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RESEARCH PAPER · Inorganic Chemistry · 2015

High-Temperature Salt Flux Crystal Growth of New Lanthanide Molybdenum Oxides, Ln5Mo2O12 Ln = Eu, Tb, Dy, Ho, and Er: Magnetic Coupling within Mixed Valent Mo(IV/V) Rutile-Like Chains

Anthony J. Cortese, Dileka Abeysinghe, Branford O. Wilkins, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

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High-Temperature Salt Flux Crystal Growth of New Lanthanide Molybdenum Oxides, Ln5Mo2O12 Ln = Eu, Tb, Dy, Ho, and Er: Magnetic Coupling within Mixed Valent Mo(IV/V) Rutile-Like ChainsOriginalChemInform Abstract: High‐Temperature Salt Flux Crystal Growth of new Lanthanide Molybdenum Oxides, Ln5Mo2O12 Ln: Eu, Tb, Dy, Ho, and Er: Magnetic Coupling within Mixed Valent Mo(IV/V) Rutile‐Like Chains.0New Lanthanide Mixed-Valent Vanadium(III/IV) Oxosilicates, Ln4V5–xZnxSi4O22 (Ln = La, Ce, Pr, and Nd), Crystallizing in a Quasi Two-Dimensional Rutile-Based Structure15Single crystal growth and characterization of NaxLn1−xMoO4, Ln=La, Ce, Pr, Nd, Sm, and Eu (x=0.397–0.499)9Counter anion and pH directed assembly of europium(III) compounds based on tetrazole containing carboxylic acids11Isomer dependent assembly of Ce(III) and Gd(III) coordination polymers containing 5-(n-pyridyl)tetrazole-2-acetato (n = 3,4)15Oxygen Anion Solubility as a Factor in Molten Flux Crystal Growth, Synthesis, and Characterization of Four New Reduced Lanthanide Molybdenum Oxides: Ce4.918(3)Mo3O16, Pr4.880(3)Mo3O16, Nd4.910(3)Mo3O16, and Sm4.952(3)Mo3O1615A fresnoite-structure-related mixed valent titanium(III/IV) chlorosilicate, Ba3Ti2Si4O14Cl: A flux crystal growth route to Ti(III) containing oxides11Thermal Expansion Behavior in TcO2. Toward Breaking the Tc–Tc Bond8Observation of Vacancies, Faults, and Superstructures in Ln5Mo2O12 (Ln = La, Y, and Lu) Compounds with Direct Mo–Mo Bonding5Growth of {100}-faceted NaFeTiO 4 crystals with a tunable aspect ratio from a NaCl–Na 2 SO 4 binary flux7RE (SO 4 )[B(OH) 4 ](H 2 O), RE (SO 4 )[B(OH) 4 ](H 2 O) 2 , and RE (SO 4 )[B(OH) 4 ](H 2 O)·H 2 O: Rare-Earth Borate-Sulfates Featuring Three Types of Layered Structures19High temperature hydrothermal synthesis of rare-earth titanates: synthesis and structure of RE 5 Ti 4 O 15 (OH) (RE = La, Er), Sm 3 TiO 5 (OH) 3 , RE 5 Ti 2 O 11 (OH) (RE = Tm–Lu) and Ce 2 Ti 4 O 116In Situ Neutron Diffraction Studies of the Flux Crystal Growth of the Reduced Molybdates La 4 Mo 2 O 11 and Ce 4 Mo 2 O 11 : Revealing Unexpected Mixed-Valent Transient Intermediates and Determining the Sequence of Events during Crystal Growth19Facile in-situ reduction: Crystal growth and magnetic studies of reduced vanadium (III/IV) silicates CaxLn1−xVSiO5 (Ln = Ce–Nd, Sm–Lu, Y)2Fabrication of Fluorapatite Nanocrystal-Activated Carbon Composite by the Atmospheric Pressure Plasma-Assisted Flux Method7Electronic correlations and competing orders in multiorbital dimers: A cluster DMFT study10Molten Alkali Halide Flux Growth of an Extensive Family of Noncentrosymmetric Rare Earth Sulfides: Structure and Magnetic and Optical (SHG) Properties47One-Dimensional Quaternary and Penternary Alkali Rare Earth Thiophosphates Obtained via Alkali Halide Flux Crystal Growth12Stacking Faults and Short‐Range Magnetic Correlations in Single Crystal Y5Ru2O12: A Structure with Ru+4.5 One‐Dimensional Chains8Hydrothermal synthesis of lanthanide ruthenate single crystals11Peculiar crystal structure and long-range order of spin-1/2 ladders in MoOBr36Discovery at the Interface between Known Structure Types: The Layered Y10Ni x Cu1– x Ti4O24 Family0

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  1. ChemInform Abstract: High‐Temperature Salt Flux Crystal Growth of new Lanthanide Molybdenum Oxides, Ln5Mo2O12 Ln: Eu, Tb, Dy, Ho, and Er: Magnetic Coupling within Mixed Valent Mo(IV/V) Rutile‐Like Chains.

    ChemInform · 2016-02-01

    Anthony J. Cortese, Dileka Abeysinghe, Branford O. Wilkins, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  2. New Lanthanide Mixed-Valent Vanadium(III/IV) Oxosilicates, Ln4V5–xZnxSi4O22 (Ln = La, Ce, Pr, and Nd), Crystallizing in a Quasi Two-Dimensional Rutile-Based Structure

    Inorganic Chemistry · 2016-02-02

    Dileka Abeysinghe, Mark D. Smith, Jeongho Yeon, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  3. Single crystal growth and characterization of NaxLn1−xMoO4, Ln=La, Ce, Pr, Nd, Sm, and Eu (x=0.397–0.499)

    Journal of Solid State Chemistry · 2016-05-09

    Anthony J. Cortese, Dileka Abeysinghe, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  4. Counter anion and pH directed assembly of europium(III) compounds based on tetrazole containing carboxylic acids

    Inorganica Chimica Acta · 2016-05-26

    Li-Li Miao, Meng‐Yue Guo, Jiao Wu, Yi-Ming Lu, Qi Wu, Yu Bai, Qiaoyun Li, Gao‐Wen Yang

    Read original paper ↗ ·

  5. Isomer dependent assembly of Ce(III) and Gd(III) coordination polymers containing 5-(n-pyridyl)tetrazole-2-acetato (n = 3,4)

    Inorganica Chimica Acta · 2016-06-23

    Yi-Ming Lu, Jue Wang, Jiao Wu, Kai-Kai Ding, Yue-Kang Li, Li-Li Miao, Qiaoyun Li, Gao‐Wen Yang

    Read original paper ↗ ·

  6. Oxygen Anion Solubility as a Factor in Molten Flux Crystal Growth, Synthesis, and Characterization of Four New Reduced Lanthanide Molybdenum Oxides: Ce4.918(3)Mo3O16, Pr4.880(3)Mo3O16, Nd4.910(3)Mo3O16, and Sm4.952(3)Mo3O16

    Crystal Growth & Design · 2016-07-06

    Anthony J. Cortese, Dileka Abeysinghe, Branford O. Wilkins, Mark D. Smith, Vitaly A. Rassolov, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  7. A fresnoite-structure-related mixed valent titanium(III/IV) chlorosilicate, Ba3Ti2Si4O14Cl: A flux crystal growth route to Ti(III) containing oxides

    Journal of Solid State Chemistry · 2017-03-31

    Dileka Abeysinghe, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  8. Thermal Expansion Behavior in TcO2. Toward Breaking the Tc–Tc Bond

    Inorganic Chemistry · 2017-07-24

    Emily Reynolds, Zhaoming Zhang, Maxim Avdeev, Gordon James Thorogood, Frédéric Poineau, Kenneth R. Czerwinski, Justin A. Kimpton, Brendan J. Kennedy

    Read original paper ↗ ·

  9. Observation of Vacancies, Faults, and Superstructures in Ln5Mo2O12 (Ln = La, Y, and Lu) Compounds with Direct Mo–Mo Bonding

    Inorganic Chemistry · 2017-10-26

    Diane M. Colabello, Elizabeth Sobalvarro Converse, John P. Sheckelton, Jöerg C. Neuefeind, Tyrel M. McQueen, Peter G. Khalifah

    Read original paper ↗ ·

  10. Growth of {100}-faceted NaFeTiO 4 crystals with a tunable aspect ratio from a NaCl–Na 2 SO 4 binary flux

    CrystEngComm · 2017-12-01

    Tomohito Sudare, Daiki Kawaura, Kunio Yubuta, Fumitaka Hayashi, Katsuya Teshima

    Read original paper ↗ ·

  11. RE (SO 4 )[B(OH) 4 ](H 2 O), RE (SO 4 )[B(OH) 4 ](H 2 O) 2 , and RE (SO 4 )[B(OH) 4 ](H 2 O)·H 2 O: Rare-Earth Borate-Sulfates Featuring Three Types of Layered Structures

    Inorganic Chemistry · 2017-12-14

    Wenwen Wang, Xiang Xu, Jin-Tao Kong, Jiang‐Gao Mao

    Read original paper ↗ ·

  12. High temperature hydrothermal synthesis of rare-earth titanates: synthesis and structure of RE 5 Ti 4 O 15 (OH) (RE = La, Er), Sm 3 TiO 5 (OH) 3 , RE 5 Ti 2 O 11 (OH) (RE = Tm–Lu) and Ce 2 Ti 4 O 11

    Dalton Transactions · 2018-01-01

    Kyle Fulle, Liurukara Duminda Sanjeewa, Colin D. McMillen, Joseph W. Kolis

    Read original paper ↗ ·

  13. In Situ Neutron Diffraction Studies of the Flux Crystal Growth of the Reduced Molybdates La 4 Mo 2 O 11 and Ce 4 Mo 2 O 11 : Revealing Unexpected Mixed-Valent Transient Intermediates and Determining the Sequence of Events during Crystal Growth

    Chemistry of Materials · 2018-01-10

    Dileka Abeysinghe, Ashfia Huq, Jeongho Yeon, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  14. Facile in-situ reduction: Crystal growth and magnetic studies of reduced vanadium (III/IV) silicates CaxLn1−xVSiO5 (Ln = Ce–Nd, Sm–Lu, Y)

    Journal of Solid State Chemistry · 2018-02-04

    Dileka Abeysinghe, Mark D. Smith, Gregory W. Morrison, Jeongho Yeon, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  15. Fabrication of Fluorapatite Nanocrystal-Activated Carbon Composite by the Atmospheric Pressure Plasma-Assisted Flux Method

    Crystal Growth & Design · 2018-08-15

    Tomohito Sudare, Chikara Mori, Fumitaka Hayashi, Katsuya Teshima

    Read original paper ↗ ·

  16. Electronic correlations and competing orders in multiorbital dimers: A cluster DMFT study

    Physical review. B./Physical review. B · 2019-01-08

    Malte Harland, A. I. Poteryaev, Sergey V Streltsov, Alexander I. Lichtenstein

    Read original paper ↗ ·

  17. Molten Alkali Halide Flux Growth of an Extensive Family of Noncentrosymmetric Rare Earth Sulfides: Structure and Magnetic and Optical (SHG) Properties

    Inorganic Chemistry · 2019-06-19

    Mohammad Usman, Mark D. Smith, Gregory W. Morrison, Vladislav V. Klepov, Weiguo Zhang, P. Shiv Halasyamani, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  18. One-Dimensional Quaternary and Penternary Alkali Rare Earth Thiophosphates Obtained via Alkali Halide Flux Crystal Growth

    Crystal Growth & Design · 2019-08-21

    Mohammad Usman, Mark D. Smith, Vladislav V. Klepov, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  19. Stacking Faults and Short‐Range Magnetic Correlations in Single Crystal Y5Ru2O12: A Structure with Ru+4.5 One‐Dimensional Chains

    physica status solidi (b) · 2020-09-03

    Liurukara Duminda Sanjeewa, Yaohua Liu, Jie Xing, R. S. Fishman, Mudithangani T.K. Kolambage, Michael A. McGuire, Colin D. McMillen, Joseph W. Kolis, Athena S. Sefat

    Read original paper ↗ ·

  20. Hydrothermal synthesis of lanthanide ruthenate single crystals

    Journal of Crystal Growth · 2022-11-11

    Bhakti K. Patel, Mudithangani T.K. Kolambage, Colin D. McMillen, Joseph W. Kolis

    Read original paper ↗ ·

  21. Peculiar crystal structure and long-range order of spin-1/2 ladders in MoOBr3

    Journal of Alloys and Compounds · 2023-09-07

    Anna A. Vorobyova, Evgenia V. Komleva, Michael Y. Geidorf, A.Y. Zaikina, Tatyana M. Vasilchikova, Konstantin V. Zakharov, A. I. Shilov, Sergey V. Simonov, E. A. Ovchenkov, Igor V. Morozov, Larisa Victorovna Shvanskaya, Sergey V Streltsov, Alexander N. Vasiliev, О. С. Волкова

    Read original paper ↗ ·

  22. Discovery at the Interface between Known Structure Types: The Layered Y10Ni x Cu1– x Ti4O24 Family

    Inorganic Chemistry · 2026-07-12

    Nataliya L. Gulay, Hai Lin, Batoul Almoussawi, Cara J. Hawkins, Manel Sonni, Marco Zanella, Troy D. Manning, Luke M. Daniels, Matthew Stephen Dyer, John B. Claridge, Matthew J. Rosseinsky

    Read original paper ↗ ·
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