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RESEARCH PAPER · Inorganic Chemistry · 2015

Crystal Growth of Four Oxovanadium(IV) Tartrates Prepared via a Mild Two-Step Hydrothermal Method: Observation of Spin-Dimer Behavior and Second Harmonic Generation

Anthony J. Cortese, Branford O. Wilkins, Mark D. Smith, Jeongho Yeon, Gregory W. Morrison, T. Thao Tran, P. Shiv Halasyamani, Hans‐Conrad zur Loye

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Crystal Growth of Four Oxovanadium(IV) Tartrates Prepared via a Mild Two-Step Hydrothermal Method: Observation of Spin-Dimer Behavior and Second Harmonic GenerationOriginalSynthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 617Single crystal growth and characterization of the first reduced lanthanum molybdenum oxychloride, La20Mo12O63Cl4, with an unusual trigonal prismatic MoO6 unit14Structural and spectral properties of tartrato complexes of vanadium(V) from quantum chemical calculations0Single crystal growth and characterization of NaxLn1−xMoO4, Ln=La, Ce, Pr, Nd, Sm, and Eu (x=0.397–0.499)9Understanding the Formation of Salt-Inclusion Phases: An Enhanced Flux Growth Method for the Targeted Synthesis of Salt-Inclusion Cesium Halide Uranyl Silicates61Oxygen Anion Solubility as a Factor in Molten Flux Crystal Growth, Synthesis, and Characterization of Four New Reduced Lanthanide Molybdenum Oxides: Ce4.918(3)Mo3O16, Pr4.880(3)Mo3O16, Nd4.910(3)Mo3O16, and Sm4.952(3)Mo3O1615Crystal growth, structure, and properties, of a new oxovanadium(IV) phosphate material, [H2en]4[V7P8O35(OH)6(H2O)]·3H2O prepared via a mild one step hydrothermal route4Interrelationship of the structural and nonlinear-optical properties of the carbonate crystals2Application of a mild hydrothermal method to the synthesis of mixed transition-metal( ii )/uranium( iv ) fluorides18Where Do New Materials Come From? Neither the Stork nor the Birds and the Bees! In Search of the Next “First Material”1Li3VO4: A Promising Mid-Infrared Nonlinear Optical Material with Large Laser Damage Threshold51Comparative Interrelationship of the Structural, Nonlinear-Optical and Other Acentric Properties for Oxide, Borate and Carbonate Crystals16One-step mild hydrothermal method to prepare low valent sodium vanadium(III) monohydrogenphosphate: NaV(HPO4)24A pair of new chiral polyoxovanadates with decent NLO properties19[Co(H2O)6]3[U2O4F7]2: A Model System for Understanding the Formation of Dimensionally Reduced Materials11pH Driven Hydrothermal Syntheses of Neodymium Sulfites and Mixed Sulfate-Sulfites7Mixed ligand oxidovanadium(IV) complexes: Synthesis, spectral, structural characterization and catalytic degradations of methyl orange10Exploring the Magnetic Interaction of Asymmetric Structures Based on Chiral VIII8 Clusters17Lewis Acid Dominant Windmill-Shaped V8 Clusters: A Bifunctional Heterogeneous Catalyst for CO2 Cycloaddition and Oxidation of Sulfides139Eight-membered ring petal-shaped V8 cluster: An efficient heterogeneous catalyst for selective sulfur oxidation6Chiral Template‐Driven Macroscopic Chirality Control: Structure‐Second‐Harmonic Generation Properties Relationship24Protonated and deprotonated vanadyl imidazole tartrates for the mimics of the vanadium coordination in the FeV-cofactor of V-nitrogenase1Flux Synthesis, UV–vis Absorbance, and Magnetism of Cesium Copper Silicates with an Isolated Super-Super Exchange Spin Dimer in Cs6Cu2Si9O230Synthesis and Structure of High-Nuclearity Carboxylate-Modified Heteropolyoxovanadate Serving as a Heterogeneous Catalyst for Selective Oxidation of Alkylbenzenes8Controlling Electron Delocalization in Vanadium‐Based Hybrid Bronzes through Molecular Templation11Controlling Electron Delocalization in Vanadium‐Based Hybrid Bronzes through Molecular Templation0Visible-Light-Induced Oxidation of Styrene by a Polyoxovanadate-Based Carboxylate Derivative9A Hybrid Bronze Age: Progress and Potential in Mixed-Valence Organic–Inorganic Metal Oxides6

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  1. Synthetic strategies for new vanadium oxyfluorides containing novel building blocks: structures of V( iv ) and V( v ) containing Sr 4 V 3 O 5 F 13 , Pb 7 V 4 O 8 F 18 , Pb 2 VO 2 F 5 , and Pb 2 VOF 6

    CrystEngComm · 2015-01-01

    Jeongho Yeon, Justin B. Felder, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  2. Single crystal growth and characterization of the first reduced lanthanum molybdenum oxychloride, La20Mo12O63Cl4, with an unusual trigonal prismatic MoO6 unit

    Solid State Sciences · 2015-07-30

    Anthony J. Cortese, Branford O. Wilkins, Mark D. Smith, Gregory W. Morrison, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  3. Structural and spectral properties of tartrato complexes of vanadium(V) from quantum chemical calculations

    Theoretical Chemistry Accounts · 2015-09-16

    Gabriela Orešková, Lukáš Krivosudský, Ján Šimunek, Jozef Noga

    Read original paper ↗ ·

  4. Single crystal growth and characterization of NaxLn1−xMoO4, Ln=La, Ce, Pr, Nd, Sm, and Eu (x=0.397–0.499)

    Journal of Solid State Chemistry · 2016-05-09

    Anthony J. Cortese, Dileka Abeysinghe, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  5. Understanding the Formation of Salt-Inclusion Phases: An Enhanced Flux Growth Method for the Targeted Synthesis of Salt-Inclusion Cesium Halide Uranyl Silicates

    Journal of the American Chemical Society · 2016-05-24

    Gregory W. Morrison, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  6. Oxygen Anion Solubility as a Factor in Molten Flux Crystal Growth, Synthesis, and Characterization of Four New Reduced Lanthanide Molybdenum Oxides: Ce4.918(3)Mo3O16, Pr4.880(3)Mo3O16, Nd4.910(3)Mo3O16, and Sm4.952(3)Mo3O16

    Crystal Growth & Design · 2016-07-06

    Anthony J. Cortese, Dileka Abeysinghe, Branford O. Wilkins, Mark D. Smith, Vitaly A. Rassolov, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  7. Crystal growth, structure, and properties, of a new oxovanadium(IV) phosphate material, [H2en]4[V7P8O35(OH)6(H2O)]·3H2O prepared via a mild one step hydrothermal route

    Solid State Sciences · 2016-08-07

    Anthony J. Cortese, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  8. Interrelationship of the structural and nonlinear-optical properties of the carbonate crystals

    International Scientific-Technical Conference on Actual Problems of Electronics Instrument Engineering (APEIE) · 2016-10-01

    Boris I. Kidyarov, Vladimir K. Makukha

    Read original paper ↗ ·

  9. Application of a mild hydrothermal method to the synthesis of mixed transition-metal( ii )/uranium( iv ) fluorides

    Inorganic Chemistry Frontiers · 2017-01-01

    Justin B. Felder, Jeongho Yeon, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  10. Where Do New Materials Come From? Neither the Stork nor the Birds and the Bees! In Search of the Next “First Material”

    Scholar Commons (University of South Carolina) · 2017-01-01

    Gregory W. Morrison, Dileka Abeysinghe, Justin B. Felder, Shani Egodawatte, Timothy Ferreira, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  11. Li3VO4: A Promising Mid-Infrared Nonlinear Optical Material with Large Laser Damage Threshold

    Crystal Growth & Design · 2017-03-30

    Zhaohui Chen, Zhizhong Zhang, Xiaoyu Dong, Yunjing Shi, Yaqin Liu, Qun Jing

    Read original paper ↗ ·

  12. Comparative Interrelationship of the Structural, Nonlinear-Optical and Other Acentric Properties for Oxide, Borate and Carbonate Crystals

    Crystals · 2017-04-12

    Boris I. Kidyarov

    Read original paper ↗ ·

  13. One-step mild hydrothermal method to prepare low valent sodium vanadium(III) monohydrogenphosphate: NaV(HPO4)2

    Solid State Sciences · 2017-05-04

    Dileka Abeysinghe, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  14. A pair of new chiral polyoxovanadates with decent NLO properties

    Dalton Transactions · 2018-01-01

    Jia‐Peng Cao, Yao Kun Xiong, Xi‐Ming Luo, Lu Chen, Jie Shi, Mengjie Zhou, Yan Xu

    Read original paper ↗ ·

  15. [Co(H2O)6]3[U2O4F7]2: A Model System for Understanding the Formation of Dimensionally Reduced Materials

    Crystal Growth & Design · 2018-01-09

    Justin B. Felder, Mark D. Smith, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  16. pH Driven Hydrothermal Syntheses of Neodymium Sulfites and Mixed Sulfate-Sulfites

    Crystal Growth & Design · 2018-08-03

    Jakob T. Dovgan, Matthew J. Polinski, Brandon Q. Mercado, Eric M. Villa

    Read original paper ↗ ·

  17. Mixed ligand oxidovanadium(IV) complexes: Synthesis, spectral, structural characterization and catalytic degradations of methyl orange

    Inorganica Chimica Acta · 2018-11-02

    Shuang-Shuang Zhu, Xin Yu Ming Dong, Zhao‐Hui Zhou

    Read original paper ↗ ·

  18. Exploring the Magnetic Interaction of Asymmetric Structures Based on Chiral VIII8 Clusters

    Inorganic Chemistry · 2019-02-07

    Jia‐Peng Cao, Yun‐Shan Xue, Zhao‐Bo Hu, Xi‐Ming Luo, Chenhui Cui, You Song, Yan Xu

    Read original paper ↗ ·

  19. Lewis Acid Dominant Windmill-Shaped V8 Clusters: A Bifunctional Heterogeneous Catalyst for CO2 Cycloaddition and Oxidation of Sulfides

    Journal of the American Chemical Society · 2019-11-17

    Jia‐Peng Cao, Yun‐Shan Xue, Ning-Fang Li, Jun-Jie Gong, Run‐Kun Kang, Yan Xu

    Read original paper ↗ ·

  20. Eight-membered ring petal-shaped V8 cluster: An efficient heterogeneous catalyst for selective sulfur oxidation

    Inorganica Chimica Acta · 2020-12-16

    Qing-Dong Ping, Jia‐Peng Cao, Ye‐Min Han, Mu‐Xiu Yang, Ya-Lin Hong, Jia-Nian Li, Ji‐Lei Wang, Jiali Chen, Hua Mei, Yan Xu

    Read original paper ↗ ·

  21. Chiral Template‐Driven Macroscopic Chirality Control: Structure‐Second‐Harmonic Generation Properties Relationship

    European Journal of Inorganic Chemistry · 2020-12-22

    Hongil Jo, Xinglong Chen, Hee‐Seung Lee, Kang Min Ok

    Read original paper ↗ ·

  22. Protonated and deprotonated vanadyl imidazole tartrates for the mimics of the vanadium coordination in the FeV-cofactor of V-nitrogenase

    Dalton Transactions · 2023-01-01

    Shuang-Shuang Zhu, Zhen‐Lang Xie, Lan Qing Deng, Siyuan Wang, Lubin Ni, Zhao‐Hui Zhou

    Read original paper ↗ ·

  23. Flux Synthesis, UV–vis Absorbance, and Magnetism of Cesium Copper Silicates with an Isolated Super-Super Exchange Spin Dimer in Cs6Cu2Si9O23

    Inorganic Chemistry · 2023-07-12

    Gregory W. Morrison, Virginia G. Jones, K. Pilar Zamorano, John E. Greedan, Hans‐Conrad zur Loye

    Read original paper ↗ ·

  24. Synthesis and Structure of High-Nuclearity Carboxylate-Modified Heteropolyoxovanadate Serving as a Heterogeneous Catalyst for Selective Oxidation of Alkylbenzenes

    Inorganic Chemistry · 2023-10-31

    Siyu Liu, Yuzan He, Xinyi Ma, Jiayu Liu, Pengtao Ma, Jingping Wang, Jingyang Niu

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  25. Controlling Electron Delocalization in Vanadium‐Based Hybrid Bronzes through Molecular Templation

    Angewandte Chemie International Edition · 2023-11-02

    Suchen Wan, Nicole Musielak, Allen G. Oliver, Adam Jaffe

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  26. Controlling Electron Delocalization in Vanadium‐Based Hybrid Bronzes through Molecular Templation

    Angewandte Chemie · 2023-11-02

    Suchen Wan, Nicole Musielak, Allen G. Oliver, Adam Jaffe

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  27. Visible-Light-Induced Oxidation of Styrene by a Polyoxovanadate-Based Carboxylate Derivative

    Inorganic Chemistry · 2025-01-07

    Yumei Hong, Sen Liu, Zhen Jing, Haojie Xu, Xiaodong Zhang, Pengtao Ma, Jingyang Niu, Jingping Wang

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  28. A Hybrid Bronze Age: Progress and Potential in Mixed-Valence Organic–Inorganic Metal Oxides

    Inorganic Chemistry · 2025-06-20

    W. Lakna N. Dayaratne, Raúl Torres-Cadena, Anton F. Walte, Suchen Wan, Joshua Morales Campos, Adam Jaffe

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