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RESEARCH PAPER · Accounts of Chemical Research · 2000

Aufbau Principle of Complex Open-Framework Structures of Metal Phosphates with Different Dimensionalities

C. N. R. Rao, Srinivasan Natarajan, Amitava Choudhury, S. Neeraj, Ayi A. Ayi

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Aufbau Principle of Complex Open-Framework Structures of Metal Phosphates with Different DimensionalitiesOriginalAmbient temperature crystallisation of a lamellar gallium fluorophosphate from the synthesis solution of microporous ULM-518Direct in situ observation of increasing structural dimensionality during the hydrothermal formation of open-framework zinc phosphates53Synthesis of a hierarchy of zinc oxalate structures from amine oxalates81Transformations of low-dimensional zinc phosphates to complex open-framework structures. Part 1: zero-dimensional to one-, two- and three-dimensional structures111Transformations of the low-dimensional zinc phosphates to complex open-framework structures. Part 2: one-dimensional ladder to two- and three-dimensional structures103Basic building units, self-assembly and crystallization in the formation of complex inorganic open architectures13Hydrothermal synthesis and structural characterization of a new layered zincophosphate co-templated by diprotonated 1,6-diaminohexane and orthoboric acid moleculesElectronic supplementary information (ESI) available: powder XRD data for I. See http://www.rsc.org/suppdata/jm/b1/b105057p/21Synthesis, Crystal Structure, and Solid State NMR Spectroscopy of (C10N4H28)[Zn6(HPO4)2(PO4)4]·2H2O, a New Zinc Phosphate with a Layer Structure14An approach to the synthesis of organically templated open-framework metal sulfates by the amine–sulfate route94A sponge-like luminescent coordination framework via an Aufbau approach63Two new diamine templated lanthanum sulfates, La 2 (H 2 O) 2 (C 4 H 12 N 2 )(SO 4 ) 4 and La 2 (H 2 O) 2 (C 2 H 10 N 2 ) 3 (SO 4 ) 6 ·4H 2 O, with 3D and 2D crystal structures113A Coordination Polymer of Cobalt(II)−Glutarate: Two-Dimensional Interlocking Structure by Dicarboxylate Ligands with Two Different Conformations163[Zn3(HPO4)4](NMe4)2: a zincophosphate containing interruptions of isolated hydrogen-bonding [H–O(P)]4 groupings within a novel three-dimensional four-connected framework38Synthesis and Structure of a Novel Layered Zincophosphate Zn4P3O11(OH)·3C3N2H4 with Organic Amine Acting as Ligand19Perovskites by Design: A Toolbox of Solid-State Reactions736Reversible Gas−Solid Reactions between the Organometallic Zwitterion [(η5-C5H4COOH)(η5-C5H4COO)CoIII] and Vapors of Trifluoroacetic and Tetrafluoroboric Acids41Transformations of two-dimensional layered zinc phosphates to three-dimensional and one-dimensional structures43Synthesis of a layered zinc phosphate, [NH3(CH2)2NH2(CH2)3NH3][Zn2(PO4)(HPO4)2]·H2O, and its transformation to a extra-large pore three-dimensional zinc phosphate, [NH3(CH2)2NH2(CH2)3NH3][Zn3(PO4)(HPO4)3]26Synthesis and Structure of an Open-Framework Zincophosphate [C6N4H22][ZnPO4]412A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates50A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates6Synthesis and structure of a layered zinc phosphate–acetate, [C5H10NH2]2[Zn(ZnO2CCH3)(PO4)(HPO4)]8Hydrothermal Synthesis and Structure of a Neutral Open-Framework Zincophosphate6Synthesis of Open-Framework Iron Phosphates, [C6N2H14][FeIII2F2(HPO4)2(H2PO4)2]·2H2O and [C6N2H14]2[FeIII3(OH)F3(PO4)(HPO4)2]2·H2O, with One- and Three-Dimensional Structures33Manganese Metallamacrocycles with Various Coordination Solvents15Synthesis and Structure of a New Layered Zincophosphate Zn6(PO4)5(HPO4)·C8N5H28·5H2O, Intercalated with Quintuply Protonated Tetraethylenepentamine12Synthesis and structure of an open-framework cobalt zincophosphate17Recent results from the in situ study of hydrothermal crystallisations using time-resolved X-ray and neutron diffraction methods33Hydrothermal synthesis, structure and magnetism of square-grid cobalt(ii)-carboxylate layered compounds with and without pillars45The hydrogen oxalate anion allows one-dimensional columnar aggregation of organometallic sandwich cations19Open-Framework Rubidium Halides Incorporated in Cadmium Oxalate Host Lattices15Open-Framework Cadmium Succinates of Different Dimensionalities69Organically templated linear and layered cadmium sulfatesElectronic supplementary information (ESI) available: powder diffraction data for IV, view of I down the a-axis, the structure of II in the ac-plane and a polyhedral view of IV in the ab-plane. See http://www.rsc.org/suppdata/dt/b2/b204482j/77Synthesis and Structure of Low-Dimensional Gallium Fluorodiphosphates Seen during the Crystallization of the Three-Dimensional Microporous Gallium Fluorophosphate ULM-334Hydro/Solvothermal Synthesis and Structures of New Zinc Phosphates of Varying Dimensionality36Synthesis and structure of a zinc oxalate with honeycomb layers and zinc phosphates with one- and three-dimensional structures31C4N3OH7·Zn(H2O)HPO4, a Neutral Zincophosphate Cluster26Novel Inorganic Frameworks Constructed from Double-Four-Ring (D4R) Units: Computational Design, Structures, and Lattice Energies of Silicate, Aluminophosphate, and Gallophosphate Candidates87Large cavities with nanosized channels in a three-dimensional neutral framework: structure and properties of a novel oxovanadium arsenate: As2VIVVVO26(OH)]·8H2O10{[Cu(H 2 O) 3 ][Cu(phmal) 2 ]} n : a new two-dimensional copper( ii ) complex with intralayer ferromagnetic interactions (phmal = phenylmalonate dianion)51Aluminophosphonate clusters: a new architecture8Assembly of one-dimensional AlP 2 O 8 3− chains into three-dimensional MAlP 2 O 8 ·C 2 N 2 H 9 frameworks through transition metal cations (M = Ni 2+ , Co 2+ and Fe 2+ )36Isolation of a monomeric hybrid zinc phosphate and its one-dimensional relative24Mixed-valence phosphato–hydrogenphosphato–iron network compounds 1 ∞ {[C 4 N 2 H 11.6 ] 1.5 [Fe II Fe III (PO 4 )(H 0.8 PO 4 ) 2 ]·H 2 O} and 3 ∞ [Fe II 5 Fe III 2 (PO 4 ) 2 (H 0.5 PO 4 ) 4 ]: structure elucidation with the help of Mössbauer spectroscopy and a caveat on X-ray diffraction13Open-framework iron phosphates: Syntheses, structures, sorption studies and oxidation catalysisThis article is based (partly) on a presentation which will be made at the European Research Conference (EURESCO) on "Molecular Crystal Engineering - EuroConference on Design and Preparation of Molecular Materials" (Acquafredda di Maratea, Italy, 31 May - 5 June 2003) organised by the European Science Foundation and supported by the European Commission, Research DG, Human Potential Programme, High-Level Scientific Conferences, Contract HPCF-CT-2002-00270. This information is the sole responsibility of the author(s) and does not reflect the ESF or Community's opinion. The ESF and the Community are not responsible for any use that might be made of data appearing in this publication.28Rational design of porous titanophosphates69Synthesis and characterization of a new layered gallium phosphate [Co(en)3][Ga3(H2PO4)6(HPO4)3] templated by cobalt complex42Transformation of a 4-membered ring zinc phosphate SBU to a sodalite-related 3-dimensional structure through a linear chain structure47Understanding the building-up process of three dimensional open-framework metal phosphates: Acid degradation of the 3D structures to lower dimensional structuresElectronic supplementary information (ESI) available: typical experimental parameters. See http://www.rsc.org/suppdata/cc/b2/b210037c/11(C6H16N2)Zn3(HPO3)4H2O: a new layered zinc phosphite templated by diprotonated trans-1,4-diaminocyclohexane35Organically Templated Linear and Layered Iron Sulfates103Amine-Templated Linear Vanadium Sulfates with Different Chain Structures59An Open-framework Zincophosphate with Intersecting Channels3Synthesis and structure of a new layered zinc phosphite (C5H6N2)Zn(HPO3) containing helical chains107Role of Chains in the Formation of Extended Framework Tin(II) Phosphates and Related Materials30Hydrothermal Synthesis of Nanoporous Metalofluorophosphates. 2. In Situ and ex Situ 19F and 31P NMR of Nano- and Mesostructured Titanium Phosphates Crystallogenesis26Synthesis, structure and properties of a neutral zincophosphate monomer decorated with 2,2′-bipyridine ligands20Comparison of one-, two-, and three-dimensional iron phosphates containing ethylenediamine20Synthesis and structure of organically templated lanthanum sulfate [C4N3H16][La(SO4)3]·H2O57Synthesis of a Single Four-Ring (S4R) Molecular Zinc Phosphate and Its Assembly to an Extended Polymeric Structure: A Single-Crystal and in-Situ MAS NMR Investigation53Structure and Properties of a Novel 3D Straight-Channel Polyoxovanadate and an Unexpected Trimeric Barbiturate Obtained by Hydrothermal Reactions352D molecular square grid of Cobalt(II) with tridentate phenylglycinate and mandelate: structure and magnetism32Synthesis and characterization of [Zn(2,2′-bipy)]2(H2PO3)4: A neutral zinc phosphite cluster containing ZnO3N2 and H2PO3 units18Hydrothermal synthesis, crystal structure and characterizations of a lanthanum(III) sulfate oxalate with a 3D network structure53Solvothermal synthesis and structures of one- and two-dimensional zinc phosphates11Host–guest and network structures of some tetraphenylmethane derivatives23Molecular zinc phosphonates: synthesis and X-ray crystal structures of [{(ZnMe) 4 (THF) 2 }{tBuPO 3 } 2 ] and [{(ZnEt) 3 (Zn(THF)) 3 }{tBuPO 3 } 4 {μ 3 -OEt}]44Open-framework zinc and cobalt phosphates synthesized by the tributylphosphate route25Organically templated rare earth sulfates with three-dimensional and layered structures68Synthesis and characterization of a family of lamellar manganese phosphates0Synthesis and structure of a new three-dimentional open-framework zinc phosphate with 12-membered ring channels0The first organically templated open-framework metal selenate with a three-dimensional architecture30Toward the rational design and synthesis of inorganic microporous and related materials10Synthesis, Structure, and the Unusual Magnetic Properties of an Amine-Templated Iron(II) Sulfate Possessing the Kagomé Lattice102Hydrothermal synthesis and structure of a novel solid material with 3-D open-framework: (NH3CH2CH2NH3)(NH3CH2CH2NH2)3Na3[Co4Mo12O24(OH)6 (H2O)2(HPO4)2(PO4)6]·8H2O31Template-Free Synthesis of the Nanoporous Nickel Phosphate VSB-5 under Microwave Irradiation44Crystal structure of bis(ethylenediammonium) discandium(III) hexafluoride bis(hydrogenphosphate), (C2N2H10)2Sc2F6(HPO4)22A novel self-complementary three-dimensional inorganic network organized by H-bond dimers of inorganic chains Synthesis and crystal structure of (C6H16N2)[Zn(HPO4)2]5Kinetic and Mechanistic Investigations of Hydrothermal Transformations in Zinc Phosphates64(C6H17N3)[Zn4(PO4)2(HPO3)2]: a new layered zinc phosphate–phosphite templated by 1-(2-Aminoethyl) piperazine10[Co(en)3][In3(H2PO4)6(HPO4)3]·H2O: A new layered indium phosphate templated by cobalt complex23Hydrothermal synthesis and structure of a molybdenum(VI) phosphate cluster and a three dimensional cobalt molybdenum(V) phosphate44Synthesis and characterization of two novel organocation containing group 13 metal ethylenediphosphonates11Syntheses, characterizations and crystal structures of three new organically templated or organically bonded zinc selenates25Syntheses and structures of two new 3D open-framework germanates constructed from Ge9O18(OH)4 clusters22Synthesis and structure of [C3N2H5][Cu(H2PO4)2Cl]·H2O with a chain structure: the first example of an organically templated copper (II) phosphate25Syntheses and Characterization of Two New Open-Framework Zinc Phosphites with 12-Ring Channels, [H3N(CH2)4NH3]·[Zn3(HPO3)4]·H2O and [C3N2H5]2·[Zn3(HPO3)4]25Water-vapor-induced transformation of two-dimensional vanadyl hydrogen phosphate hemihydrate, VOHPO4·0.5H2O, to one-dimensional tetrahydrate, VOHPO4·4H2O0Synthesis and characterisation of a new vanadyl oxalatophosphate compound: (C10H10N2)[(VO)(HPO4)]2(C2O4)16A Templated Bimetallic Phosphate Open-structure with 16-MR Channels6Observation and Reactivity of the Chainlike Species ([Al(PO4)2]3-)n during the X-ray Diffraction Investigation of the Hydrothermal Synthesis of the Super-sodalite Sodium Aluminophosphate MIL-74 (Na2Al7(PO4)12·4trenH3·Na(H2O)16)42A New Inorganic‐Organic Hybrid with Zinc Phosphate Layers Pillared by the 4, 4'‐Bipyridine Units10Synthesis and Characterization of a Molecular Zinc Phosphate Ni(2, 2'‐bipy)3·[ZnCl(H2PO4)3]4Isomorphous Substitution of Transition-Metal Ions in the Nanoporous Nickel Phosphate VSB-549Knotted Network Consisting of 3-Threads and a Zwitterionic One-Dimensional Polymorphs oftrans-3-(3-Pyridyl)acrylate of Cobalt and Nickel, MII(C8H6NO2)2(H2O)21501,2-, 1,3- and 1,4-Benzenedicarboxylates of Cd and Zn of different dimensionalities: Process of formation of the three-dimensional structure94A two-dimensional cationic lattice built from [Zn6(HPO4)2(PO4)2]2+ clusters57Co-templated synthesis and characterization of two new 1D zincophosphates, [Co III (dien) 2 ][Zn(PO 4 )(HPO 4 )]·H 3 BO 3 and [Co III (dien) 2 ][Zn 2 (PO 4 )(HPO 4 ) 2 ]·C 2 H 6 O 24Controlled Nanoparticle Metal Phosphates (Metal=Al, Fe, Ce, and Sr) Coatings on LiCoO[sub 2] Cathode Materials99Hydrothermal synthesis and structure determination of UH-6 and UH-8: Two novel zincophosphates containing cobalt complexes1Making crystals from crystals: a green route to crystal engineering and polymorphism211The pH-controlled hydrothermal synthesis and crystal structures of two zinc N,N′-piperazinebis(methylenephosphonate) frameworks26New Zinc Phosphates Decorated by Imidazole-Containing Ligands95Synthesis and crystal structure of a 3-D zinc phosphate, [C5N2H14][Zn2(PO3(OH))3], containing (4.8) net sheets7Coordination Polymers Based on Inorganic Lanthanide(III) Sulfate Skeletons and an Organic Isonicotinate N-oxide Connector: Segregation into Three Structural Types by the Lanthanide Contraction Effect172Toward the Rational Design of Open-Framework Materials21Hydrothermal reversible interconversion of two zincophosphates with three-dimensional open frameworks containing diprotonated 1,4-diazacycloheptane molecules6Zn2(bipy)2V4TeO14: A new type of layered vanadium(V) tellurite with organically covalently bonded zinc(II) complex12Synthesis and Structure of a Novel Three-dimensional Organo-zincophosphite with Three Intersecting Channels3Five New Zinc Phosphite Structures: Tertiary Building Blocks in the Construction of Hybrid Materials75A novel organically templated three-dimensional open framework vanadium tellurite: (NH3CH2CH2NH3)2V2Te6O1812Synthesis, Crystal Structure, and Solid-State NMR Spectroscopy of a New Open-Framework Aluminophosphate (NH4)2Al4(PO4)4(HPO4)·H2O27[C10N2H10][ZnCl(HPO4)]2: A New Templated Zincophosphate Containing Tetrahedral Nets with 63 Topology9Syntheses and crystal structures of the first organically templated metal tellurites16A mixed-valence vanadium phosphate with odd-number rings: Synthesis and structure of [(C6H16N2)3(VO)(V2O4)2(PO4)4· 2H2O]11Synthesis, structure and properties of a new layered gadolinium benzenedicarboxylate with piperazine4Syntheses and characterization of two new zinc phosphites with 1D chains decorated by Zn-centered complexes23Synthesis and characterization of two new open-framework zinc phosphites [M(C6N4H18)][Zn3(HPO3)4] (M=Ni, Co) with multi-directional intersecting 12-membered ring channels17Facile Synthesis of Nanoporous Nickel Phosphates without Organic Templates under Microwave Irradiation93An Organo-templated Iron Zincophosphate with Zeolite DFT Topology11Novel Zinc Phosphate Topologies Defined by Organic Ligands95{Zn3(Et2O)2[(EtO)PO2(C6H5NH)]6·2THF}: A Trinuclear Zinc Amidophosphate with an Hourglass Structure6Supramolecular assembly of coordination networks in silver(I) triple salts containing acetylenediide and some N,O-donor ligands8MnII/CoII‐Terephthalate Frameworks Containing Dipyridine Coligands: Syntheses, Crystal Structures, Magnetic Behaviors, and Thermal Studies74Hydrothermal synthesis and structures of two zero-dimensional zinc phosphate polymorphs4Organically‐Templated Zinc and Thorium Sulfates with Chain and Layered Structures17A tetranuclear zinc cluster, (bipy)4Zn4(HPO3)4, that stabilizes a hydrogen bonded chain of water molecules: Transformation of a zinc phosphite 4-ring to a cluster16Polymorphism of [Zn(2,2′‐bipy)(H2PO4)2]261, 2-, 1, 3- and 1, 4-Cyclohexanedicarboxylates of Cd and Mn with chain and layered structures54Syntheses, Structures, and Magnetic Properties of Inorganic−Organic Hybrid Cobalt(II) Phosphites Containing Bifunctional Ligands137Hydrogen-bond tuning of ferromagnetic interactions: synthesis, structure and magnetic properties of polynuclear copper(ii) complexes incorporating p-block oxo-anions44Organically-templated metal sulfates, selenites and selenates194Structural diversity and chemical trends in hybrid inorganic–organic framework materials1082Triarylcarbinol derivatives barter intermolecular interactions to accommodate substituents and create polymorphs9Two novel luminescent lanthanide sulfate–carboxylates with an unusual 2-D bamboo-raft-like structure based on the linkages of left- and right-handed helical tubes involving in situ decarboxylation147Synthesis, structures of cobalt/copper complexes and magnetic property of copper complex with the mixed ligands 5-nitro-1,3-benzenedicarboxylic acid and imidazole34Synthesis and Characterization of New Open-Framework Iron(II) Phosphate with 1D Tube and Double Layer Structure, NaFe2(PO4)(HPO4)11Assembly of a Secondary Building Unit (SBU) into Two- and Three-Dimensional Structures in Lanthanide Benzenedicarboxylates51A novel hydrogen-bonded cyclic dibromide in an organic diammonium salt7Hydrothermal synthesis, structure and magnetic properties of a new three-dimensional iron arsenate [C6N4H21][FeIII3(HAsO4)6]4Synthesis of open-framework zinc phosphite structures of varying dimensionality17Hydrothermal synthesis and characterization of the first 1-D indiumphosphate chain In2(HPO4)2(H2PO4)2F2·C4N2H12, a precursor for high dimensional structures9[C4N2H12]2[In3(HPO4)5(H2PO4)F2]: The first 2-D fluorinated indium phosphate with double-sheet layers and 8-ring channels8Syntheses and Structures of Two Low-Dimensional Beryllium Phosphate Compounds: [C5H14N2]2[Be3(HPO4)5]·H2O and [C6H18N2]0.5[Be2(PO4)(HPO4)OH]·0.5H2O16Assembly of Lipophilic Tetranuclear (Cu4 and Zn4) Molecular Metallophosphonates from 2,4,6-Triisopropylphenylphosponic Acid and Pyrazole Ligands88Hydrothermal synthesis of a new open-framework zinc phosphate containing 20-ring channels5Synthesis and characterization of a new open-framework aluminophosphate C4N3H16·Al4P5O20(H2O)2 (AlPO-CJ31)9Synthesis and structure of the first organic–inorganic hybrid tin (II) chlorosulfate: [C6N2H14][SnCl2SO4]2[Ni(C6N2H14)2][Zn4(H2O)(HPO3)5]: A new open-framework zinc phosphite with intersecting 8-, 12- and 16-ring channels15A novel zeolite-like structure based on zinc and aluminum phosphate synthesized from H3PO3-containing gel5

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  1. Ambient temperature crystallisation of a lamellar gallium fluorophosphate from the synthesis solution of microporous ULM-5

    Chemical Communications · 2001-01-01

    Carine Livage, Franck Millange, Thierry Loiseau, Nathalie Simon, Gérard Férey, Richard I. Walton, Dermot M. O'Hare

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  2. Direct in situ observation of increasing structural dimensionality during the hydrothermal formation of open-framework zinc phosphates

    Chemical Communications · 2001-01-01

    Richard I. Walton, Alexander J. Norquist, Dermot M. O'Hare, S. Neeraj, Srinivasan Natarajan, C.N.R. Rao

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  3. Synthesis of a hierarchy of zinc oxalate structures from amine oxalates

    Journal of the Chemical Society Dalton Transactions · 2001-01-01

    Ramanathan Vaidhyanathan, Srinivasan Natarajan, C. N. R. Rao

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  4. Transformations of low-dimensional zinc phosphates to complex open-framework structures. Part 1: zero-dimensional to one-, two- and three-dimensional structures

    Journal of Materials Chemistry · 2001-01-01

    Ayi A. Ayi, Amitava Choudhury, Srinivasan Natarajan, S. Neeraj, C. N. R. Rao

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  5. Transformations of the low-dimensional zinc phosphates to complex open-framework structures. Part 2: one-dimensional ladder to two- and three-dimensional structures

    Journal of Materials Chemistry · 2001-01-01

    Amitava Choudhury, S. Neeraj, Srinivasan Natarajan, C. N. R. Rao

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  6. Basic building units, self-assembly and crystallization in the formation of complex inorganic open architectures

    Journal of Chemical Sciences · 2001-10-01

    C. N. R. Rao

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  7. Hydrothermal synthesis and structural characterization of a new layered zincophosphate co-templated by diprotonated 1,6-diaminohexane and orthoboric acid moleculesElectronic supplementary information (ESI) available: powder XRD data for I. See http://www.rsc.org/suppdata/jm/b1/b105057p/

    Journal of Materials Chemistry · 2001-11-21

    Michael Wiebcke

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  8. Synthesis, Crystal Structure, and Solid State NMR Spectroscopy of (C10N4H28)[Zn6(HPO4)2(PO4)4]·2H2O, a New Zinc Phosphate with a Layer Structure

    Journal of Solid State Chemistry · 2001-12-01

    Yung-Ping Chiang, Hsien‐Ming Kao, Kwang‐Hwa Lii

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  9. An approach to the synthesis of organically templated open-framework metal sulfates by the amine–sulfate route

    Chemical Communications · 2001-12-10

    Amitava Choudhury, Jayaraman Krishnamoorthy, C. N. R. Rao

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  10. A sponge-like luminescent coordination framework via an Aufbau approach

    Chemical Communications · 2002-01-01

    Brett D. Chandler, Adrien P. Côté, David T. Cramb, Josephine Mary Hill, George K. H. Shimizu

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  11. Two new diamine templated lanthanum sulfates, La 2 (H 2 O) 2 (C 4 H 12 N 2 )(SO 4 ) 4 and La 2 (H 2 O) 2 (C 2 H 10 N 2 ) 3 (SO 4 ) 6 ·4H 2 O, with 3D and 2D crystal structures

    Journal of Materials Chemistry · 2002-01-01

    Thierry Bataille B, Daniel Louer

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  12. A Coordination Polymer of Cobalt(II)−Glutarate: Two-Dimensional Interlocking Structure by Dicarboxylate Ligands with Two Different Conformations

    Inorganic Chemistry · 2002-01-10

    Lee, Kim, Duk‐Young Jung

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  13. [Zn3(HPO4)4](NMe4)2: a zincophosphate containing interruptions of isolated hydrogen-bonding [H–O(P)]4 groupings within a novel three-dimensional four-connected framework

    Journal of Materials Chemistry · 2002-01-24

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  14. Synthesis and Structure of a Novel Layered Zincophosphate Zn4P3O11(OH)·3C3N2H4 with Organic Amine Acting as Ligand

    Journal of Solid State Chemistry · 2002-02-01

    Yan Xing, Yunling Liu, Zhan Shi, Ping Zhang, Yunlong Fu, Chang Cheng, Wenqin Pang

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  15. Perovskites by Design: A Toolbox of Solid-State Reactions

    Chemistry of Materials · 2002-02-09

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  16. Reversible Gas−Solid Reactions between the Organometallic Zwitterion [(η5-C5H4COOH)(η5-C5H4COO)CoIII] and Vapors of Trifluoroacetic and Tetrafluoroboric Acids

    Organometallics · 2002-02-19

    Dario Braga, Gianna Cojazzi, Dario Emiliani, Lucia Maini, Fabrizia Grepioni

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  17. Transformations of two-dimensional layered zinc phosphates to three-dimensional and one-dimensional structures

    Journal of Materials Chemistry · 2002-03-05

    Amitava Choudhury, S. Neeraj, Srinivasan Natarajan, C.N.R. Rao

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  18. Synthesis of a layered zinc phosphate, [NH3(CH2)2NH2(CH2)3NH3][Zn2(PO4)(HPO4)2]·H2O, and its transformation to a extra-large pore three-dimensional zinc phosphate, [NH3(CH2)2NH2(CH2)3NH3][Zn3(PO4)(HPO4)3]

    Chemical Communications · 2002-03-12

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  19. Synthesis and Structure of an Open-Framework Zincophosphate [C6N4H22][ZnPO4]4

    Journal of Solid State Chemistry · 2002-04-01

    Yongnan Zhao, Jing Ju, Xiangming Chen, Xiuhong Li, Ru‐Ji Wang, Zhenhong Mai

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  20. A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates

    Angewandte Chemie International Edition · 2002-04-02

    Sandip Chakrabarti, Srinivasan Natarajan

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  21. A Reactive Intermediate in the Synthesis of Iron Arsenates: Synthesis of the First One-Dimensional Iron Arsenate Oxalate and Its Transformation into Two- and Three-Dimensional Iron Arsenates

    Angewandte Chemie · 2002-04-02

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  22. Synthesis and structure of a layered zinc phosphate–acetate, [C5H10NH2]2[Zn(ZnO2CCH3)(PO4)(HPO4)]

    Journal of the Chemical Society Dalton Transactions · 2002-04-11

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  23. Hydrothermal Synthesis and Structure of a Neutral Open-Framework Zincophosphate

    Chemistry Letters · 2002-05-01

    Yongnan Zhao, Youwei Yao, Xiuhong Li, Xiangming Chen, Ming Li, Zhenhong Mai

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  24. Synthesis of Open-Framework Iron Phosphates, [C6N2H14][FeIII2F2(HPO4)2(H2PO4)2]·2H2O and [C6N2H14]2[FeIII3(OH)F3(PO4)(HPO4)2]2·H2O, with One- and Three-Dimensional Structures

    Journal of Solid State Chemistry · 2002-05-01

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  25. Manganese Metallamacrocycles with Various Coordination Solvents

    Bulletin of the Korean Chemical Society · 2002-05-20

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  26. Synthesis and Structure of a New Layered Zincophosphate Zn6(PO4)5(HPO4)·C8N5H28·5H2O, Intercalated with Quintuply Protonated Tetraethylenepentamine

    Journal of Solid State Chemistry · 2002-07-01

    Yunling Liu, Wang Liu, Yan Xing, Zhan Shi, Yunlong Fu, Wenqin Pang

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  27. Synthesis and structure of an open-framework cobalt zincophosphate

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  28. Recent results from the in situ study of hydrothermal crystallisations using time-resolved X-ray and neutron diffraction methods

    Faraday Discussions · 2002-07-30

    Richard I. Walton, Alexander J. Norquist, Ronald I. Smith, Dermot M. O'Hare

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  29. Hydrothermal synthesis, structure and magnetism of square-grid cobalt(ii)-carboxylate layered compounds with and without pillars

    Journal of the Chemical Society Dalton Transactions · 2002-08-14

    Hitoshi Kumagai, Yoshimi Oka, Katsuya Inoue, Mohamedally Kurmoo

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  30. The hydrogen oxalate anion allows one-dimensional columnar aggregation of organometallic sandwich cations

    New Journal of Chemistry · 2002-08-27

    Dario Braga, Matthieu Eckert, M. Fraccastoro, Lucia Maini, Fabrizia Grepioni, Andréa Caneschi, Roberta Sessoli

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  31. Open-Framework Rubidium Halides Incorporated in Cadmium Oxalate Host Lattices

    Journal of Solid State Chemistry · 2002-09-01

    R. Vaidhyanathan, Srinivasan Natarajan, C.N.R. Rao

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  32. Open-Framework Cadmium Succinates of Different Dimensionalities

    Inorganic Chemistry · 2002-09-13

    Ramanathan Vaidhyanathan, Srinivasan Natarajan, C. N. R. Rao

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  33. Organically templated linear and layered cadmium sulfatesElectronic supplementary information (ESI) available: powder diffraction data for IV, view of I down the a-axis, the structure of II in the ac-plane and a polyhedral view of IV in the ab-plane. See http://www.rsc.org/suppdata/dt/b2/b204482j/

    Journal of the Chemical Society Dalton Transactions · 2002-09-13

    Geo Paul, Amitava Choudhury, C. N. R. Rao

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  34. Synthesis and Structure of Low-Dimensional Gallium Fluorodiphosphates Seen during the Crystallization of the Three-Dimensional Microporous Gallium Fluorophosphate ULM-3

    Chemistry of Materials · 2002-09-14

    Franck Millange, Richard I. Walton, Nathalie Guillou, Thierry Loiseau, Dermot M. O'Hare, Gérard Férey

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  35. Hydro/Solvothermal Synthesis and Structures of New Zinc Phosphates of Varying Dimensionality

    Inorganic Chemistry · 2002-09-21

    Srinivasan Natarajan

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  36. Synthesis and structure of a zinc oxalate with honeycomb layers and zinc phosphates with one- and three-dimensional structures

    Solid State Sciences · 2002-10-01

    Srinivasan Natarajan

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  37. C4N3OH7·Zn(H2O)HPO4, a Neutral Zincophosphate Cluster

    Inorganic Chemistry · 2002-10-26

    I. Ross Macdonald, William T. A. Harrison

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  38. Novel Inorganic Frameworks Constructed from Double-Four-Ring (D4R) Units: Computational Design, Structures, and Lattice Energies of Silicate, Aluminophosphate, and Gallophosphate Candidates

    Journal of the American Chemical Society · 2002-11-28

    Caroline Mellot‐Draznieks, Stéphanie Girard, Gérard Férey

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  39. Large cavities with nanosized channels in a three-dimensional neutral framework: structure and properties of a novel oxovanadium arsenate: As2VIVVVO26(OH)]·8H2O

    Journal of Solid State Chemistry · 2002-12-01

    Yongnan Zhao, Yafeng Li, Qingsheng Liu, Xiangming Chen, Yong Wang, LI Xiu-hong, Ming Li, Zhenhong Mai

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  40. {[Cu(H 2 O) 3 ][Cu(phmal) 2 ]} n : a new two-dimensional copper( ii ) complex with intralayer ferromagnetic interactions (phmal = phenylmalonate dianion)

    New Journal of Chemistry · 2003-01-01

    Jorge Pasán, Joaquín Sanchiz, Catalina Ruíz-Pérez, Francesc Lloret, Miguel Julve

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  41. Aluminophosphonate clusters: a new architecture

    Dalton Transactions · 2003-01-01

    Thierry Azaı̈s, Christian Bonhomme, Laure Bonhomme-Coury, Guido Kickelbick

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  42. Assembly of one-dimensional AlP 2 O 8 3− chains into three-dimensional MAlP 2 O 8 ·C 2 N 2 H 9 frameworks through transition metal cations (M = Ni 2+ , Co 2+ and Fe 2+ )

    Dalton Transactions · 2003-01-01

    Kaixue Wang, Jihong Yu, Yu Song, Ruren Xu

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  43. Isolation of a monomeric hybrid zinc phosphate and its one-dimensional relative

    Dalton Transactions · 2003-01-01

    Zhien Lin, Youwei Yao, Jie Zhang, Guo‐Yu Yang

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  44. Mixed-valence phosphato–hydrogenphosphato–iron network compounds 1 ∞ {[C 4 N 2 H 11.6 ] 1.5 [Fe II Fe III (PO 4 )(H 0.8 PO 4 ) 2 ]·H 2 O} and 3 ∞ [Fe II 5 Fe III 2 (PO 4 ) 2 (H 0.5 PO 4 ) 4 ]: structure elucidation with the help of Mössbauer spectroscopy and a caveat on X-ray diffraction

    Dalton Transactions · 2003-01-01

    Khalid Hamad Abu-Shandi, Heiner WINKLER, Michael Gerdan, Franziska Emmerling, Biao Wu, Christoph Janiak

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  45. Open-framework iron phosphates: Syntheses, structures, sorption studies and oxidation catalysisThis article is based (partly) on a presentation which will be made at the European Research Conference (EURESCO) on "Molecular Crystal Engineering - EuroConference on Design and Preparation of Molecular Materials" (Acquafredda di Maratea, Italy, 31 May - 5 June 2003) organised by the European Science Foundation and supported by the European Commission, Research DG, Human Potential Programme, High-Level Scientific Conferences, Contract HPCF-CT-2002-00270. This information is the sole responsibility of the author(s) and does not reflect the ESF or Community's opinion. The ESF and the Community are not responsible for any use that might be made of data appearing in this publication.

    CrystEngComm · 2003-01-01

    Khalid Hamad Abu-Shandi, Heiner WINKLER, Biao Wu, Christoph Janiak

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  46. Rational design of porous titanophosphates

    Chemical Communications · 2003-01-01

    Christian Serre, Françis Taulelle, Gérard Férey

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  47. Synthesis and characterization of a new layered gallium phosphate [Co(en)3][Ga3(H2PO4)6(HPO4)3] templated by cobalt complex

    Journal of Solid State Chemistry · 2003-01-01

    Yu Wang, Jihong Yu, Zhan Shi, Ruren Xu

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  48. Transformation of a 4-membered ring zinc phosphate SBU to a sodalite-related 3-dimensional structure through a linear chain structure

    Chemical Communications · 2003-01-01

    Meenakshi Dan, D. Udayakumar, C. N. R. Rao

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  49. Understanding the building-up process of three dimensional open-framework metal phosphates: Acid degradation of the 3D structures to lower dimensional structuresElectronic supplementary information (ESI) available: typical experimental parameters. See http://www.rsc.org/suppdata/cc/b2/b210037c/

    Chemical Communications · 2003-01-06

    Amitava Choudhury, C.N.R. Rao

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  50. (C6H16N2)Zn3(HPO3)4H2O: a new layered zinc phosphite templated by diprotonated trans-1,4-diaminocyclohexane

    Journal of Solid State Chemistry · 2003-02-01

    Yu Wang, Jihong Yu, Yi Li, Yu Du, Ruren Xu, Ling Ye

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