‐like Fusion Processes0Unveiling the Dynamic Pathways of Metal–Organic Framework Crystallization and Nanoparticle Incorporation for Li–S Batteries21Multiscale Crystallization of Inorganic Materials1Interrogating the Solid–Solid Phase Transition Behavior of a Molecular Crystal with a Diverse Range of Solid-State Analytical Techniques and Computational Predictions1Morphology Regulation of Organophosphate Crystals by Micro‐Jetting Technique0Heterogeneous nucleation and growth of manganese (oxyhydr)oxides on mineral surfaces and their geochemical significances0Real-time observation of crystals growth under optical microscopy: A self-assembly process of organic-inorganic intercalation composites driven by electrostatic interaction1Recent Progress on Crystal Nucleation of Amorphous Solid Dispersion6Enhanced synergistic catalysis of bisphenol A in river water using an anti-aging photocatalytic membrane3Preparation of Near-Spherical α-Al2O3 Particles by Enhanced Precipitation of Gibbsite from Sodium Aluminate Solution Using Highly Dispersed Al2O3 as Seeds2Micro/nano plastics inhibit the formation of barium sulfate scale on metal surface7In situ formulation of biomaterials for disease therapy: Recent advances in peptide assembly strategies12Rapid Microwave Annealing for Improved Crystallinity and Morphology of Perovskite Materials7Molecular recognition characteristics of co-assembled peptides on atomically flat graphite surfaces3A review on synthesis, capping and applications of superparamagnetic magnetic nanoparticles40Entropy Engineering of 2D Materials31Growth Mechanism of Hexagonal Zinc Nanocrystals via Liquid Cell Transmission Electron Microscopic2Growing a single suspended perfect protein crystal in a fully noncontact manner4A bifunctional nanocomplex with remineralizing and antibacterial activities to interrupt dental caries17Controlled Growth of 2D‐3D Perovskite Lateral Heterostructures for Wavelength‐Tunable Light Communication25Impact of Cathodic Scaling on Electrocatalytic Degradation of Organic Pollutants2Surface Self-Diffusion Induced Sintering of Nanoparticles39Atomic Force Microscopy and its Applications in Secondary Batteries0In-situ characterization techniques for investigations of heterogeneous catalysis11Role of Na2CO3 as Nucleation Seeds to Accelerate the CO2 Uptake Kinetics of MgO-Based Sorbents17Industrial-level production of ultrastable selenium nanoparticles using a confined coordination synthetic strategy12MgPO2F3: An Ultraviolet Nonlinear Optical System with an Extremely Short Phase-Matching Wavelength Achieved by Introducing Dual-Type Fluorine via Structure Prediction1Advancing cryogenic carbon capture technology through understanding the CO2 frosting crystallization mechanism19Boosting low-temperature CO2 methanation activity through Tailored electronic structures and step-edge defects in Niε−-Ov-Ceδ+ inverse interfaces16Computer‐Aided Development of New Nonlinear Optical Materials38Computer‐Aided Development of New Nonlinear Optical Materials14Effects of natural inhibitors-modified superhydrophobic coatings on BaSO4 scaling and the associated surface interaction mechanisms4Morphological approach to understanding mineral alteration and nanoparticle formation under alkaline conditions using granitic rock thin sections0

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